FINAL REMEDIAL ACTION REPORTforDebris Removal and ContainerizedHazardous Waste and Toxic Waste RemovalGambell , AlaskaDelivery Order No . 0004Contract . No . DACA85-97-D-0010November 5, 2001Oil Spill Consultants, Inc .209 East 51st AvenueAnchorage, Alaska 99503Telephone : (907) 562-7169Fax : (907) 562-7225NPDL WO# 99-092200-1fF10AK069601 _07 .08000 1_p"Oil Spill Consultants - A Commitment to Environmental Excellence"Final Remedial Action ReportforDebris Removal and ContainerizedHazardous Waste and Toxic Waste RemovalGambell, AlaskaTABLE OF CONTENTSPage1 .0 EXECUTIVE SUMMARY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12.0 BACKGROUND INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32.1 Site Location and Ownership . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32.2 Site History . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32.3 Project Scope of Work . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62.4 Project Planning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62.5 Land Access Fees . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.6 Applicable Regulations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.7 Delivery Order Modifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83 .0 COMMUNITY RELATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 .1 Population and Lifestyle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 .2 Services . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 .3 Economy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 .4 Community Benefits from Project . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 .5 Meetings Between Community Leaders and Project Manager . . . . . . . . . . 114.0 WORK DESCRIPTION AND EQUIPMENT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124 .1 Weather Conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124 .2 Physical Conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124.3 Findings at Project Sites . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 144.4 Project Equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 154.5 Clearing and Grubbing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 164.6 Metal Debris Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 164.7 Hazardous and Toxic Waste (HTW) Removal . . . . . . . . . . . . . . . . . . . . . . 184.8 Stained Soil Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 204.9 Contaminated Soil Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 214.10 Weights and Measurements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 224.11 Waste Shipment and Disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 224.12 Site Restoration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 224.13 Daily Quality Control Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 224.14 Safety and Health Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 225.0 SAMPLE COLLECTION AND LABORATORY RESULTS . . . . . . . . . . . . . . . . . . . 305.1 Data Quality Objectives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305.2 Waste Characterization . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305.3 Samples for Waste Identification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315 .4 Confirmation Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 415.5 Procedures for Sample Collection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 475.6 Personnel Collecting Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 485 .7 Sample Shipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 485.8 Chemical Data Quality Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48iFinal Remedial Action ReportforDebris Removal and ContainerizedHazardous Waste and Toxic Waste RemovalGambell, AlaskaTABLE OF CONTENTSPage6 .0 CONCLUSIONS AND RECOMMENDATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . 526 .1 Waste Shipped and Received . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 526 .2 Contaminant Reduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 526 .3 Work Limitations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 536 .4 Lessons Learned . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55LIST OF FIGURESFigure 1 :Project Location - Debris Removal and Containerized Hazardous Waste . . . . . . 4Figure 2 :Terrain Features - Northwest Cape , Saint Lawrence Island . . . . . . . . . . . . . 13Figure 3 :Site 8 - Sample Collection Locations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35Figure 4 :Site 12 - Sample Collection Locations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36Figure 5 : Site 2 - Sample Collection Locations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37Site 4/Area 4B - Sample Collection Locations . . . . . . . . . . . . . . . . . . . . . . . . 38Figure 6 :Figure 7 :Site 4/Area 4A - Sample Collection Locations . . . . . . . . . . . . . . . . . . . . . . . . 39Figure 8 :Site 6 - Sample Collection Locations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40LIST OF TABLESSummary of Metal Debris Quantities Removed from Gambell, Alaska . . . . . 17Table 1 :Table 2: Summary of HTW Quantities Removed from Gambell , Alaska . . . . . . . . . . . 19Table 3 : Manifest Tracking Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23Table 4 :Summary of Contractor Quality Control Reports . . . . . . . . . . . . . . . . . . . . . . . . 26Table 5 :Waste Identification Sample Results for Organics . . . . . . . . . . . . . . . . . . . . . 32Table 6 : Waste Identification Sample Results for TCLP Metals . . . . . . . . . . . . . . . . . . 33Table 7 : Waste Identification Sample Results for Dioxin . . . . . . . . . . . . . . . . . . . . . . . 34Table 8 : Confirmation Sample Results Summary for Organics . . . . . . . . . . . . . . . . . . 42Table 9 : Confirmation Sample Results for Total Metals . . . . . . . . . . . . . . . . . . . . . . . . 43Table 10 : Metal Results for Site 4/Area 4B Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . 45Table 11 : Confirmation Sample Results for Dioxin . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46Table 12 : Site4/Area 4B Pre-Excavation and Post Dioxin Results . . . . . . . . . . . . . . . . 54LIST OF APPENDICESAppendix A : Photo Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1Appendix B : Scale Tickets Showing Debris, HTW and Soil Weights . . . . . . . . . . . . . . B-1Appendix C : Waste Manifests and Certificates of Disposal . . . . . . . . . . . . . . . . . . . . . . C-1Appendix D : Daily Quality Control Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-1Appendix E : Laboratory Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-1Appendix F : Chain of Custody and Laboratory Data Reports . . . . . . . . . . . . . . . . . . . . F-1Appendix G : Data Deliverables for Project Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . G-1Appendix H : Safety and Health Phase-Out Report . . . . . . . . . . . . . . . . . . . . . . . . . . . . H-1Appendix I : Chemical Data Quality Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . I-1iiLIST OF ACRONYMSAAC Alaska Administrative CodeADEC Alaska Department of Environmental ConservationARARs Applicable or Relevant and Appropriate RequirementsATVs All-Terrain VehiclesCFR Code of Federal RegulationsCOC Chain of CustodyCQC Contractor Quality ControlC. T. & E . Environmental ServicesC. T . & E .CWMN Chemical Waste Management of the NorthwestDOT Department of Transportation (U .S.)DOT&PF Department of Transportation and Public Facilities (State of Alaska)DQCR Daily Quality Control ReportsDQO Data Quality ObjectivesDRO Diesel Range OrganicsEPA Environmental Protection AgencyFAA Federal Aviation AdministrationGRO Gasoline Range OrganicsHAZMAT Hazardous MaterialsHDPE High-Density PolyethyleneHTW Hazardous and Toxic Wastemg/kg Milligrams per Kilogrammg/L Milligrams per Literml MilliliterMS Matrix SpikeMSD Matrix Spike DuplicateNAO Northern Area OfficeOSCI Oil Spill Consultants, Inc .OSHA Occupational Safety and Health AdministrationPCB Polychlorinated BiphenylPES Philip Environmental ServicesPPE Personal Protective Equipmentppt Parts Per TrillionPQL Practical Quantitation LimitPWD Public Works DepartmentQAR Quality Assurance RepresentativeRCRA Resource Conservation and Recovery ActRRO Residual Range OrganicsSL Sample Matrix for SoilSVOA Semi-Volatile Organic AnalysisSVOC Semi-Volatile Organic CompoundsTCDD TetrachlordibenzodioxinTCLP Toxic Characteristic Leaching ProcedureTSCA Toxic Substance Control ActU UndetectedUSAEDA U .S . Army Engineer District, AlaskaVOA Volatile Organic AnalysesVOC Volatile Organic CompoundsIII1 .0 EXECUTIVE SUMMARYOn June 30 , 1998, the U .S . Army Engineer District , Alaska (USAEDA) contracted Oil SpillConsultants , Inc . (OSCI) to remove and dispose of metal debris , containerized hazardous andtoxic waste ( HTW) and contaminated soil located at Gambell , Alaska .In accordance with contract requirements, the following items were removed from the projectsite and shipped to the Lower-48 states for disposal :•HTW Removal . Approximately, 26 .8 tons of HTW (battery, parts, dried paint, drums andtransformer carcasses) were collected from five locations at the project site .•Metal Debris . Based on field weights, 142,234 pounds of metal debris consisting ofrunway matting , cable , fuel tanks and equipment parts were removed from sitesidentified by USAEDA .•Contaminated Soil . Workers using picks and shovels excavated 52 tons ofcontaminated soil from Sevuokuk Mountain .•Stained Soil . A total of 20 tons of petroleum-stained soil were excavated from severalsites at Gambell .Twenty-seven connex containers and one 20-foot flat loaded with project waste departedGambell, Alaska, on August 26, 1999, and arrived at the designated disposal facilities duringmid-November 1999 . Metal items (including empty drums) and petroleum contaminated soilwere shipped to Rabanco Recycling in Seattle, Washington . Contaminated soil and HTW wereshipped to Chemical Waste Management in Arlington, Oregon, and Burlington Environmental,Inc . in Seattle, Washington, respectively .Fifty-two tons of contaminated soil were removed from Site 4/Area 4B . Samples from theexcavated area revealed that the residual diesel range organics (DRO) level ranged from 24 .8to 13,900 milligrams per kilogram (mg/kg) . By comparison, the State of Alaska cleanup levelfor DRO under Alaska Department of Environmental Conservation (ADEC) Method 2 is 250mg/kg for the project site . Other analytes detected in the samples from Site 4/Area 4B werebelow regulatory thresholds established by the State of Alaska and the U .S . EnvironmentalProtection Agency (EPA) . Residual dioxin levels in the excavation at this site ranged fromnon-detect to 1,250 parts per trillion .Several soil stains were removed from Site 4/Area 4A and Site 12 . Confirmation samples showthat the residual DRO levels in these areas are 1,310 mg/kg and 463 mg/kg, respectively . Theresidual total chromium level for Site 4/Area 4A was 422 mg/kg . Residual total lead for Site12 was 562 mg/kg . ADEC Method 2 cleanup levels for chromium and lead are 26 mg/kg and400 mg/kg, respectively .From start to finish, 45 days were required to complete all site work . Despite difficultenvironmental conditions (wet tundra, large boulders restricting access to work sites onSevuokuk Mountain, and reduced visibility due to fog and low ceilings), there were noaccidents or spills . This is particularly noteworthy since most of the project labor was provided1by local residents . (Prior to project startup, local Gambell residents experienced three seriousaccidents . However, daily safety meetings and adherence to established safety protocolprevented problems while work was in progress .)A photo summary of project activities is provided in Appendix A . Scale tickets showing debrisand soil weights are provided in Appendix B . Waste manifests and certificates of disposal arein Appendix C . Daily quality control reports are provided in Appendix D . Laboratory data forproject samples is summarized in Appendix E . Chain of custody forms for project samples andlaboratory data reports are in Appendix F . Data deliverables for project samples are inAppendix G . The Safety and Health Phase-Out Report for this report is in Appendix H . Achemical data quality review is provided in Appendix I .22 .0 BACKGROUND INFORMATION2 .1 Site Location and OwnershipAs shown in Figure 1 , Gambell , Alaska , is located on the northwest cape of St . LawrenceIsland , 200 miles southwest of Nome, Alaska at 63 ° 47' N Latitude, 171 ° 45' W Longitude(Section 03,TO20S,R067W, Kateel River Meridian) .St. Lawrence Island has two villages, Gambell and Savoonga . Under the 1971 Alaska NativeClaims Settlement Act, Gambell residents established Sivuqaq Incorporated . Residents inSavoonga established Savoonga Incorporated . Following this, the federal governmentawarded a joint title to all land on St . Lawrence Island to these corporations .Points of contact for this project are :USAEDANAOUSAEDA(Alaska DistrictNamePaul SchneiderSusan BeachampPatricia OwenJob KoonookaPatty MillerTitleResidentEngineerProject ManagerNorthern RegionProject ManagerPresidentHead ofAviation DesignAddressU .S . ArmyEngineer District,Northern AlaskaArea OfficeP .O . Box 355066Ft . Wainwright,Alaska 99703-0066U .S . ArmyEngineer DistrictP .O . Box 898Anchorage, Alaska99506-0898222 W . 7`hAvenue, #14Anchorage,Alaska 99513Sivuqaq Inc .P .O . Box 101Gambell,Alaska99742State of AlaskaDOT & PF2301 PegerRoadFairbanks,Alaska 99709PhoneNumber(907) 353-7850(907) 451-2275(907) 271-5445(907) 985-5826(907) 451-2275Point ofContactFederal AviationAdministrationState of AlaskaDepartment ofTransportation& PublicFacilitiesDOT&PFSivu a Inc .2.2 Site HistoryFrom 1948 through the late 1950s, the U . S . Air Force, Army and Navy conducted limitedmilitary activities sites in Gambell, Alaska . Based on previous investigations performed for thegovernment by Ecology and Environment under Contract No. DACA85-91-D-003, the militaryestablished the following sites at Gambell :•Site 2 - Former Housing and Operations Center . A military housing and operationscenter was located at this site . It included 12 Quonset huts, a dining hall, a utilitybuilding and a small power plant . These structures were demolished by the militaryprior to demobilizing from Gambell . The ground at this site contains about 1,600pounds of metal debris ( weasel tracks, metal boxes and wire), one drum and severalsoil stains that resulted from previous military activities .3Figure 1 : Project Location4•Site 3 - Former Communications Facility . A 75 ft. by 45 ft . communications facility waslocated at this site . It included an electrical power plant, fuel storage tanks and twoJamesway huts for equipment and personnel shelter . Surface debris at this site includea fuel storage tank, weasel tracks, aircraft landing mat and drums . The weight for thisdebris is estimated at 1,800 pounds .•Site 4 - Former Air Force Radar Station . This site is located on the top of SevuokukMountain (600 ft . above sea level) . It contained a 375 ft . by 500 ft. radar station whichwas used to monitor Russian ships in the Bering Sea . Site 4 also had two Quonset hutsfor personnel shelter and several transformers which were part of the system thatdelivered electrical power from other locations to the radar station . A tram at Site 5and a trail through Site 10 were used to access to Site 4 . (Overland access to Site 4is limited by large boulders on Sevuokuk Mountain and wet tundra in Site 10 .)Site 4 contains about 7,300 pounds of metal debris which consists of siding and framesfrom Quonset huts, drums and wire . It also contains 4,370 pounds of HTW (drums,transformers, engine blocks and generators) . Along with this, Site 4 has a surfacestain that may contain up to 52 tons of contaminated soil .•Site 5 - Former Tramway Site . Site 5 is on the northwest face of Sevuokuk Mountainand served as the location for a tram which transported personnel and equipment toSite 4 . This site also served as the corridor for sonar and electrical cables . It containsapproximately 370 pounds of scattered metal debris .•Site 6 - Former Military Landfill . A 275 ft . by 135 ft . landfill was constructed at this site .Along with metal drums filled with human waste, materials from a power plant andcommunications facility may be buried in the landfill . (The landfill is covered withgravel .) Surface debris from previous government activities at this site is limited to 350pounds of metal (drum remnants, landing mat, wire and weasel tracks) .•Site 7 - Former Military Power Facility . Based on previous investigations, a militarypower plant was located at this site . The ground at this site contains about 150 poundsof miscellaneous metal debris .•Site 8 - West Beach . This 3-mile long area is located on the west site of TroutmanLake . It begins near the northwest end of Gambell and extends southward toNayvaghaq Lake . The military placed metal landing mats in this area to support aircraftoperation . At several locations in Site 8, storms have removed the gravel and exposedthe landing matting . It is estimated that this site contains at least 115,000 pounds oflanding mat and several drums filled with asphalt .Site 8 also contains a 4,500 ft . paved runway . Energized electrical cables for therunway lights are buried in the gravel next to the runway .•Site 10 - Sevuokuk Mountain Trail System . As shown in Figure 1, these trails start nearthe south end of Troutman Lake and provide access to a former radar station locatedat Site 4 on the top of Sevuokuk Mountain . Military personnel placed over 150 metaldrums at 200 ft . intervals to mark the trails . Site 10 also has about 1,300 pounds ofweasel tracks . (Due to the presence of wet tundra in Site 10, track-mounted vehiclesshould be considered for using the trail system during the summer months .)5•Site 12 - Nayvaghaq Lake Disposal Area . This site is located between Nayvaghaq Lakeand Troutman Lake . Along with several stains, it has 66 drums and 10 lead-acidbatteries on the ground .•Site 13 - Former Radar Power Station . This site is located near the south end ofTroutman Lake and previously contained three wooden buildings and several 150-ft .towers . About 300 pounds of metal pipe and wire from the radar power station remainon the ground at Site 13 .Prior to demobilizing, the military demolished most of the buildings that were constructed tosupport its operations in Gambell, Alaska. Reports prepared by Ecology and Environment andMontgomery Watson for the USAEDA Contract Numbers DACA85-91 -D-0003 and DACA8593-D-001 1 state that the demolition debris and most of the military equipment were buried onsite .2.3 Project Scope of WorkUnder Delivery Order No. 0004 for Contract No . DACA85-97-D-001 0 issued on June 30, 1998,USAEDA requested OSCI to remove the following items from Gambell, Alaska :•Hazardous and Toxic Waste (HTW) . A total of 8 .5 tons of hazardous and toxic wastewere identified for shipment to government-approved disposal facilities in the Lower-48states . This waste included lead-acid batteries, transformers, asphalt, generators,engine blocks, storage tanks, empty drums, and stained soil in locations containingHTW .•Metal Debris. The delivery order required removal and disposal of 64 tons of metaldebris from various sites at Gambell, Alaska . This debris consisted of metal runwaymatting near the Gambell airport landing strip, abandoned communication cable andcable spools, sheet metal, metal frames, pipes and parts from track-mounted vehicles .•Contaminated Soil . Area 4/4B on Sevuokuk Mountain had a soil stain which resultedfrom a previous spill . The scope of work required the contractor to remove and ship52 tons of soil from the stained area to government-approved disposal facilities in theLower-48 states .•Stained Soil . Several sites identified in the project scope of work contained petroleumstained soil . The delivery order required the contractor to remove and provide offsitedisposal for 20 tons of stained soil from these sites .Work at the project site began on July 5, 1999, and was completed on August 18, 1999 .2.4 Project PlanningThe following project plans were prepared by OSCI and approved by USAEDA to support thisproject :• Work Plan . This document includes the project schedule and identifies the scope ofwork on a site-by-site basis . Along with this, it delineates responsibilities for project6personnel, discusses mobilization, and identifies the sources for project resources . Thework plan also addresses steps used to remove, segregate, and quantify the waste bycontract line items and track waste movement from the project site to Lower-48 disposalfacilities .•Site Safety and Health Plan . This plan identifies site safety requirements, discussesaccident prevention, and outlines the steps for complying with EM 385-1-1 . It includesa hazard analysis for each work feature, lists precautionary measures for handlingHTW, and describes procedures for identifying and resolving safety problems at theproject site .•Contractor's Quality Control Plan (QCP) . This plan outlines OSCI's provisions forassuring the scope of work is completed in accordance with contract specifications . Itdescribes the company's quality control (QC) program and lists responsibilities forOSCI's QC personnel . The QCP also identifies potential QC problems for each workfeature and describes corrective actions . This plan also discusses OSCI's proceduresfor weighing the HTW, debris, and contaminated soil removed from each project site .•Sampling and Analysis Plan . This plan identifies : 1) data quality objectives for meetingU .S. EPA and Department of Transportation (DOT) waste identification and shippingrequirements, 2) the number of samples that would be collected at the project site, and3) analytical methods for each sample . It also discusses OSCI's field screening andsample handling procedures .•Waste Management Plan . This plan lists the project waste streams and discussesOSCI's procedures for waste identification, tracking, weighing, packaging, and storageat the project site . It also includes the steps for waste labeling, land ban restrictionnotifications, and manifest preparation . In addition, the waste management plan listscompanies identified for waste transportation and disposal .•Environmental Protection Plan . This plan outlines steps for protecting and restoringareas accessed by OSCI for HTW removal . As part of this plan, track-mounted vehicleswere used to transport personnel , HTW, contaminated soil, and debris across wettundra . It also explains how trails through the wet tundra will be seeded and fertilizedto minimize the potential for soil erosion ; how plastic liners will be used to protect theground in areas used for equipment and HTW storage ; and how graders will be usedto restore smooth surfaces on gravel beaches .2.5 Land Access FeesSivuqaq Incorporated levies a $100 .00 access fee for each person who crosses its land . Underarrangements made by USAEDA, neither OSCI nor its subcontractors had to pay this fee whileperforming project activities on the corporation's land . However, this fee was required if OSCI'spersonnel used the corporation's land for recreation or other activities .2.6 Applicable RegulationsHazardous and toxic waste included identified in the project scope of work was handled,transported and disposed of in accordance with the following regulations :7•29 CFR 1910 .120 . Under this section of the Code of Federal Regulations (CFR),persons handling or working in areas containing hazardous or toxic materials wererequired to complete a 40 -hour HAZWOPER or an 8 -hour HAZWOPER refresher(if the one-year certification for the 40-hour HAZWOPER had expired ) course priorbeginning work . These courses familiarized the worker with the procedures forwearing and caring for personal protective equipment , material safety data sheets,and steps for personnel decontamination .•40 CFR 261 . This regulation provides the criteria for determining if a substance isa hazardous waste . It also provides EPA codes that must be placed on hazardouswaste labels and manifests . Additionally , it provides criteria or determining if asubstance meets the EPA definition for hazardous waste under toxicitycharacteristic leaching procedure (TCLP) .•40 CFR 263 . EPA requirements for hazardous waste manifests , record keeping andspill cleanup are cited in this regulation .•40 CFR 761 . EPA requirements for handling, labeling and storing PCBcontaminated wastes are defined in this regulation . This regulation also establishesregulatory thresholds for liquids containing PCBs and PCB contaminated waste .•49 CFR 172. U .S . DOT requirements for waste shipping names, packagingmaterials, and hazard class identification are provided in this section of CFR .•18 AAC75 .341, Method 2 . This section of the Alaska Administrative Code definessoil cleanup levels for petroleum , chemical , PCB, and metal contamination .2.7 Delivery Order ModificationsThe following modifications were issued for Delivery Order 0004 :•Full-Time Archeologist . The delivery order included 10 days for an Archeologist at theproject site . Due to the possibility of encountering items that may have cultural orarcheological significance, the delivery order was modified to include : 1) a full-timeArcheologist for the project duration, 2) a separate vehicle for the Archeologist, and 3)additional report writing for the Archeologist if significant findings were discovered .•Corporation Meeting Attendance . Sivuqaq Incorporated requested USAEDA and OSCIrepresentatives to attend a March 25, 1999 public meeting in Gambell, Alaska, todiscuss Delivery Order 0004 . A modification was issued to cover OSCI's cost formeeting attendance .•Increase HTW Removal . The original delivery order identified 8 .5 tons of HTW forremoval and disposal . A modification was issued to increase the HTW quantity to 24tons .•Road Access at Project Site . The negotiated delivery order included one truck and four4-wheel all-terrain vehicles (ATVs) with trailers for hauling metal debris andcontaminated soil at Gambell . During April 1999, a USAEDA representative advisedOSCI that these vehicles were not suitable for the steep terrain on Sevuokuk Mountain .8He recommended replacing the ATVs with a Nodwell and several Argos . In responseto this, OSCI requested and USAEDA issued a modification which allowed three of the4-wheel ATVs to be replaced with one track -mounted Nodwell and two track-mountedArgos .•Revised Unit Cost for Contaminated Soil Removal . Drawings provided by USAEDAshowed well-defined trails to the contaminated soil removal area on SevuokukMountain . On arriving at the project site, OSCI discovered that there were no trails toSite 4, Areas 4A, 4B, and 4D on Sevuokuk Mountain . Instead, this area was surroundedby large boulders which prevented access by trucks, excavation equipment, and largetrack-mounted vehicles such as the Nodwell . In view of this, a modification was issuedfor revising the unit cost for removing contaminated soil from Site 4, Area 4B usingshovels, sand bags and Argos .•Delete Debris Removal Near Buried Power Line . The delivery order required OSCI toremove 64 tons of metal matting near the Gambell airport runway . While performingthis work, an energized cable for the runway lights was discovered near a portion of themetal matting . A modification from USAEDA deleted the requirement to remove themetal matting near the energized cable .•Increase Quantity for Metal Debris Removal . The debris quantity was increased from64 to 71 tons . This included an additional 410 linear feet of metal matting, 2 .2 miles ofNavy sonar cable, cable reels and one metal cargo sled .•Additional Sampling and Analyses . The delivery order included one sample to satisfywaste disposal facility acceptance criteria for soil excavated from Site 4, Area 4B . Amodification was issued to collect four post excavation confirmation samples from thissite . (This modification also included one quality control and one quality assurancesample .)•Confirmation Samples . A modification expanded the scope of work to include 10confirmation samples from areas that appear to have contamination . These sampleswere to be tested for GRO by AK1 01, DRO by AK1 02, RRO by AK1 03, VOC by EPAMethod 8260, VOA by EPA Method 8270, PCBs by EPA Method 8082 and Pesticidesby EPA Method 8081 .93.0 COMMUNITY RELATIONS3 .1 Population and LifestyleGambell , Alaska , is a small community which has about 525 full-time residents (Photo 1) . Mostresidents are Yup'ik Eskimos who depend on birds , fish, marine mammals and reindeer forsubsistence .3 .2 ServicesTwo commuter airlines provide four flights per day from Nome, Alaska, to Gambell, Alaska .There is no airport terminal in Gambell . The village is approximately 1/2 mile from the landingstrip . Since there are no taxis or public transportation in the village, persons traveling toGambell must make advance arrangements for someone to meet them at the runway .The village normally receives one cargo barge per year (Photo 2) and up to two fuel barges peryear . During the summer months, several small cruise ships visit the village .Sivuqaq Incorporated operates a 15-room lodge in Gambell (Photos 3 through 6) . It has a fullkitchen which prepares fast food for the community . Persons staying in the lodge can orderfrom the menu or use the kitchen to prepare their own meals .3 .3 EconomyCommercial activities in Gambell are limited to a small Native store which caters to the localcommunity and Sivuqaq Lodge which caters to bird watchers during the summer months . Jobsare limited to a few positions offered by the school, post office, power plant, city government,tribal council, the local store and local Native corporation (which owns the lodge) .The village corporations (Sivuqaq, Inc . and Savoonga, Inc .) own all land and mineral rights onSt. Lawrence Island . As a result, they generate revenue by selling gravel to the State of Alaskafor airport runway construction and maintenance . These corporations also charge fees topersons and organizations that use their land for recreation or bird watching .When jobs are not available, Gambell residents depend on state assistance . Some residentsmake and sell ivory carvings to tourists who visit the island .3 .4 Community Benefits from ProjectUnder USAEDA specifications for this project , all site workers were required to meetOccupational Safety and Health Administration (OSHA) hazardous materials (HAZMAT)requirements (29 CFR 1910 .120 ) for handling contaminated soil and hazardous waste . Sincethere were only six persons in Gambell who met this requirement , the following steps weretaken to maximize employment opportunities for local residents :• Tasks Restricted to HAZMAT Workers. Work such as contaminated soil excavation,drum handling , transformer packaging and battery handling was limited to residentswho had met the OSHA HAZMAT requirements . This work was supervised by PhilipServices Corporation .10•Tasks Set-Aside for Non-HAZMAT Workers . The project scope of work required OSCIto remove 115,000 pounds of metal landing matting from Site 8 . Since this debris wasnot contaminated or in areas containing HTW, persons handling it were not required tomeet the OSHA HAZMAT requirements cited in 29 CFR 1910 .120 . After obtaininggovernment approval, OSCI hired local workers who did not have HAZMAT training toremove, cut and package metal landing . They were also used to remove wire and othermetal debris from areas that did not contain HTW .Local residents provided 61 percent of the total project labor hours and received $86,302 inwages .To support the local community, OSCI purchased meals and lodging from the Sivuqaq Lodgeat a cost of $33,715. Along with this, OSCI spent $4,839 for food and fuel at the communitystore. In summary, this project contributed $124,856 to Gambell's economy .OSCI shipped $3,000 worth of canned goods and dry food to Gambell for crew meals . Lessthan 50 percent of this was consumed by the project personnel . Excess food was given tolocal residents and several Siberian Eskimos who were visiting Gambell . OSCI also gave acomputer and printer to a local family . The company sold a full-size refrigerator, microwaveoven, VCR and television to various residents for less than 10 percent of the purchase cost .3.5 Meetings Between Community Leaders and Project ManagerThe Gambell Mayor and Sivuqaq Board of Directors requested several meetings with OSCI'sproject manager. During each meeting, they questioned the steps OSCI was taking to hiremore local workers . Although local workers received 61 percent of the man-hours devoted toproject labor, the mayor and board of directors encouraged OSCI to provide training soGambell residents could fill all labor and equipment operator positions during futureenvironmental remediation projects on St . Lawrence Island .114.0 WORK DESCRIPTION AND EQUIPMENT4.1 Weather ConditionsGambell, Alaska, has a maritime climate with average summer temperatures ranging from 34to 48 °F . Average winter temperatures range from -2 to 10 °F .Project work began on July 6, 1999, and was completed on August 17, 1999 . During thisperiod, temperatures ranged from a low of 39 °F to a high of 55 °F . Based on data from aweather station at the Gambell airport runway, wind speeds ranged from 0 to 35 knots duringthis project .This delivery order required OSCI to remove 170 tons of debris, HTW and contaminated soilfrom Gambell . Approximately, 40 percent of this material was located on the top of SevuokukMountain (600 ft . above sea level .) Each day, low ceilings covered this area with dense fog .Surveyor's stakes with colored tape were used to mark routes on the mountain top and wettundra in Site 10 . This made it possible for personnel to navigate during reduced visibility .No significant project delays were caused by weather . Due to blowing rain and dense fog, nowork was performed on August 4, 1999 . No accidents or spills resulted from weatherconditions at the project site .4.2 Physical ConditionsThe following conditions were observed when OSCI arrived at the project site on July 5, 1999 :•Loose Gravel on North Beach . Project equipment and connex containers for wasteshipment were mobilized to Gambell, Alaska, by Northland Services . Due to wind andsea conditions, the barge offloaded these items on the north beach (Figure 2) . Thisbeach has loose gravel and could not provide a stable working surface for personnelor equipment . While walking on this beach, personnel would sink 3 to 6 inches witheach step . The company's 4-wheel drive truck was frequently stuck in the beach gravel .Small trailers loaded with debris bottomed out in the gravel .•Hard Packed Gravel on South Beach . In view of poor conditions on the north beach,OSCI set up an equipment staging area on the south beach where the gravel was hardpacked and would support both equipment and personnel . At this location, metaldebris, soil, and HTW were weighed with an electronic scale and placed in connexcontainers .•Limited Road System . As shown in Figure 2 and Photo 37, a hard-packed gravel roadis located on the east, west and south side of Troutman Lake . This road starts at therock quarry near the east side of the lake . It ends near the Gambell School . Therewere no roads through the housing area or trails through Site 4 or Site 10 .•Wet Tundra . Site 10 consisted of wet tundra that could not be crossed by trucks orheavy equipment . As shown in Photo 38, 4-wheel ATVs were frequently stuck whilecrossing the tundra . As noted in Photo 39, a track-mounted Nodwell was able to12Figure 2 : Terrain Features - Northwest Cape, Saint Lawrence Island13cross the tundra . However, initial testing showed that the tracks on this vehicle causedextensive tundra damage (Photo 40) . In view of this, Nodwell use was restricted togravel surfaces at the project site .•Boulder Field on Mountain Top . Site 4 is located on top of Sevuokuk Mountain . Largeboulders on the mountain (Photos 24 and 52) prevented site access by trucks or heavyequipment .•Low Ceilings Reduce Visibility on Mountain . The top of Sevuokuk Mountain isapproximately 600 ft . above sea level . At least 85 percent of the time, low ceilingsreduced visibility on the mountain top to 50 ft . or less .•High Water Table . Site 12 (Photo 45) contained dried paint, batteries and several largesurface stains that may have resulted from leaking drums . Due to its proximity toTroutman Lake, Nayvagag Lake and the Bering Sea, this site has a high water table .During calm weather, the water table was 6 to 8 inches below grade . When low windsoccurred, about 20 percent of this site was under water .4 .3 Findings at Project SitesThe scope of work identified nine sites at Gambell, Alaska, that contained soil, metal debris orHTW designated for removal under Delivery Order 0004 . The following items were found ateach site :•Site 2 - Petroleum Contaminated Soil . Site 2 (Photo 7) is at the base of SevuokukMountain, about 3/4 miles northeast of the Gambell school and 150 yards from theBering Sea shoreline . Based on pictures provided in the scope of work, this site wasidentified by small cable reels surrounding a large rock . All of the soil within 49 feet ofthis rock contained heavy petroleum stains . At the base of the rock, the stain was 2 ft .deep . At 49 ft . from the rock, it was 3 inches deep . Laboratory analyses revealed thatthe stained soil contained gasoline range organics (GRO) at 309 mg/kg, diesel rangeorganics (DRO) at 6,440 mg/kg and residual range organics (RRO) at 388 mg/kg . Nometals, pesticides or PCBs were detected in this soil .•Site 3 - Tanks and Metal Debris . Site 3 (Photos 10 through 12) was on the southwestslope of Sevuokuk Mountain . It started at ground level and ascended to approximately400 ft above grade . Three empty fuel tanks and several sheets of metal siding werefound at this site .•Site 4 - Contaminated Soil Metal Debris, and Transformers . As shown in Figure 2, Site4 is on the top of Sevuokuk Mountain . Pictures provided by the government made itpossible to identify Areas 4A, 4B and 4D . A generator was located near Area 4B .Additionally, Area 4B contained a large area of contaminated soil identified forexcavation during this project . Area 4D included metal debris from two Quonset huts(Photo 13) and three empty transformers (Photo 14) .Together, Areas 4A, 4B and 4C were at least 300 ft . long by 300 ft. wide. Wind blownmetal debris was lodged between the boulders throughout these areas . Skeletalremains and burial boxes were found near Area 4D . (These items were handled byOSCI's Archeologist and local residents from Gambell .)14As discussed in Section 2 .6, there were no trails to the project areas on SevuokukMountain . It was necessary to cross 1 .6 miles of wet tundra (Photo 41) to reach theseareas .•Site 5 - Metal Debris . This site was on the southwest slope of Sevuokuk Mountain . Itstarted at ground level and ended at the mountain top . Due to a steep slope containingjagged rocks, it was impossible to inspect this site at elevations above 450 ft . Thelocations which were inspected contained small pieces of metal debris .•Site 6 -HTW . Site 6 was near the Gambell school . It contained a stack of empty drums(Photos 25 and 26) . Local residents said these drums were excavated from the sitewhere the school was constructed .•Site 8 - Metal Debris . This site included all of the area west of Troutman Lake betweenthe contractor's main staging area on the south beach and the container staging areaon the north beach . As shown in Photo 27, this site contained an unknown quantity ofmetal runway matting . In some areas, the matting was fully exposed . In other areasit was covered with up to 1 ft of gravel . (Based on comments from Gambell residents,the metal runway matting presents a safety hazard for persons operating 4-wheel ATVsduring reduced visibility resulting from fog or blowing snow .)Site 8 also included a large metal sled (Photo 33), drums containing asphalt and a smallsteam boiler .•Site 10 - HTW . Hundreds of empty 55 - gallon drums were located in this site (Photo 41) .Based on comments from local workers , Gambell residents strategically placed manyof the drums so they would serve as trail markers for persons traveling to remotecamps . The terrain throughout most of Site 10 consisted of wet tundra that could notbe crossed with trucks or heavy equipment .•Site 12 - HTW . This site was on the road system at the south end of Troutman Lake .It included dozens of drums, batteries, dried paint and miscellaneous metal debris(Photos 43 through 48) . Most of the drums were punctured . This along with large soilstains suggests that some of the drums were allowed to drain at Site 12 .•Site 13 - HTW . Site 13 was also on the road system at the south end of Troutman Lake .It contained a few drums and several small pieces of metal debris .4.4 Project EquipmentThe following equipment was mobilized from other areas to Gambell, Alaska, for projectsupport :•Crew Transportation . Two 4-wheel ATVs , two track-mounted Argos and one crew cab4-wheel drive Ford pickup truck were shipped from Anchorage to Gambell by barge forcrew transportation . Four additional Argos were shipped to the project site by airfreight . Two additional 4-wheel ATVs were transported to the island by barge fromNome , Alaska .15•Soil and Debris Hauling . One Nodwell track-mounted vehicle along with the pickuptruck was mobilized for hauling soil, HTW and debris at the project site .•Heavy Equipment . A backhoe was leased from the Gambell Public Works Department(PWD) for excavating soil and loading items into connex containers . A 966 front-endloader was leased from a local construction company for moving empty connexcontainers and placing metal on the Nodwell . A 973 dozer with forks was leased fromthe Gambell PWD for moving connex containers filled with metal debris, soil or HTWto a location where they could be placed on a barge for demobilization .Fuel for Equipment . Gasoline and diesel fuel were purchased from the Gambell NativeStore . Once during this project, the store ran out of fuel . The fuel barge to Gambellwas delayed for a week by high winds . (It was possible to continue project activitiesbecause several drums of fuel were included with the equipment mobilized fromAnchorage .)•Miscellaneous Equipment . A pressure washer, drum crusher, demolition saws, cuttingtorches, pumps, scales, plastic fencing, hand tools, personal protective equipment,plastic liners, first aid equipment and sorbent materials were mobilized from Anchorage .Field screening and sampling equipment were also shipped from Anchorage .Clearing and Grubbing4.5No clearing or grubbing was required for this project .4 .6 Metal Debris RemovalTable 1 summarizes the metal debris removed from Gambell, Alaska, under Delivery Order No .0004 . This debris was characterized as follows :•Metal Runway Matting . About 67 percent of the debris (95,290 pounds) consisted ofmetal runway matting from Site 8 . Prior to removing this material from the ground,workers used demolition saws and propane torches to cut it into sections that could belifted with a 966 front-end loader . Following this, the loader placed the sections on aNodwell which hauled them to a lay down area (Photos 28 through 30) . At this location,the matting was cut into smaller sections (if required), weighed by an electronic scaleand placed in connex shipping containers .While work was in progress, energized electrical power cables were discovered on theeast side of the Gambell airport runway (Photo 32) . To avoid problems, the governmentinstructed OSCI to leave the matting in place (1,820 linear feet) near the cable . Basedon visual observation, less than 50 percent of the metal matting in Site 8 was removedduring this project .Metal Sled . A 12,800 pound sled was removed from Site 8 . It was cut into pieces,weighed and placed on a shipping flat for transportation from Gambell to Seattle,Washington .16Table 1Summary of Metal Debris Quantities Removed from Gambell, AlaskaDelivery Order No . 0004, Contract No . DACA85-97-D-0010Project SiteDebris Quantity Estimatedby Delivery OrderPoundsActual Quantity ofDebris RemovedPounds21,600037701,8804/Area 4A5,41012,3484/Area 4B9051,0524/Area 4D1,0006,96853156,268Between 5 and 3551,44163501,748715008115,000108,090101,3001,388121079813300343Total127,255142,324Notes:1 . Scale tickets showing field weights for metal debris are provided in Appendix B .2 . Metal debris was shipped from Gambell, Alaska, to Rabanco Recycling in Seattle,Washington for disposal . Manifests are provided in Appendix C .17•Cable, Wire and Weasel Tracks . A total of 13,866 pounds of miscellaneous metaldebris consisting of wire, cable, cable spools, weasel tracks and a steam boiler werecollected from Sites 3, 5, 6, 10, 12 and 13 . These items were placed in trailers pulledby ATVs and hauled to a lay down area for weighing, cutting and placement in connexcontainers .•Quonset Hut Debris and Metal Siding . Debris from Site 4 (Areas 4A, 4B and 4D)included 20,368 pounds of metal framing and siding from Quonset huts on SevuokukMountain . This material was manually removed from the ground and placed in trailers .Afterward, the trailers were pulled down the mountain by Argos (Photos 15 through 17) .When the Argos reached the access road around Troutman Lake, the debris wastransferred to a pickup truck and transported to a lay down area for weighing, cuttingand placement in connex containers (Photos 18, 34 and 36) .4 .7 Hazardous and Toxic Waste ( HTW) RemovalTable 2 lists the HTW quantities removed from each site at Gambell . For this project, HTWincluded fuel tanks, generators , engine blocks, asphalt, batteries , paint and empty drumspreviously containing unidentified materials .Under the original scope of work, OSCI was required to remove 16,140 pounds of HTW fromGambell . A modification issued by USAEDA, increased the HTW quantity to 53,738 pounds .This material was transported from the project site under the following U .S . DOT approvedshipping names :•Hazardous Waste , Solid, N .O.S . 9, NA3077, PG III, (D008) . Shovels were used toremove stained soil (601 pounds ) from areas at Site 12 that previously containedbatteries . This soil was placed in a 55-gallon drum . Based on laboratory results whichidentified high lead levels , it was shipped to Burlington Environmental Services inSeattle , Washington as Line Item 11 .a. on Manifest GAM02 .•Waste Tars, Liquid, 3, UN 1999, PG II, (D001) . Nine drums of asphalt were removedfrom Site 8 . Each drum was placed in an 85-gallon overpack container and shipped toBurlington Environmental Services in Seattle, Washington for disposal . The total weightfor these drums (4,458 pounds) was noted in Line Item 11 . b . on Manifest No . GAM02 .•Hazardous Waste , Solid, N .O.S . 9, NA3077, PG III, (D008 ) . Five 5-gallon cans of driedpaint (378 pounds ) were found in Site 12 . They were placed in an 85-gallon overpackand shipped to Burlington Environmental Services as Line Item 11 .c. on ManifestGAM02.•Environmentally Hazardous Substances , Solid, N .O .S. 9, UN3077, PG III (D008) .Several deteriorated lead acid batteries were found at Site 12 . Personnel wearing Level"C" personal protective equipment (PPE) packaged the batteries (619 pounds) in aplastic fish tote . Following this, the batteries were shipped to Burlington EnvironmentalServices as Line Item 11 .d. on Manifest GAM02 .18Table 2Summary of HTW Quantities Removed from Gambell , AlaskaDelivery Order No . 0004, Contract No . DACA85-97-D-0010Project SiteDebris Quantity Estimatedby Delivery OrderPoundsActual Quantity ofDebris RemovedPounds220036001,1504/Area 4A2,1402,4244/Area 4B2,2301,7644/Area 4D06,00850470Between 5and31000607,89770086,20012,807102,30012,516122,5508,7021300Total16,14053,738Notes :1 . Scale tickets showing field weights for metal debris are provided in Appendix B .2. Metal debris was shipped from Gambell, Alaska, to Burlington Environmental in Seattle,Washington for disposal . Manifests are provided in Appendix C .19•Non-RCRA Waste Solid . About 450 drums (including drum parts) were collected fromSites 3, 4A, 4D, 6, 8, 10 and 12 . Prior to being moved, each drum was inspected byexperienced HAZMAT personnel to discern which ones contained compatible materialsor required special handling to prevent spills .Most of the drums were previously punctured (by an unknown party) or contained openingscaused by natural deterioration . As a result, all of the drums were either empty or containedonly a few ounces of rainwater . For all sites except Sites 4 and 10, the drums were placed onthe back of a pickup truck (Photo 46) and transported to a staging area where they were placedon a liner, cleaned, crushed and weighed (Photo 34) . Following this, they were placed in aconnex shipping container.Drums in Sites 4 and 10 were placed in trailers towed by ATVs . Once the drivers reached theroad system , the drums were transferred to a pickup truck and transported to a staging areafor cleaning , crushing , weighing and packaging .All drums were shipped to Rabanco Recycling in Seattle, Washington, on Manifests GAM01,GAM12, GAM13, GAM14 and GAM15 . Empty transformers, engine blocks and generatorswere also shipped to Rabanco Recycling as Non-RCRA Waste Solid on Manifest No . GAM12 .(Laboratory testing revealed that the transformers did not contain PCBs . The engine blocksand generators did not contain fuel, fluid or lubricating oil .)4.8 Stained Soil RemovalBased on visual inspections, stained soil was identified at the following locations :SiteSoil RemovedPounds224,9824/Area 4A1,8774/Area 4D46384,79010540127,237At Site 2, dark stains were limited to an area surrounding a large boulder (Photos 7 through 9) .Heavy oil stains were present 3 ft . below grade at the base of the boulder . At 30 ft . from theboulder, the stains were 8 inches below the surface .After OSCI filled 24 supersacks with oil stained gravel (24,982 pounds) from Site 2, thegovernment's on-site Quality Assurance Representative (QAR) suspended further excavationpending clarification as to whether sufficient material should be removed to obtain site closureunder Alaska's oil pollution regulations .20After reviewing an environmental investigation for Gambell , Alaska , the QAR determined thatSite 2 was previously identified as an oil spill site and should not have been listed as a stainedsoil site under Task Order No . 0004 . Comments from local workers revealed that thepetroleum stain at this site probably resulted from oil that was drained from ATVs by Gambellresidents . In view of this, the QAR directed OSCI not to remove anymore stained gravel fromthis location .The 24 supersacks of stained gravel from Site 2 were identified as a Non-RCRA Waste Solidand shipped to Rabanco Recycling in Seattle, Washington for landfill disposal .At Site 4 (Areas 4A and 4D), Site 8, Site 10, and Site 12, shovels were used to scrape stainsfrom the ground . The soil from each site was placed in a separate supersack . After thesupersacks were weighed, the soil was shipped to Rabanco Recycling as a Non-RCRA WasteSolid under Manifests GAM01, GAM09, GAM 10, and GAM11 .4 .9 Contaminated Soil RemovalReference Drawing No . HTW-3 provided in the scope of work for Task Order 0004 was usedto locate the contaminated soil at Site 4/Area 4B on Sevuokuk Mountain . Following thedimensions provided in this drawing, spray paint was used to mark this oval shaped area whichhad a maximum length of 36 .6 ft . and a maximum width of 29 .0 ft .The surface soil at Site 4/Area 4B had a uniform brownish color . There were no significantstains indicating a spill occurred at this location . After excavation began, a strong odor camefrom the soil . Between the boulders in the excavated area, the soil was black and had an oilyfilm .Based on field measurements, 103,885 pounds of contaminated soil was removed from thedesignated area at Site 4/Area 4B . The excavation depth after removing this soil, ranged from22 to 24 inches below grade .Large boulders in this site made it impossible to use heavy equipment for soil excavation . Asshown in Photos 19 through 24, HAZMAT certified workers used shovels to place the soil in50-pound sand bags . Following this , the sand bags were placed in track-mounted Argos andhauled down the mountain to the access road on the east side of Troutman Lake . Here, theywere transferred to a pickup truck and taken to a lay down area where they were placed insupersacks and weighed . When the weight was recorded , the supersacks were placed inconnex containers .Chemical Waste Management of the Northwest (CWMN) in Arlington, Oregon, agreed toaccept the Site 4/Area 4B soil for landfill disposal . After reviewing laboratory data provided byOSCI, CWMN designated the soil as "Hazardous Waste, Solid, N .O .S . (D008), 9, NA3077,PGIII ."Manifests GAM03, GAM04, GAM05, GAM06, GAM07 and GAM08 were used to ship the soilto CWMN . Block 11 .j. on the manifests identified dioxin as one of the contaminants in the soil .(Manifest copies are provided in Appendix C .)Contaminated soil was also removed from Site 12 . Several deteriorated lead-acid batterieswere located at this site . As shown in Table 6, laboratory analysis revealed that the TCLP leadin the soil under the batteries was 1,450 mg/L . Since this exceeded the 5 .0 mg /L regulatory21limit for TCLP lead established by 40 CFR261 .24, shovels were used to remove 601 poundsof soil from the areas that previously contained batteries . The soil was place in a 55-gallonmetal drum and shipped to Burlington Environmental Services in Seattle , Washington as LineItem 11 .a . on Manifest No. GAM02 .4 .10 Weights and MeasurementsAn electronic scale certified by the Alaska Department of Transportation and Public Facilitieswas used to weigh metal debris, HTW and soil removed from the project site (Photo 34) . Aseach item was weighed, the scale reading was recorded on a separate weigh ticket (Photo 35) .Copies of the weight tickets are provided in Appendix B . Each ticket has a unique identificationnumber and shows the source and description of the item weighed . The tickets also providethe gross weight, tare weight and net weight for the items weighed . Along with this, the weighticket identifies the connex that was used to ship the waste .Throughout this project, weights and measurements were repeatedly checked by OSCI'sQuality Control System Manager and the government's QAR .4.11 Waste Shipment and DisposalManifests were used to document and track waste movement from Gambell, Alaska, todesignated disposal facilities in the Lower-48 states . Table 3 summarizes the manifests usedfor this project . A copy of each manifest is provided in Appendix C .4.12 Site RestorationRepeated trips to remove contaminated soil from Sevuokuk Mountain destroyed the grass andcreated ruts in the tundra at the base of the mountain (Site 10 ) . Argos with flat tracks wereused to smooth out the ruts . After completing this, local workers placed 210 pounds of grassseed (50 percent Tufted Hairgrass , 40 percent Arctared Fescue, and 10 percent Annual Rye)and 3 , 850 pounds of fertilizer (20-20-10) to restore the damaged area . ( Prior to placement, theseed mix and fertilizer were approved by USAEDA .)Based on a request from local residents and approval from Sivuqaq Incorporated, OSCI didnot install silt fences as part of its tundra restoration program . Local residents on OSCI's workcrew said that silt fence should not be placed because it would create safety hazards forpersonnel traveling through the area on 4-wheel ATVs and snowmobiles . They believe highwinds would blow the silt fence over the tundra . Following this, the filter fence fabric wouldcause accidents if it was tangled in the moving parts on their snowmobiles and ATVs .4 .13 Daily Quality Control ReportsDaily quality control reports (DQCRs) are summarized in Table 4 . A copy of these reports isprovided in Appendix D .4 .14 Safety and Health SummaryA total of 5,629 man-hours were required to complete this project . There were no accidents,spills, or equipment failures . A copy of the Safety and Health Phase-Out Report for this projectis provided in Appendix H .22Table 3Manifest Tracking LogDebris Removal and Containerized Hazardous and Toxic Waste RemovalGambell, Alaska.0004,Contract No DACA85-97-D-0010Delivery Order NoManifestNumberWaste DescriptionWeightPoundsConnexNumberShippingDateDisposalFacilityReceiptDateGAM01Non-RCRA Waste Solid (POL Soil)Non-RCRA Waste Solid (Drums)1,8778,0892993278-26-99Rabanco RecyclingSeattle, Washington11-11-99GAM02Hazardous Waste, Solid (Soil w/Lead)Waste Tars, LiquidHazardous Waste, Solid (Paint)Environmentally Hazardous Substances, Solid(Batteries)6014,4583786192992648-26-99Burlington EnvironmentalSeattle, Washington11-10-99GAM03Hazardous Waste, Solid, D008 (leadcontaminated soil) (Soil also contains Dioxin)18,9962056768-26-99Chemical Waste ManageArlington, Oregon11-10-99GAM04Hazardous Waste, Solid, D008 (leadcontaminated soil) (Soil also contains Dioxin)18,3242055638-26-99Chemical Waste ManageArlington, Oregon11-10-99GAM05Hazardous Waste, Solid, D008 (leadcontaminated soil) (Soil also contains Dioxin)17,7492591768-26-99Chemical Waste ManageArlington, Oregon11-15-99GAM06Hazardous Waste, Solid, D008 (leadcontaminated soil) (Soil also contains Dioxin)15,5052592328-26-99Chemical Waste ManageArlington, Oregon11-09-99GAM07Hazardous Waste, Solid, D008 (leadcontaminated soil) (Soil also contains Dioxin)16,8302992728-26-99Chemical Waste ManageArlington, Oregon11-10-99GAM08Hazardous Waste, Solid, D008 (leadcontaminated soil) (Soil also contains Dioxin)17,2632053268-26-99Chemical Waste ManageArlington, Oregon11-09-99GAM09Non-RCRA Waste Solid (POL Soil)15,7962015708-26-99Rabanco RecyclingSeattle, Washington11-17-99Table 3 (Continued)Manifest Tracking LogDebris Removal and Containerized Hazardous and Toxic Waste RemovalGambell, Alaska.0004,Contract No DACA85-97-D-0010Delivery Order NoManifestNumberWaste DescriptionWeightPoundsConnexNumberShippingDateDisposalFacilityReceiptDateGAM10Non-RCRA Waste Solid (POL Soil)7,4602992358-26-99Rabanco RecyclingSeattle, Washington11-11-99GAM1 1Non-RCRA Waste Solid (POL Soil)14,7412057848-26-99Rabanco RecyclingSeattle, Washington11-11-99GAM12Non-RCRA Waste Solid (Drums)9,8652012168-26-99Rabanco RecyclingSeattle, Washington11-16-99GAM13Non-RCRA Waste Solid (Drums)9,0472057558-26-99Rabanco RecyclingSeattle, Washington11-11-99GAM14Non-RCRA Waste Solid (Drums)12,0482012918-26-99Rabanco RecyclingSeattle, Washington11-14-99GAM15Non-RCRA Waste Solid (Drums)9,5441006858-26-99Rabanco RecyclingSeattle, Washington11-11-99GAM16Non-RCRA Waste Solid (Drums)12,8000247548-26-99Rabanco RecyclingSeattle, Washington11-15-99GAM17Material Not Regulated byDOT (Scrap Metal)15,8802016228-26-99Rabanco RecyclingSeattle, Washington11-16-99GAM18Material Not Regulated byDOT (Scrap Metal)6,4982991538-26-99Rabanco RecyclingSeattle, Washington11-16-99GAM19Material Not Regulated byDOT (Scrap Metal)9,5312052558-26-99Rabanco RecyclingSeattle, Washington11-12-99Table 3 (Continued)Manifest Tracking LogDebris Removal and Containerized Hazardous and Toxic Waste RemovalGambell, AlaskaDelivery Order No . 0004, Contract No DACA85-97-D-0010ManifestNumberWaste DescriptionWeightPoundsConnexNumberShippingDateDisposalFacilityReceiptDateGAM20Material Not Regulated byDOT (Scrap Metal)12,4601007168-26-99Rabanco RecyclingSeattle, Washington11-12-99GAM21Material Not Regulated byDOT (Scrap Metal)8,7782610688-26-99Rabanco RecyclingSeattle, Washington11-12-99GAM22Material Not Regulated byDOT (Scrap Metal)7,7252012788-26-99Rabanco RecyclingSeattle, Washington11-16-99GAM23Material Not Regulated byDOT (Scrap Metal)11,7692014488-26-99Rabanco RecyclingSeattle, Washington11-17-99GAM24Material Not Regulated byDOT (Scrap Metal)12,9802011538-26-99Rabanco RecyclingSeattle, Washington11-12-99GAM25Material Not Regulated byDOT (Scrap Metal)6,2532990748-26-99Rabanco RecyclingSeattle, Washington11-09-99GAM26Material Not Regulated byDOT (Scrap Metal)12,4652011248-26-99Rabanco RecyclingSeattle, Washington11-17-99GAM27Material Not Regulated byDOT (Scrap Metal)12,1692590428-26-99Rabanco RecyclingSeattle, Washington11-12-99GAM28Material Not Regulated byDOT (Scrap Metal)13,0162002568-26-99Rabanco RecyclingSeattle, Washington11-11-99Table 4Summary of Contractor Quality Control ReportsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order No . 0004, Contract No . DACA85-97-D-0010Re ortDateTemp°FWindKnots17-6-9940 to 5015Offloaded equipment from barge and located Sites 2,3,8,10, 12, and 13 .27-7-9940 to 5015Set up field offices and continued reconnaissance for project sites .37-8-9940 to 5010Loose gravel on north beach and in village make these locations unsuitable forproject operating areas .47-9-9938 to 535Worked with local personnel to identify rental equipment for project support .57-10-9939 to 5515Located excavation area in Site 4 . Located debris in Sites 4 and 10 . Discoveredthat trails to these sites did not exist . Site 4 contains large boulders which preventvehicle access . Site 10 contains wet tundra which limits access to track-mountedvehicles .67-11-9940 to 51CalmContinued local investigation of local rental equipment .77-12-9940 to 50CalmDecided to set up work site at south beach due to stable gravel at this location .Requested Federal Aviation Administration (FAA) in Nome to provide locates forburied electrical cables supporting runway navigational aids .87-13-9939 to 48CalmLight rain and fog . Continued setting up work site on south beach . Front-endloader was stuck in loose gravel . Rented 966 dozer to free front-end loader .97-14-9943 to 483Light rain and fog . Hired three local workers . Unpacked and inspected tools .107-15-9946 to 48CalmRain . QAR and Project Manager arrived and inspected difficult travel conditions inSites 4 and Site 10 .117-16-9943 to 4815Collected and stockpiled metal debris at Site 8 . Contractor sent letter to FROidentifying differing conditions in Site 4 and Site 10 . Mechanic from Anchoragemade Nodwell repairs .127-17-9943 to 4833Nodwell placed in service . Live FAA power cable discovered in Site 8 near airportrunway . Work was terminated for 1,820 linear feet metal runway matting to avoidcontact with live cable .Significant Events and RemarksTable 4 (Continued)Summary of Contractor Quality Control ReportsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order No . 0004, Contract No . DACA85-97-D-0010Re ortDateTemp°FWindKnots137-18-9943 to 4728Continued to stockpile metal debris in Site 8 . Set up scale for weighing debris .147-19-9943 to 4728Continued stockpiling and weighing metal debris in Site 8 . QAR suspended heavydebris removal, cutting and equipment operation near buried cable in Site 8 . FROapproved use of non-HAZMAT trained local workers for metal debris handling . Foursamples were collected for waste characterization .157-20-9947 to 5221Sunny . Removed HTW and stained soil from Site 12 . Collected sample for wastecharacterization .167-21-9943 to 4910Completed removal for Site 12 . Continued debris removal and weighing in Site 8 .177-22-9939 to 4725Light rain . Removed HTW and stained soil from Site 8 . Completed debris removalfrom Site 13 . Shipped two additional Argos to project site . QAR defined steepmountain slopes as "Off-Limit" for project activities .187-23-9945 to 4736Blowing rain . Removed drums from Site 6 . Completed debris from Sites 2 and 3 .Since metal debris was left in place in Site 8 to avoid contact with buried powercables, contractor was authorized to remove metal debris from the archeologicalarea located near the northern end of Site 8 .197-24-9942 to 4721Light rain . Started stained soil removal in Site 2 . QAR suspended soil removal atthis site because previous environmental investigation said it was an oil spill site .(This information was not included in the scope of work for Delivery Order No .0004 .) Identified route through Site 10 to work sites on mountain .207-25-9945 to 473Weighed and loaded stockpiled debris . CQC issued deficiency tracking report dueto placement of drums with petroleum odor in connex container and failure toremove tops from empty drums .Significant Events and RemarksTable 4 (Continued)Summary of Contractor Quality Control ReportsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order No . 0004, Contract No . DACA85-97-D-0010Re ortDateTemp°FWindKnots217-26-9945 to 488Light rain and fog . Hired four additional local workers . Work continued foridentifying acceptable route to project sites on mountain top . 7-25-99 deficienciesfor connex containers were corrected .227-27-9945 to 488Light rain and fog . Established camp on mountain top . Since 4-wheel and 8-wheelATVS were causing damage to tundra, it was agreed to limit tundra traffic to trackmounted vehicles .237-28-9943 to 4720Light rain and fog . Removed debris from Site 5 . Stockpiled debris from Quonsethuts247-29-9944 to 4635Light rain and fog . Collected and stockpiled debris at Site 4, Areas 4A and 4B .257-30-9942 to 4617Light rain and fog . Hand digging started for removing 52 tons of contaminated soilfrom mountain top . Two additional Argos were mobilized to the job site .267-31-9944 to 4615Light rain and fog . Continued soil excavation at Site 4, Area 4B .278-01-9944 to 4715Light rain and fog . Continued soil excavation at Site 4 . Used 973 track loader tostage full connex containers for barge pickup .288-02-9944 to 4715Cloudy . Transported excavated soil to stagging area .298-03-9944 to 4725Rain . Weighed and loaded debris from Sites 4A and 4D . Terminated work onmountain due to poor weather conditions .308-04-9944 to 4735No work due to poor weather conditions .318-05-9946 to 4835Wind and rain . Transported, weighed and loaded HTW and contaminated soil .Located Navy cable .328-06-9946 to 4815Wind and rain . Continued removal, weighing and loading contaminated soil . QARruled that drums excavated by other contractors would not be included in scope ofwork for this delivery order . Archeological area debris in Site 8removed today .Significant Events and RemarksTable 4 (Continued)Summary of Contractor Quality Control ReportsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order No . 0004, Contract No . DACA85-97-D-0010Re ortDateTemp°FWindKnots338-07-9944 to 4615Cloudy . Continued removal, weighing and loading contaminated soil . Movedloaded connex containers to north beach . Sites 2, 3, 6, 7, 12 and 13 offered to QARfor final inspection .348-08-9946 to 4815Site 4 (mountain top) continues to experience heavy fog . Continued removal,weighing and loading contaminated soil . Collected 2 miles of Navy cable .358-09-9944 to 4431Heavy fog at mountain top . Continued removal, weighing and loading contaminatedsoil . Maintenance problems with Argos increasing .368-10-994416Light rain . Fog at mountain top . Hauled excavated soil down mountain to stagingarea for weighing . Moved loaded connex containers to north beach .378-11-9944 to 4615QAR inspected and approved Sites 2, 6, 7, 12, and 13 . Small debris needs to beremoved from Site 3 . Weighed contaminated soil .388-12-9941 to 4415Fog limited visibility and prevented plane with Resident Engineer from landing .Removed HTW and debris from archeological area in Site 8 . Completedcontaminated soil excavation . Picked up Navy cable .398-13-9944 to 4615Removed Navy shack . QAR issued final punch list for inspected sites .408-14-9944 to 4615Fog on mountain top . Confirmation samples collected . Site demobilization started .418-15-9944 to 4615Cleaned up staging areas .428-16-9944 to 4620Placed fertilizer and seed on tundra .438-17-9944 to 4610Completed fertilizing and seeding tundra . All site work completed . In response torequest from local workers and approval by local corporation, no silt fence wasinstalled .Significant Events and Remarks5 .0 SAMPLE COLLECTION AND LABORATORY RESULTS5 .1 Data Quality ObjectivesThe following data quality objectives (DQO) were established for this delivery order :•DQO -1 : Waste Characterization . Perform sufficient hazardous categorization to avoidconsolidating incompatible waste streams or mixing waste with different chemical orphysical characteristics .•DQO -2 : Obtain Data to Meet EPA Requirements for HTW Identification . Under Titles 40and 49 of the Code of Federal Regulations (CFR), a chemical description of thecontaminants must be provided before HTW can be : 1) transported over public highwaysor 2) accepted by an EPA-approved disposal facility . To satisfy this DQO, a separatecomposite sample will be collected from each site with stained soil and analyzed for TCLPmetals, semi-volatile organics, volatile organics, halogenated organics, petroleumhydrocarbons, pesticides, herbicides, PCBs, and reactivity . The analytical results will beused to prepare hazardous waste profiles which will be submitted to disposal facilities forwaste acceptance . The results will also be used to identify the proper EPA waste codesand shipping names from the Code of Federal Regulations .•DQO -3 : Identify PCB Level for Transformers . Under the Toxic Substance Control Act,PCBs at concentrations equal to or greater than 50 parts per million (ppm) are regulatedas PCB waste by the federal government . Under 18 AAC 75 .341, Method 2, the State ofAlaska regulates PCB contamination in soil when concentrations exceed 1 mg/kg insurface soil or 10 mg/kg in subsurface soil . For this DQO, discrete samples will becollected from liquids that are in the transformers . If the transformers are dry, wipe sampleswill be collected from the interior walls . The analytical results will be used to prepareprofiles which will be submitted to the disposal facilities for waste acceptance . They willalso be used to identify the proper EPA waste codes and shipping names from the Codeof Federal Regulations .DQO - 4 : Residual Contaminant Confirmation Sampling . To satisfy this DQO, samples willbe collected from contaminated soil and stained soil areas to identify residual contaminantlevels after the specified soil quantities are excavated .5 .2 Waste CharacterizationTo assure proper handling, each drum at the project site was inspected by experienced hazardouswaste technicians provided by OSCI and Philip Environmental Services (PES) . The objective wasto determine which drums : 1) required special handling to prevent spills during movement at theproject site and 2) could be consolidated for waste transportation and disposal .Approximately 460 drums were found . The drums at Sites 3 and 6 were empty and dry (containingno film or residue). Four drums at Site 4 were filled with gravel . Other drums at this location wereempty and dry . Nine drums at Site 8 were filled with solidified asphalt .30Site 10 contained wet tundra . Most of the drums at this location were punctured and standing in6 to 12 inches of clear water . An inspection revealed that the drums contained several inches oftundra water . This water quickly drained from the drums as they were removed from the tundra .At Site 12, five drums were filled with household trash . The other drums at this location wereempty .All empty drums were taken to a processing station and temporarily stored in a cell containing a20-millimeter (mm) high-density polyethylene (HDPE) liner . Following this, they were crushed,weighed, placed in connex containers (Photos 34 and 36) and shipped to Rabanco Recycling inSeattle, Washington, for disposal . (No liquid waste was generated by this process .)The drums containing asphalt were placed in overpack containers and shipped to BurlingtonEnvironmental as a hazardous waste . Trash from the Site 12 drums was placed in supersacks andshipped to Rabanco Recycling for disposal .5 .3 Samples for Waste Identification5 .3 .1 Soil SamplesSoil samples for waste identification were collected from the following locations :•Site 8 . Sample 99-GAM-001-SL was collected from a supersack filled with oil stained soilfrom Site 8 . As shown in Table 5, DRO and RRO levels for this soil were 2,380 and 13,500mg/kg, respectively . No PCBs were detected . Pesticides were 0 .0486 pg/L . As shown inTable 6, no TCLP metals were detected for this sample . (Sample locations are shown inFigures 3 through 8 .)•Site 12 . Samples 99-GAM -002-SL and 99-GAM-003-SL were collected from separate oilstained areas at Site 12 . Although both samples had relatively low DRO and RRO levels,Sample 99-GAM -003-SL contained TCLP lead at 1 ,450 mg / L (Table 6). In view of this, soilfrom stained areas that contained batteries was placed in separate supersacks and givena "D008" EPA waste code to identify the lead content .•Site 2 . Sample 99-GAM-004-SL was collected from an oil stained area at Site 2.Laboratory results (Table 5) revealed, that the GRO, DRO, RRO levels for this sample were309 mg/kg, 6,440 mg/kg and 388 mg/kg, respectively . No metals were detected in thissample .•Site 4 . Sample 99-GAM-005-SL (a composite sample) was collected from thecontaminated soil at Site 4/Area 4B . Based on analytical results, this area contained DROand RRO at 469 mg/kg and 2,110 mg/kg (Table 5), respectively . As shown in Table 7,dioxin levels for this sample ranged from 3 .1 to 1,880 parts per trillion (ppt) . The TCLP leadfor this sample was 11 .7 mg/L . Since this exceeds the 5 mg/L regulatory threshold for leadin 40 CFR 261 .30, the soil excavated from Site 4 was given a "D008" EPA waste code toidentify it as a lead contaminated waste .31Table 5Waste Identification Sample Results Summary for OrganicsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, Alaska(mg/kg)MaximumVOAEPA 8260m /LMaximumSVOAEPA 8270m /LMaximumPCBEPA 8082/LMaximumPesticideEPA 8081A/LMaximumHerbicideEPA 8150m /LGROAK101DROAK102RROAK103ite(mg/kg)(mg/kg)SampleIdentificationDateo.199-GAM-001-SL7/19/998U (1 .95)2 ,38013, 500U (0 .10 - 0 .50)U (0 .017)U (0 .179)0 .0486U (0 .010)299-GAM-002-SL7/19/99129 .55140230U (0 .10 - 0 .50)U (0 .018)U (0 .190)U (0 .0190 - 1 .90)U (0 .010)399-GAM-003-SL7/19/9912U (2 .75)47 .2136U (0 .10 - 0 .50)U (0 .015)U (0 .151)U (0 .151 - 1 .51)U ((0 .010)499-GAM-004-SL7/19/9923096 ,440388U (0 .10 - 0 .50)U (0 .014)U (0 .105)U (0 .0105 - 1 .05)U (0 .010)599-GAM-005-SL7/19/994/4B3 .734692 ,110U (0 .10 - 0 .50)U (0 .022)U (0 .279)U (0 .0279 - 2 .79)U (0 .010)699-GAM-006-W7/28/994NRNRNRNRNRU (1 .00)NRNR799-GAM-007-W7/28/994NRNRNRNRNRU (1 .00)NRNR899-GAM-008-W7/28/994NRNRNRNRNRU (1 .00)NRNRRegulatory Limit - 18 AAC 75 .341, Method 230025011,000Notes :3 . mg/kg means milligrams per kilogram .4 . mg/L means milligrams per liter .5 . pg/L means micrograms per liter .6 . "NR" means no analyses performed by the laboratory .7 . "U" means undetected . The number in parenthesis is thelaboratory detection limit .."W"means the sample was a wipe sample .8.Laboratorydata reports are provided in Appendix F .7.Numbersprintedin boldface exceed regulatory limits .89 . TCLP extraction by EPA 1311 was performed forVOA, SVOA, PCB, Pesticides and Herbicides .10 . See Table 5A in Appendix E for VOA analyte results .11 . See Table 5B in Appendix E for SVOA analyte results .12 . See Table 5C in Appendix E for PCB analyte results .13 . See Table 5D in Appendix E for pesticides analyte results .14 . See Table 5E in Appendix E for herbicides analyte results .15 . Sample 99 - GAM-005-SL is a composite sample . Othersamples are discrete samples .Table 6Waste Identification Sample Results for TCLP MetalsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, AlaskaBariumEPA 6010m /LCadmiumEPA 6010m /LChromiumEPA 6010m /LLeadEPA 6010m /LMercuryEPA 7470m /LSeleniumEPA 7740m /LSilverEPA 7760m /LNo .IdentificationDateSiteArsenicEPA 7060m /L199-GAM-001-SL7/19/998U (0 .00500)U (0 .100)U (0 .200)U (0 .100)U (1 .00)U (0 .00200)U (0 .00500)U (0 .100)299-GAM-002-SL7/19/99120 .1922 .12U (0 .200)0 .145U (1 .00)U (0 .00200)U (0 .00500)U (0 .100)399-GAM-003-SL7/19/99120 .5520 .279U (0 .200)U (0 .100)1,450U (0 .00200)U (0 .00500)U (0 .100)499-GAM-004-SL7/19/992U (0 .00500)U (0 .100)U (0 .200)U (0 .100)U (1 .00)U (0 .00200)U (0 .00500)U (0 .100)599-GAM-005-SL7/19/994/4BU (0 .00500)7 .550 .211U (0 .100)11 .7U (0 .00200)U (0 .00500)U (0 .100)5 .0100 .01 .05 .05 .00 .21 .05 .0SampleRegulatory Limit - 40 CFR 261 .30, Table 1Notes :1 . mg/L means milligrams per liter .2. "U" means undetected . The number in parenthesis is the laboratory detection limit .3. Laboratory data reports are provided in Appendix F .4. TCLP extraction by EPA 1311 was performed for TCLP metals .5 . Numbers printed in boldface exceed regulatory limits .Table 7Waste Identification Results for DioxinDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, AlaskaAnal tesSample 99-GAM-005-SLEPA 8290t2,3,7,8-TODD3 .11,2,3,7,8-PeCDD18 .01,2,3,4,7,8-HxCDD23 .71,2,3,6,7,8-HxCDD53 .71,2,3,7,8,9-HxCDD81 .01,2,3,4,6,7,8-HpCDD4901,2,3,4,6,7,8,9-OCDD12502,3,7,8-TCDF2721,2,3,7,8-PeCDF53 .22,3,4,7,8-PeCDF1431,2,3,4,7,8-HxCDF5391,2,3,6,7,8-HxCDF1522,3,4,6,7,8-HxCDF3671,2,3,7,8,9-HxCDF8 .31,2,3,4,6,7,8-HpCDF11201,2,3,4,7,8,9-HpCDF72 .71,2,3,4,6,7,8,9-OCDF614Total TODD146Total PeCDD374Total HxCDD700Total HpCDD1090Total TCDF1350Total PeCDF1800Total HxCDF1880Total HpCDF1560Notes :1 . ppt = parts per trillion .2 . Sample collected 6 inches below surface at Site 4/4B .3 . Laboratory data sheets are provided in Appendix D .4. Sample 99-GAM-005-SL is a composite sample .34Figure 3 : Site - Sample Collection Locations35Figure 4 : Site - Sample Collection Locations36Figure 5: Site - Sample Collection Locations37Notes :1 . See Figure 2 for Site 4/Area 4B location .2 . Excavation is 22 inches to 24 inches deep .3 . Excavation was not backfilled per governmentinstructions .4 . Sample 99-GAM-005- SL was a pre - excavationcomposite sample collected from soil 6 inchesbelow the surface of the excavation area .5 . Other samples are post excavation samplescollected 6 inches below excavation bottom .6 . See Photo 22 for picture of excavation area .7 . Excavation is surrounded by large boulders .Sample Point99-GAM-024-SLExcavationExcavation BoundarySample Point13' 99-GAM-025-SLVAXSample Points99 ..GAM-020-SL99-GAM-021-SL99-GAM-022-SLf18'29'Sample Point99-GAM-023-SL15'36 .6'Sevuokuk MountainDrawing Not to Scale(DCP 2-9-01)Figure 6 1 Site 4/Area 4B - Sample Collection LocationsTrail to Site 10Notes :1 . Samples were collected 6 inches belowthe surface after soil stains were removed .2 . See Photo 13 for picture of Site 4/Area 4A .Sevuokuk Mountain3. See Figure 2 for Site 4/Area 4A location .99-GAM-018-SL2 8'Quonset HutFootprint410'20'VDrawing Not to Scale(DCP 2-9-01)Figure 7Site 4/Area 4A - Sample Collection LocationsSevuokuk Mountain--------------Sample Point99-GAM-026-SL~If ,SchoolABoundary for FormerDrum Stockpile at Site 61 . Samples was collected 6 inches belowgravel surface after drums were removed .Wind Fence2 . See Figure 2 for Site 6 location .3 . See Photos 25 and 26 for pictures of Site 6 .HousesDrawing Not to Scale(DCP 2-9-01)Figure 8Site 6 - Sample Collection Location5.3 .2 Transformer Wipe SamplesThree empty transformers were found at Site 4/Area 4D . A separate wipe sample (99-GAM-006W, 99-GAM-007-W, and 99-GAM-008-W in Table 5) was collected from the internal walls of eachtransformer . No PCBs were detected .5.3 .3 Waste Shipping Names and Regulatory CodesTo ensure proper waste identification and coding under Titles 40 and 49 of the Code of FederalRegulations, laboratory results (Appendix F) for the soil and wipe samples were sent to PES forreview . PES worked with Burlington Environmental and Chemical Waste Management of theNorthwest to determine the shipping names for the project waste . PES also prepared themanifests and shipping labels for all regulated waste shipped from Gambell, Alaska, togovernment-approved disposal sites . Copies of the manifests and laboratory analyses areprovided in Appendices C and F, respectively .5.3 .4 Items Not Requiring SamplesLaboratory analyses were not required for the asphalt from Site 8, batteries from Site 12 anddried paint from Site 12 . Burlington Environmental agreed to accept these waste streams basedon verbal information provided by PES personnel at the project site .5.4 Confirmation SamplesAfter completing soil excavation, confirmation samples were collected at following locations :•Site 12 . Workers used shovels to excavate 7,237 pounds of stained soil from Site 12 .Afterward , Samples 99 -GAM-009-SL, 99-GAM -010-SL and 99-GAM -011-SL werecollected . Analytical results showed that the DRO levels for these samples ranged from20 .5 mg /kg to 463 mg/kg (Table 8). RRO levels ranged from 98 .3 mg /kg to 1 ,890 mg/kg(Table 8) .As shown in Table 9 , total lead and total cadmium for Sample 99-GAM -009-SL were 562mg/kg and 142 mg/kg , respectively . This exceeds the 400 mg/kg limit for total lead andthe 5 mg /kg limit for cadmium established by 18 AAC 75.341 , Method 2 .The arsenic level for Sample 99-GAM-009-SL was 3 .06 mg/kg . It was 3 .64 mg/kg and6.02 mg/kg for Samples 99-GAM-010-SL and 99-GAM-011-SL, respectively . Bycomparison, the regulatory limit for arsenic is 2 mg/kg under 18 AAC 75 .341, Method 2 .•Site 8 . Samples 99-GAM-012-SL and 99-GAM-013-SL were collected after removing4,790 pounds of stained soil from Site 8 . DRO levels for these samples ranged from nondetect to 30 .0 mg/kg (Table 8) . RRO levels ranged from 15 .6 mg/kg to 70 .9 mg/kg .Most of the metal debris, HTW and soil removed from Gambell, Alaska, was weighed atSite 8 . Sample 99-GAM-013-SL was collected to confirm residual contaminant levels inthe soil at the weighing station . GRO was not detected for this sample . DRO and RROwere 30 .0 mg/kg and 70 .9 mg/kg (Table 8), respectively . Under Method 2 for Alaska'sOil and Hazardous Substance Pollution Regulations, 250 mg/kg is the state's41Table 8Confirmation Sample Results Summary for OrganicsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, Alaskao.1234567891011121314151617181920SampleIdentification99-GAM-009-SL99-GAM-010-SL99-GAM-011-SL99-GAM-012-SL99-GAM-013-SL99-GAM-014-SL99-GAM-015-SL99-GAM-016-SL99-GAM-017-SL99-GAM-018-SL99-GAM-019-SL99-GAM-020-SL99-GAM-021-SL99-GAM-022-SL99-GAM-023-SL99-GAM-024-SL99-GAM-025-SL99-GAM-026-SL99-GAM-027-SL99-GAM-028-SLGROAK101DROAK102RROAK103ateite(mg/kg)(mg/kg)(mg/kg)8/14/998/14/998/14/998/14/998/14/998/14/998/14/998/14/998/14/998/14/998/14/998/14/998/14/99121288U (3 .43)U (2 .19)U (1 .86)U (1 .79)U (1 .90)U (2 .99)U (2 .95)U (1 .7)U (1 .88)U (2 .66)U (2 .85)46340720 .5U (9 .06)30 .084 .068 .87215 .31,31077813,9001 ,7208/14/998/14/998/14/998/14/998/14/998/14/998/14/99Regulatory Limit, 18 AAC 75 .341,Method 284A4A4A4A4A4A4B4B4B4B4B4B6MFBMTB34 .934 .7NRU (2 .68)U (2 .17)U (2 .05)U (1 .36)12 .6U (0 .0900)30013,700NR643U (10 .2)24 .8U (9.35)NRNR-F1,89098 .315 .670 .959230327047 .7930450905984NR187MaximumSVOAEPA 8270(mg/kg)MaximumPCBEPA 8082m /kMaximumPesticideEPA 8081Am /kU (0 .034 - 0 .34)U (0 .022 - 0 .22)U (0 .019 - 0 .19)U (0 .018 - 0 .18)U (0 .019 - 0 .19)U (0 .030 - 0 .30)U (0 .030 - 0 .30)U (0 .015 - 0.160)U (0 .019 - 0 .19)1 .20U (0 .029 - 0 .29)0 .3820 .371U (11 - 56)U (0 .35 - 1 .8)U (0 .35 - 1 .8)U (0 .32 - 1 .6)U (9 .1 - 46)U (9 .0 - 46)U (9 .0 - 46)U (0 .370 - 1 .700)U (0 .34 - 1 .7)25 .2U (8 .4 -43)U (9 .4 - 48)U (0 .0477)U (0 .0365)U (0 .00353)U (0 .00319)U (0 .00329)0 .03170 .0111U (0 .0022 - 0 .0089)U (0 .00325)U (0 .349)U (0.0314)U (0.0390)U (0 .0386)NRU (0 .00343)U (0 .00317)0 .09210 .04380 .000950 .0332U (0 .000329 - 0 .0329)U (0 .00507 - 0 .507)U (0 .00177 - 0 .0177)U (0 .00020 - 0 .0030)0 .000358U (0 .697 - 69 .7)U (0 .0110 - 1 .10)U (0 .0117 - 1 .17)U (0 .0116 - 1 .16)NRU (0.00171 - 0 .171)U (0 .000317 - 0 .317)U (0 .00341)U (0 .00326)NRNRU (0.000341 - 0 .0341)U (0 .000326 - 0 .0326)NRNRNR0.1640 .141U (0.020 - 0 .20)0 .101.0262- 0 .262)U (0U (0 .00100 - 0 .0100 mg/L)22 .050 .125 .6NRNR250 11,000Notes :1 . mg/kg means milligrams per kilogram .2 . mg/L means milligrams per liter .3 . "NR" means no analyses performed by the laboratory .4 . "U" means undetected . The number in parenthesis islaboratory detection limit ..Laboratorydata reports are provided in Appendix F .5MaximumVOAEPA 8260(mg/kg)U (3 .5 -18)NR0 .384U (0 .31 - 1 .6)U (0 .33 - 1 .7)U (0 .31 - 1 .6)NRNR1Numbers printed in boldface exceed regulatory limits .7 . See Table 6A in Appendix E for VOA analyte results .8 . See Table 6B in Appendix E for SVOA analyte results .9 . See Table 6C in Appendix E for PCB analyte results .10 . See Table 6D in Appendix E for pesticides analyte results .6.Table 9Confirmation Samples for 8-RCRA MetalsDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, AlaskaBariumEPA 6010(mg/kg)CadmiumEPA 6010(mg/kg)ChromiumEPA 6010m /kLeadEPA 6010m /kMercuryEPA 7470(mg/kg)SeleniumEPA 7740(mg/kg)SilverEPA 7760(mg/kg)No .SampleIdentificationDateSiteArsenicEPA 7060(mg/kg)199-GAM-009-SL8/14/99123.0616914216 .65620 .6220 .7020 .114299-GAM-010-SL8/14/99123.6419 .90 .1392 .5912 .4U (0.0143)U (0 .231)U (0 .0462)399-GAM-011-SL8/14/9986.0216 .80 .18220 .056 .0U (0.0146)0 .546U (0 .0444)499-GAM-012-SL8/14/9983.913 .59U (0 .0205)1 .393 .89U (0 .00867)U (0 .205)U (0 .0410)599-GAM-013-SL8/14/9983 .6012.70 .01963 .6214 .3U (0 .00676)U (0 .192)U (0 .0384)699-GAM-014-SL (1)8/14/994A1 .7557.30 .65913 .22120 .101U (0 .439)1 .62799-GAM-015-SL (1)8/14/994A1 .6066.71 .5723 .93110 .1150 .4020 .169899-GAM-016-SL (1)8/14/994A8 .357 .0U (0 .12)24 .71970 .121 .3U (0 .23)999-GAM-017-SL8/14/994A3 .1310 .00 .06995 .526 .43U (0 .00873)U (0 .200)U (0 .0400)1099 -GAM-018-SL8/14/994A3 .0118 .60 .29042244 .30 .04450 .4880 .4401199-GAM-019-SL8/14/994A4.2216 .81 .9131135 .10 .01730 .6680 .07671299-GAM-026-SL8/14/9965 .305 .95U (0 .0202)1 .333 .47U (0 .0109)U (0 .202)0 .041921,1005264001 .43 .521ADEC Regulatory Limit - 18 AAC 75 .341,Table B1, Method 2Notes : 1 . Samples 99-GAM-014-SL, 99-GAM-015-SL, and 99-GAM-016-SL are parts of a triplicate sample where 99-GAM-014 is the project sample,99-GAM-015-SL is the quality control sample, and 99-GAM-016-SL is the quality assurance sample .2 . mg/kg means milligrams per kilogram .3. "U" means undetected . The number in parenthesis is the laboratory detection limit .4 . Laboratory data reports are provided in Appendix F .5 . Numbers printed in boldface exceeds regulatory limits .limit for DRO . The regulated threshold for RRO is 11,000 mg/kg . In view of this, Sample99-GAM-013-SL confirms that no significant petroleum contamination resulted from debrisand waste handling at the project weighing station .For Samples 99-GAM-012-SL and 99-GAM-013-SL, arsenic was the only metal thatexceeded the ADEC cleanup action levels cited in 18 AAC75 .341, Method 2 . As shownin Table 9, the arsenic levels for these samples ranged from 3 .60 mg/kg to 3 .91 mg/kg .•Site 4/Area 4A . About 1,877 pounds of stained soil were removed from Site 4, Area 4A .When this was completed, Samples 99-GAM-014-SL, 99-GAM-015-SL, 99-GAM-016-SL,99-GAM-017-SL, 99-GAM-018-SL, and 99-GAM-019-SL were collected to confirmresidual contaminant levels .Samples 99-GAM-014-SL, 99-GAM-015-SL, and 99-GAM-016-SL are parts of a triplicatesample . Samples 99-GAM-016-SL was the quality assurance 1 sample . It was analyzedby Quanterra Environmental Services . The other samples were analyzed by C .T. & E .Environmental Services .GRO was not detected in any of the samples . DRO ranged from 15 .3 mg/kg to 1,310mg/kg (Table 8) . RRO levels ranged from 47 .7 mg/kg to 930 mg/kg (Table 8) .Total chromium for Samples 99-GAM-018-SL and 99-GAM-019-SL was 422 mg/kg and311 mg/kg, respectively . This exceeds ADEC's 26 mg/kg cleanup threshold for totalchromium . Samples 99-GAM-016-SL, 99-GAM-017-SL, 99-GAM-018-SL, and 99-GAM019-SL had arsenic levels above ADEC's 2 mg/kg limit .•Site 4/Area 4B . Nearly, 52 tons of contaminated soil was excavated at Site 4/Area 4B .Samples 99-GAM-020-SL, 99-GAM-021-SL, 99-GAM-022-SL, 99-GAM-023-SL, 99-GAM024-SL, and 99-GAM-025-SL were collected to identify residual contaminant levels in theexcavated area .Samples 99 -GAM-020-SL, 99-GAM-021-SL, and 99-GAM -022-SL are parts of a triplicatesample . Samples 99 -GAM-022-SL was the quality assurance sample . It was analyzedby Quanterra Environmental Services . The other samples were analyzed by C .T. & E .Environmental Services .GRO was not detected in any of the samples . DRO levels ranged from non-detectableto 13,900 mg/kg (Table 8) . Other analytes detected in the post excavation samples forSite 4/Area 4B were below regulatory thresholds established by the state and EPA .Residual dioxins at this site varied from non-detect to 1,250 ppt (Table 11) .•Site 6 . This site contained 7,897 pounds of empty drums and 1,748 pounds of metaldebris . After removing these items, Sample 99-GAM-026-SL was collected to determineif the soil was contaminated . Laboratory results revealed that GRO and DRO were notpresent . RRO was detected at 25 .6 mg/kg (Table 8) . Total arsenic was 5.3 mg/kg (Table9).44Table 10Metal Results for Site 4/Area 4B SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, AlaskaSiteAntimonyEPA 7041(mg/kg)ArsenicEPA 7060m /kCadmiumEPA 7131(mg/kg)CopperEPA 6010B(mg/kg)LeadEPA 7421(mg/kg)8/14/994/4BU (0 .216)0 .9780 .096563 .916 .199-GAM-021-SL (1)8/14/994/4BU (0 .206)0 .6420 .092733 .222 .2399-GAM-022-SL (1)8/14/994/4BU (0 .50)1 .1U (0 .13)65 .736 .5499-GAM-023-SL8/14/994/4B3 .341 .571 .806,940396599-GAM-024-SL8/14/994/4BU (0 .211)1 .090 .03757 .325 .64699-GAM-025-SL8/14/994/4BU (0 .204)0 .6040 .12949 .39 .0225No .SampleIdentificationDate199-GAM-020-SL (1)2ADEC Regulatory Limit, 18 AAC 75 .341,Table B1, Method 2Notes :1 . mg/kg means milligrams per kilogram .4002. "U" means undetected . The number in parenthesis is the laboratory detection limit .3. "SL" means the sample matrix was soil .4. Laboratory data reports are provided in Appendix F .45Table 11Confirmation Sample Results for Dioxin by EPA Method 8290Debris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, AlaskaSample No .99-GAM-020-SLtSample No .99-GAM-021-SLtSample No .99-GAM-022-SLtSample No.99-GAM-023-SLtSample No .99-GAM-024-SLtSample No .99-GAM-025-SLt2,3,7,8-TCDDU (0 .8)U (0 .6)0 .60 JU (1 .0)U (1 .0)U (0 .7)1,2,3,7,8-PeCDD2 .6 J2 .2 JU (2 .2)3 .3 JU (1 .4)U (0 .8)1,2,3,4,7,8-HxCDD3 .8 J3 .0 J3 .3 J2 .9 JU (1 .0)U (0 .6)1,2,3,6,7,8-HxCDD14 .18 .9125 .8U (0 .9)U (0 .6)1,2,3,7,8,9-HxCDD10 .98 .25 .1 J8 .7U (0 .9)U (0 .6)1,2,3,4,6,7,8-HpCDD266151250 B46 .39 .9 B1 .3 JB1,2,3,4,6,7,8,9-OCDD1,2508001100 B18052 .49 .7 JB2,3,7,8-TCDF3 .5 B4 .1 B1 .2 CON44 .24 .8 BU (0 .7)1,2,3,7,8-PeCDFU (0 .6)0 .97 J EMPCU (1 .6)6 .9 EMPCU (0 .9)U (0 .6)2,3,4,7,8-PeCDF1 .2 J1 .7 JU (1 .5)16 .62 .5 J EMPCU (0 .7)1,2,3,4,7,8-HxCDF4 .3 J4 .6 JU (2 .9)50 .38 .61 .2 J1,2,3,6,7,8-HxCDF1 .7 J1 .8 JU (2 .1)14 .02 .2 JU (0 .4)2,3,4,6,7,8-HxCDF2 .9 J2 .9 JU (1 .8)29 .16 .7U (0 .5)1,2,3,7,8,9-HxCDFU (0 .6)U (0 .5)U (0 .18)U (0 .8)U (0 .9)U (0 .5)1,2,3,4,6,7,8-HpCDF10774 .19683 .417 .62 .4 JB1,2,3,4,7,8,9-HpCDF6 .54 .8 J5 .0 J7 .92 .1 JU (0 .7)1,2,3,4,6,7,8,9-OCDF59643657058 .115 .41 .9 J EMPCTotal TCDD1 .71 .57 .617 .1U (1 .0)U (0 .7)Total PeCDD24 .319 .1U (4 .5)45 .1U (1 .4)U (0 .8)Total HxCDD97 .967 .16873 .26 .6U (0 .6)Total HpCDD46126343091 .221 .82 .3Total TCDF24 .926 .7472147 .5U (0 .7)Total PeCDF8 .612 .81116611 .1U (0 .6)Total HxCDF85 .559 .46115726 .02 .1Total HpCDF52636247014132 .94 .1AnalytesNotes :1.2.3.4."U" means not detected .Detection limit in parenthesis .J means estimated .B = Method blank contamination .5 . EMPC is estimated maximum .6 . ppt = parts per trillion .7 . CON is confirmation analysis .465 .5 Procedures for Sample CollectionWaste characterization samples were obtained from soil 6 inches below the surface in areascontaining stains . Confirmation samples were collected from soil 6 inches below the surfacein areas where excavation was performed to remove stains or contamination from a locationthat contained HTW.At each sample point, a clean metal spoon was used to dig a hole 8 inches deep . Followingthis, a plastic spoon was used to take soil from the sides of the hole (6 inches below thesurface ) and place it into sample jars provided by the project laboratory .At each sample point, soil for the GRO and volatile organic analyses (VOA) samples wasplaced in the same 4 ounce glass sample jar (with a septa lid) . After putting 25 mg of soil inthe jar, 25 ml of methanol were added . Next, the sample jar was capped and put in a Ziplocplastic bag which had the sample identification number and required analytical results writtenon it . (No labels were placed on the jar since its weight was pre-measured by the laboratory .)Based on instructions from the project laboratory (C.T . & E . Environmental Services ), soil forDRO, RRO, semi-volatile organic analysis (SVOA), metals , PCBs , herbicides and pesticideswere placed in the same 8-ounce glass sample jar . Each jar contained a typed label identifyingthe required analysis and analytical method . The date and time were written on the labelsimmediately after the sample was collected . Following this , the sample was logged on a chainof custody form and placed in an ice chest containing blue ice (Photos 53 and 54 ). A separate8-ounce glass jar was used for the dioxin sample .The following steps were used to collect triplicate samples :•GRO and VOA Samples . A plastic spoon was used to place 25 mg of soil (each) fromthe designated sample point in three 4-oz . sample bottles (with septa lids) . Immediatelyfollowing this, 25 ml of methanol was poured over the soil in each jar . Afterward, thejars were closed and put in separate Ziploc plastic bags which had the sampleidentification number and the required analytical results written on them .•DRO RRO SVOA PCB Metals Herbicides and Pesticides Samples . Plastic spoonswere used to partly fill a large Ziploc plastic bag with soil from the designated samplepoint . After the bag was sealed and shaken to mix the soil, new plastic spoons wereused to remove the soil from the bag and place it in three 8-ounce pre-labeled samplejars . No preservatives were added to the sample jars .•Dioxin Sample . Plastic spoons were used to partly fill a large Ziploc plastic bag with soilfrom the designated sample point . After the bag was sealed and shaken to mix the soil,new plastic spoons were used to remove the soil from the bag and place it in three 8ounce pre-labeled sample jars . No preservatives were added to the sample jars .All samples were logged on a chain of custody form and stored in coolers containing blue ice .Wooden stakes were placed in the ground to mark the sample point locations . Laboratory datareports for the soil samples are provided in Appendix F .475 .6 Personnel Collecting SamplesAll samples were collected , labeled, packaged and shipped to the project laboratory by Mr .Randy Easley. He holds a degree in Chemical Engineering and is recognized as a "QualifiedPerson" for sample collection by ADEC .Mr . David Rein was the Contractor Quality Control System Manager for this project . He waspresent during sample collection .5 .7 Sample ShipmentSealed coolers containing the project samples were air freighted from Gambell to Anchorage .In Anchorage , project and quality control samples were delivered to C.T .& E . by Mr. Easley .The quality assurance samples were delivered to Quanterra per instructions from the FairbanksResident Office . Both C .T. & E . and Quanterra used Triangle Laboratories , Inc . in Durham,North Carolina for dioxin analysis .5 .8 Chemical Data Quality ReviewUnder a separate contract issued by the USAEDA, analytical data for Samples 99-GAM-009SL through 99-GAM-028-SL was evaluated by Laboratory Data Consultants, Inc . (LDC) locatedin Carlsbad, California . A complete copy of LDC's evaluation is provided in Appendix I of thisreport .During this project, two triplicate samples were collected for quality control (QC) and qualityassurance (QA) . The components for these samples were :TriplicateSampleProject SampleQC SampleQA Sample199-GAM-014-SL99-GAM-015-SL99-GAM-016-SL299-GAM-020-SL99-GAM-021-SL99-GAM-022-SLThe quality assurance samples were analyzed by Quanterra Environmental Services andreferred to as Sample Delivery Group (SDG) 064096 in LDC's report . The other samples wereanalyzed by C .T. & E . Environmental and identified as SDG 994255 in LDC's report .LDC's chemical data evaluation is summarized as follows :•Sample Custody and Preservation . All samples were properly preserved and deliveredto the laboratories with chain-of-custody forms . The forms were signed and date .Sample temperatures ranged from 2 .2 to 5 .3 °C .•Holding Times . All samples were analyzed within the required holding times .•GC/MS Instrument Performance Checks . For EPA Method 8260B (VOA analysis),differences in the initial and continuing instrument calibrations exceeded QC limits for2-butanone and 2-chloroethylvinyl ether for both samples in the SDG 064096 and48chloroethane for Sample 99-GAM-028-SL in SDG 994255 . In view of this, the resultsfor these analytes for these samples are qualified as estimates .For EPA Method 8270 (SVOA analysis), differences in the initial and continuinginstrument calibration exceeded QC limits for N-nitrosodimethylamine for SDG 064096 .These samples are also qualified as estimates .•Method Blanks . Methylene chloride was detected in the method blanks associated withSamples 99 GAM-009 through 99-GAM-019-SL and Samples 99-GAM-026 through 99GAM-028-SL . Bomomethane was detected in the method blank associated withSample 99-GAM-028-SL .DRO was detected in the method blank associated with the samples in SDG 994255 .Cadmium and lead were detected in the preparation blanks for Samples 99 -GAM-009SL, 99-GAM-010-SL, 99-GAM-011-SL, 99-GAM-012-SL, and 99-GAM-013-SL . Bariumand Chromium was detected in the preparation blanks for Samples 99 -GAM-014-SL,99-GAM-015-SL, 99-GAM-017-SL, 99-GAM-018-SL, 99-GAM-019-SL, and 99-GAM026-SL .Dioxin (EPA Method 8290) compounds were found in the blanks for all samples in SDG064096 and 994255 .•Surrogate Recoveries . Bromofluorobenzene surrogate recoveries exceeded QC limitsfor Samples 99-GAM-009-SL, 99-GAM-014-SL, 99-GAM-015-SL and 99-GAM-016-SLunder EPA Method 8260B . Therefore, the VOA results for these samples are qualifiedas estimates .Under EPA Method 8082 (PCB), the decahlorobiphenyl surrogate recovery levelexceeded QC limits for Sample 99-GAM-009-SL . All PCB results for this sample arequalified as estimates .For GRO analysis by AK101, low 4-bromofluorobenzene surrogate recoveries werereported for Samples 99-GAM-009-SL, 99-GAM-011-SL, 99-GAM-014-SL, and 99GAM-015-SL, and 99-GAM-016-SL . As a result the GRO values reported for thesesamples are qualified as estimates .Samples 99-GAM-014-SL, 99-GAM-016-SL, 99-GAM-019-SL, and 99-GAM-026-SLexperienced high surrogate recovery levels under AK102 . As a result, the DRO valuesfor these samples were qualified as estimates . The DRO surrogates were diluted outfor Samples 99-GAM-009-SL, 99-GAM-010-SL, and 99-GAM-018-SL . No dataqualifications were made for high surrogate recoveries based on the diluted sampleresults .•Matrix Spikes and Matrix Spike Duplicates (MS/MSD) . MS/MSD were not run for EPAMethods 82608, 8270, 8081, 8082 and 8290 . MS/MSD were not performed for AK 101,AK102 and AK103 .49•Laboratory Control Samples and Laboratory Control Sample Duplicates (LCS/LCSD) .Both laboratories ran LCS/ LCSD to assess precision and accuracy . Under EPA Method8260B , high LCS and LCSD recoveries were obtained for methylene chloride forSample 99-GAM -028-SL . Therefore , detected methylene chloride results for thissample are deemed to be estimates.Under EPA Method 8270, LCS and LCSD recoveries were outside the QC limits for3,3'-dichlorobenzidine, butylbenzylphthalate, bis(2-ethylhexyl)phthalate, pyridine, anddi-n-octylphthalate for all samples in SDG 994255 . Consequently, reported results forthese compounds are qualified as estimates .The LCS and LCSD recoveries for EPA Method 8082 were outside the QC limits forendosulfan sulfate . Therefore, detectable results under this method are qualified asestimates .•Internal Standard Recoveries (ISR) . Samples 99-GAM-021-SL and 99-GAM-023-SLhad high ISR for 1,2,3,4,6,7,8-HpCDD under EPA Method 8290 . As a result, reportedvalues for 1,2,3,4,6,7,8-HpCDD and total HpCDD are qualified as estimates .•Triplicate Sample 1 . GRO, VOA, SVOA, pesticides , and herbicides were not detectedin the components for this triplicate sample (99-GAM-014-SL , 99-GAM-015-SL and 99GAM-016-SL) . PCBs were not detected in Sample 99 -GAM-014-SL . Samples 99GAM-015-SL and 99-GAM-016-SL contained PCBs at 0 .0317 mg/kg and 0 .0111 mg/kg,respectively . This low degree of variability for the PCB results was deemed to betechnically acceptable by LDC .Detected DRO levels for the components of this triplicate sample ranges from 68 .8mg/kg to 84 mg/kg . RRO levels ranged from 270 mg/kg to 592 mg/kg . Hence, thecomparability for DRO results and RRO results for the triplicate sample componentswere viewed as technically acceptable by LDC .Except for the following analytes, components for Triplicate Sample 1 had acceptablecomparability for total metal results :AnalyteSample99-GAM-014-SL(mg/kg)Sample99-GAM-015-SL(mg/kg)Sample99-GAM-016-SL(mg/kg)Arsenic1 .751 .608 .3Cadmium0.6591 .57U(1 .2)SeleniumU(0.127)0.402U(1 .2)Silver1 .620 .169U(2.3)Sample homogeneity or subsampling in the laboratories may account for the variabilityin the sample results for these analytes .50Triplicate Sample 2 . This triplicate sample was collected from Site4/Area 4B at theproject site and included Samples 99-GAM-020-SL, 99-GAM-021 -SL and 99-GAM-022SL . Under Modification 04P4 issued by USAEDA, the required analyses forconfirmation samples from this area were limited to dioxin, antimony, arsenic, cadmium,copper and lead .Antimony was not detected in the Triplicate Sample 2 . Comparability for the othermetals is as follows :AnalyteSample99-GAM-020-SL(mg/kg)Sample99-GAM-021-SL(mg/kg)Sample99-GAM-022-SL(mg/kg)Arsenic0.9870.6421 .1Cadmium0.09650 .0927U(0 .63)Copper63.933 .265.7Lead16.122.236.5Sample homogeneity or subsampling in the laboratories may account for the variabilityin the sample results for these analytes .LDC's chemical data evaluation revealed acceptable comparability for all but thefollowing dioxin analytes for Triplicate Sample 2 :AnalyteSample99-GAM-020-SLtSample99-GAM-021-SLtSample99-GAM-022-SLtTotal TCDD1 .71 .57 .6Total PeCDD24.319.1U(4.5)Again, sample homogeneity or subsampling in the laboratories may account for thevariability in the sample results for these analytes .Overall, LDC concluded that the chemical data for the confirmation samples are acceptablewith the limitations noted in its report .516.0 CONCLUSIONS AND RECOMMENDATIONS6 .1 Waste Shipped and ReceivedIn accordance with the scope of work for Delivery Order 0004 under Contract No . DACA85-97D-0010, OSCI removed the following debris, HTW and soil from Gambell :OriginalQuantityPoundsQuantityRemovedPoundsDebris127 , 255142,324Rabanco RecyclingSeattle , WashingtonHTW16, 14053 ,738Burlington EnvironmentalWasteCategoryDisposal Facilities/LocationsSeattle , WashingtonRabanco RecyclingSeattle, WashingtonStained Soil40,00039 ,889Rabanco RecyclingSeattle , WashingtonContaminatedSoil104,000103,885Chemical Waste Managementof the NorthwestArlington, OregonAll waste departed Alaska under manifests signed by the government . After the waste arrivedat the designated disposal facilities during November 1999, the manifests were signed by adisposal facility representative and copies were mailed to the government at : "US ArmyEngineering District AK CEPOA-CO-FR (Gambell), P .O . Box 35066, Ft . Wainwright, Alaska99703-0066 ."6 .2 Contaminant ReductionBy removing 103,885 pounds of soil from Site 4/Area 4B, petroleum contaminate levelschanged as follows :GROAK101(mg/kg)DROAK102(mg/kg)RROAK103(mg/kg)Pre-ExcavationComposite Sample3.734692,100Maximum Level for PostExcavation Discrete Sample34.913,900984Regulatory Limit18 AAC 75 .341, Method 230025011,000Sample/Regulatory Limit52Based on laboratory results , the residual DRO level in Site 4 /Area 4B is above the 250 mg/kgregulatory limit established by ADEC Method 2 . As shown in Table 10 , post excavation metalconcentrations at this location are below regulatory levels .Confirmation samples for this project reveal that following analytes at Site 12 exceededregulatory limits :Regulatory Limit18 AAC 75 .341 , Method 2(mg/kg)Maximum DetectedResidual Level(mg/kg)DRO250463Arsenic23 .64Cadmium5142Lead400562Analytes(Site 12At Site 4/Area 4A, the following analytes are above regulatory limits :Regulatory Limit18 AAC 75 .341, Method 2(mg/kg)Maximum DetectedResidual Levelm /kDRO2501,310Arsenic28.3Chromium26422Analytes(Site 4/ Area 4AArsenic at 5 .3 mg/kg was the only analyte at Site 6 that exceeded regulatory limits . Thearsenic level at Site 8 (6 .02 mg/kg) was also above the state's 2 mg/kg limit .Pre-excavation and post excavation dioxin levels for Site 4/Area 4B are listed in Table 12 . Thevalues in the "Maximum Detected Residual Level Column" are the maximum analyteconcentrations for the confirmation samples listed in Table 11 . By removing 52 tons of soilfrom Site 4/Area 4B, the average reduction for the dioxin analytes was 77 .7 percent .6 .3 Work LimitationsThe original scope of work for this delivery order required OSCI to remove 115,000 poundsmetal matting on the east and west sides of the paved airport runway at Gambell, Alaska .While performing this work, energized electrical cables connecting the runway lights to a powersource were discovered on the east side of the runway . To avoid safety problems, thegovernment terminated work in areas where the cables were observed .Although 108,090 pounds of metal debris were removed from this area, visual observationsuggests that an equal quantity of metal runway matting remain at the project site . To safelyremove this matting, the electrical cables must be de-energized and elevated .53Table 12Pre-Excavation and Post Dioxin Results by EPA Method 8290 for Site 4/Area 4BDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010Gambell, AlaskaPre-ExcavationLeveltMaximum DetectedResidual LeveltPercentReductiont2,3,7,8-TODD3 .1U (1 .0)1001,2,3,7,8-PeCDD18 .03 .381 .71,2,3,4,7,8-HxCDD23 .73 .883 .91,2,3,6,7,8-HxCDD53 .714 .173 .41,2,3,7,8,9-HxCDD81 .010 .986 .51,2,3,4,6,7,8-HpCDD49026645 .71,2,3,4,6,7,8,9-OCDD1250125002, 3, 7, 8-TCDF27244.283 .61,2,3,7,8-PeCDF53 .26 .9 EMPC87 .02, 3, 4, 7, 8-PeCDF14316 .688 .41,2,3,4,7,8-HxCDF53950 .390 .71,2,3,6,7,8-HxCDF15214 .090 .82,3,4,6,7,8-HxCDF36729 .192 .11,2,3,7,8,9-HxCDF8 .3U (0 .6)1001,2,3,4,6,7,8-HpCDF112010790 .51,2,3,4,7,8,9-HpCDF72 .76 .591 .01,2,3,4,6,7,8,9-OCDF6145962 .9Total TCDD14617 .188 .3Total PeCDD37445 .187 .3Total HxCDD70097 .986 .0Total HpCDD109046157 .7Total TCDF135021484 .2Total PeCDF180016690 .8Total HxCDF188015791 .7Total HpCDF156052666 .3Anal tesNotes :1.2.3.4.5."U" means not detected . The number in parenthesis is the laboratory limit .Detection limit in parenthesis.Pre-excavation dioxin levels are the results for Sample No . 99-GAM-005-SLppt means parts per trillion .Maximum residual level is the highest analyte level for the Site 4/Area 4Bconfirmation samples listed in Table 11 .6 . EMPC is estimated maximum .54Two Quonset huts were located on the top of Sevuokuk Mountain at Site 4/Area 4D . Prior toproject mobilization, winds scattered metal from these huts along the west side of themountain . Steep cliffs made it impossible for OSCI to access and remove metal debris fromthe side of the mountain at elevations exceeding 400 feet above sea level .6 .4 Lessons LearnedThe following lessons learned during this project may benefit others who are consideringremedial activities at Gambell, Alaska :•Lodging and Meals . The Sivuqaq Lodge is a former work camp that is operated as ahotel by the village corporation . It has an industrial kitchen and four restrooms and canprovide accommodations for 16 to 20 people . Meals served by the lodge are limited tofast food . The cooks do not prepare breakfast . Occasionally, they do not work on theweekend . Firms planning to use the lodge to house their work crews should : 1) hire afull-time cook and a full-time housekeeper, 2) plan meals in advance and 3) shipsufficient food to Gambell for the meals . Since the lodge uses most of its refrigeratorand freezer space to store fast food items, it would be advisable for firms using thelodge to provide their own refrigerators . It would also be a good idea to shiptelephones, a television, VCR and videos for crew entertainment .•Local Transportation . Gambell does not have public transportation . Persons travelingto this location should ask the lodge to have someone with an ATV meet them at theairport . Wet tundra is located on the south end of Troutman Lake . This area must becrossed to get to Sevuokuk Mountain . Four-wheel ATVs have trouble crossing thetundra . They get stuck in locations where the mud and water are more than 18 inchesdeep . Eight-wheel Argos with tracks are better suited for crossing the tundra . Tops arerecommended for the Argos to keep the passengers and cargo from being coated withmud. (The tundra contains many submerged boulders that can damage Argos andATVs. To avoid problems , low speeds should be used while crossing the tundra .)•Track-Mounted Vehicles . Track-mounted vehicles are needed for crossing and workingon wet tundra in the Gambell area . To minimize tundra damage, these vehicles shouldhave flat tracks that will not dig into the ground . Tracks that have a "U" shapedsprockets will uproot vegetation that holds the tundra soil together and create ruts thatwill cause rapid erosion . This will destroy the tundra by creating lakes in flat areas andcausing erosion in sloping areas .•Boulders and Reduced Visibility on Mountain Top. The top of Sevuokuk Mountain iscovered with large boulders that prevent access by trucks and heavy equipment . Asdemonstrated during this project , Argos can drive over the boulders . Low ceilingscause dense fog on the mountain . As a result, visibility can be limited to 50 feet or less .•Beach Conditions . Barges transporting cargo to Gambell land at the north beach . Thegravel at this location is loose and difficult to work on . The south beach has hardpacked gravel and is suitable for heavy equipment and trucks .•Security is Required . During the first week at Gambell, gas was removed from vehiclesstored at the work site overnight . This was stopped by using locking gas caps .55•Local Rental Equipment . The Gambell Public Works Department has heavy equipmentthat can be leased . For this project, it was necessary to hire a mechanic to installbackup alarms and correct other problems so this equipment would meet requirementsestablished by the USAEDA .•Limit Crew Working Hours . Workers mobilized to Gambell from Anchorage insisted onworking seven 12-hour days per week to maximize their earnings . Due to harshenvironmental conditions and strenuous labor requirements, this proved to be too muchover a 43-day period . Although there were no accidents or spills, work related stresscaused friction between crew members . A shorter work week consisting of six 10-hourdays will create less stress for personnel at the job site .•Native Burial Sites on Mountain . Many burial boxes with skeletal remains werediscovered near debris removal sites on Sevuokuk Mountain . High winds havedamaged the boxes and scattered some of the remains . In view of this, firmsperforming remedial actions at Gambell, Alaska, should include an Archeologist on theirfield crews and make arrangements with the Gambell Native Council for handlingskeletal remains and artifacts found at the work site .56LIST OF APPENDICESAppendix A : Photo Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1Appendix B : Scale Tickets Showing Debris , HTW and Soil Weights . . . . . . . . . . . . . . B-1Appendix C : Waste Manifests and Certificates of Disposal . . . . . . . . . . . . . . . . . . . . . . C-1Appendix D :Daily Quality Control Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . D-1Appendix E :Laboratory Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-1Appendix F :Chain of Custody and Laboratory Data Reports . . . . . . . . . . . . . . . . . . . . F-1Appendix G : Data Deliverables for Project Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . G-1Appendix H : Safety and Health Phase-Out Report . . . . . . . . . . . . . . . . . . . . . . . . . . . . H-1Appendix I :Chemical Data Quality Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . I-1Appendix APhoto SummaryDebris Removal and Containerized Hazardous and Toxic RemovalGambell , AlaskaContract No. DACA85 -97-D-0010, Delivery Order No . 0004July and August 1999Photo 1 : Gambell , Alaska (looking west) .Photo 2: Barge landing at North Beachwith contractor equipment .Photo 3 : Floor plan for Sivugag Lodge(used for contractor meals andlodging) .Photo 4 : Cooks and kitchen in SivugagLodge .Photo 5:Photo 6 :Dining area in Sivugag Lodge .Bedroom in Sivugag Lodge .Debris Removal and Containerized Hazardous and Toxic RemovalGambell, AlaskaContract No. DACA85-97-D-0010, Delivery Order No . 0004July and August 1999Photo 7 : Worker collecting soil sample atSite 2 .Photo 8 : Backhoe moving supersack filledwith stained soil at Site 2.Photo 9: Site 2 after stained soilexcavation .Photo 10 : Empty fuel tank at Site 3 .Photo 11 : Backhoe preparing to removeempty fuel tank at Site 3 .Photo 12 : Government Representativeand contractor inspecting Site 3after debris removal .Debris Removal and Containerized Hazardous and Toxic RemovalGambell, AlaskaContract No . DACA85-97-D-001 0, Delivery Order No . 0004July and August 1999Photo 13 : Metal debris from Quonset Hutsat Site 4A/Area 4A .Photo 14 : Empty transformer at Site4/Area 4A .Photo 15 :Workers loading bagscontaining small pieces ofmetal debris into Argo at Site4/Area 4A .Photo 16 :Argo hauling debris fromSite 4/Area 4A through Site10 to transfer station .Photo 17 :Worker transferring metaldebris from Argo to wagon fortransportation to weighingstation at Site 8 .Photo 18 :Backhoe removing supersackcontaining Site 4/Area 4Adebris from Argo to pickuptruck .Debris Removal and Containerized Hazardous and Toxic RemovalGambell, AlaskaContract No. DACA85-97-D-0010 , Delivery Order No . 0004July and August 1999Photo 19 :Worker preparing for debrisremoval at Site 4/Area 4B .Photo 20 : Shovels used to excavatecontaminated soil at Site 4/Area4B.Photo 21 : Sand bags filled withcontaminated soil at Site 4/Area4B.Photo 22 : Sand bags filled with soil placedin Argo for transportation downthe mountain .Photo 23 : Supersacks filled withcontaminated soil placed inconnex .Photo 24 : Site 4/Area 4B after 52 tons ofcontaminated soil excavated .Debris Removal and Containerized Hazardous and Toxic RemovalGambell, AlaskaContract No . DACA85-97-D-0010, Delivery Order No . 0004July and August 1999IIIPhoto 25 : Drums at Site 6 .Photo 26 : Site 6 after drum removal .Photo 27 : Metal runway matting at Site 8 .Photo 28 : Loader placing runway mattingon Nodwell .Photo 29 : Nodwell hauling runway matting .Photo 30 : Nodwell offloading runwaymatting .Debris Removal and Containerized Hazardous and Toxic RemovalGambell, AlaskaContract No. DACA85 -97-D-0010 , Delivery Order No . 0004July and August 1999Photo 31 : Metal debris stockpiled at Site 8 .Photo 32 : Energized power cable forrunway lights exposed at Site 8 .(Metal debris suspended nearpower cable .)Photo 33 : Workers dismantle metal sled atSite 8 .Photo 34 : Drums weighed with anelectronic scale at Site 8 .Photo 35 : Scale weights for each loadrecorded at Site 8 processingstation .Photo 36 : Workers load crushed drumsinto connex container at Site 8 .Debris Removal and Containerized Hazardous and Toxic RemovalGambell , AlaskaContract No . DACA85-97-D-0010 , Delivery Order No . 0004July and August 1999Photo 37 : Access road to Site 10 . (Eastsite of Troutman Lake .)Photo 39 : Nodwell tested on tundra atSite 10 .Photo 41 : Drums on tundra at Site 10 .Photo 38 : 4-Wheel AN stuck in wettundra at Site 10 .Photo 40 : Tundra after three passes withNodwell . (Tundra was seeded torestore vegetation.)Photo 42 : Site 10 after drums removed .Debris Removal and Containerized Hazardous and Toxic RemovalGambell, AlaskaContract No. DACA85-97-D-0010, Delivery Order No . 0004July and August 1999Photo 43 : Drums at Site 12 .Photo 44 : Deteriorated battery at Site 12 .Photo 45 : Dried paint and batteries at Site12.Photo 46 : Drums from Site 12 placed onpickup truck and hauled to Site8 processing station .Photo 47 : Workers in Level "C" PPEremove batteries and dried paintat Site 12 .Photo 48 : Site 12 after HTW removal .Debris Removal and Containerized Hazardous and Toxic RemovalGambell , AlaskaContract No . DACA85 -97-D-0010 , Delivery Order No . 0004July and August 1999Photo 49 : Argo used to transportpersonnel and samplingsupplies .Photo 50 : Sample collection tocharacterize soil in supersack atSite 8 .Photo 51 : Soil characterization sampling atSite 2 .Photo 52 : Post-excavation confirmationsampling at Site4/Area 4B .Photo 53 : Samples labeled and logged onchain of custody form .Photo 54 : Cooler with samples and chainof custody form in Ziploc bags .Debris Removal and Containerized Hazardous and Toxic RemovalGambell , AlaskaContract No. DACA85-97-D-0010, Delivery Order No . 0004July and August 1999Photo 55 : Top view of excavation at Site4/Area 4B . Soil was excavatedto 24" below grade .Photo 56 : Sample Point 99 -GAM-20-SL .(6" below excavation bottom .)Photo 57 : Yellow tape is Sample Point 99GAM-023-SL .Photo 58 : Sample Point 99-GAM -024-SL .Soil was excavated betweenrocks .Photo 59 : Sample Point 99-GAM-025-SL .(6" below excavation bottom .)Appendix BScale Tickets Showing Debris, HTW and Soil WeightsW'.- .cketDebris Removal and Contains . ,d HTW Removal, Gambell AlaskaTicket #b f fl/ ( QSiteGrossWeightDate 7 -1CollectedDateWeighed} (/)fjDescriptionDateLoaded7- ,r 10/7HTW41 1Count PIA: r f=-~~GyTare Weight -~ / Z Net Weight !7'507q5SSOtherInitialsCSM)ct LNetWeightTicket #~Tare toConnext)"6_ mm l,.DateCollectedGross toConnex7' Connex#Date 7~~Weighed7SiteDescriptionW~ ,OG VV1 A TGrossWeightTare WeightZ ~ ' Net Weight tNetWeight~~Tare to-- Connex144• DateCollectedTicket #lowSiteGrossWeight 7NetWeight2~fl7-1 -qql dGZ002-5,">/DateLoaded ~~SSOtherCount :qGross to ~~Connex -~ Connex#1-001'DateWeighedDateLoadedA'1 A7DescriptionG_Tare Weight2 - Net WeightTare to Gross toConnex Connex13Count:Vq 5Initialsc6 ~'GR"SSOtherHTWCSInitialsConnex#HTWCS_Weigl i _ .:ketDebris Removal and Containerized HTW Removal, Gambell AlaskaTicket #CollectedWeighedDescriptionG 'D1AI6 /214TG A KO L~Site~~19DateLoaded-z- /9--q7BDHTWCSCount: ~~OtherGrossWeight7ZNet//Weight 1(~Tare WeightTare6 ?'-_Z97-,Net Weight q32Gross toConnextoConnexDateTicket # ~'o0_Initials c CZConnex#DateCollected7`"f1 9Description°/1/AWeighed72-00DateLoaded/7 gHTWBDH'SiteGrossWeightCount:MIATare Weight 2-92- Net WeightNet LWeight7`6SSOtherCSInitialsTare to Gross toConnex ConnexConnex#ZOO -~"‚VTicket #Date _ ~G/ rMCPCollected(f31,EI~C1'Ticket #Vl11,5SiteDateCollectedDescriptionDateWeighed2a'I A l)LDate 7 ~~ ,c 9Loaded7-Z -`__Count: _}HTWCSSSOtherGrossWeight5f)Net1 C3~~Gl ____WeightTicket #-6AM i I ~;SiteTare WeightNet WeightTare toGross toConnex0Connex~~Tare toConnexGPO /17CollectedrDateSite1))l5DateLoaded`"9971- z.c9(i r (lIt"363 ~vl l19~Conned71DateDateCollected '~ WeighedCount:HTWCSSSOtherrTare WeightNetWeightGrossWeightl -3Description'rGrossWeightTicket #InitialsNet WeightInitialsGrossConnex_to''Connex# / /S___VDate -~We9 hedDescriptionTare WeightNetTare toWeightConnexNet WeightGross toConnexq6 "C,~(,)Initials/~O/l IConnex#757-11Weigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaTicket #(-AAA. I ~SiteGrossWeightDateCollected 7-Description .~!Tarec~-M) ISiteGrossWeightDate 7 ZWeighed .Date`~Loaded~r1313HTWCSOtherCount :WeightNet WeightGrossDate'~ pp~Collected ~` / ~ 1 1Descriptionq~,' 4' /toConnexInitial s'Connex#Date(~Weighed 2 ` 1j m A~l_. }l~Lhf/7l L rS~DateLoaded 7- Z' 1 ~qBD$Count: 1I /NetWeightTicket #Tare Weightk'y__Net WeightInitialsTare toConnexGross toConnex1~~DateDateWeighed4~~Collected ______ cfC onnex#Description9Count :L-A0N(j I ', p ITare WeightNet WeightNet ? Tare to Gross toWeightConnexConnex L--t~20 :31b144S_DateLoadedOtherGross~,''(~Weight 2- GCS/V//Zo / I~ovrSiteHTWOther'~I )9'7~~~~Tare toNetWeightConnexl(Ticket #~C onnex#InitialsHTWCSAWeigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaDate-~ --~2~ Collected l - l J tdTicket # (NetWeightDateLoadedDescriptionSiteGrossWeightDateWeighed~~TareWeightTare to770Count:-~<Neta0Weight1' bConnexTicket # 1C7 /~ ~ ~.DateCollectedInitialsGross toConnex 4nnex#DateLoadedDate__WeighedNetWeightTare Weight .Net WeightTare .toConnexGross toConnexDateTicket#GAM /1'Site .5~ NetWeight3 , . Collected)-0 /DateWeighedtionDescri p4Gross ~~Weight540Tare WeightTare to,Conne)t)-2,5-R7Count:_ . FS.5f5 OtherSite Description,GrossWeight'OtherConnex#-~DateLoaded -*A9Count :Net Weightb ross to\ J Connex,6q~a&ywInitialsHTWCSIWeigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaTicket #(A-14 I.9 rZV vNetWeight-/ Ticket #NetWeightDateLoadede7F /-2'b10 _Net WeightTare toConnexIGross toConnexDate ~~~CollectedCAM 12-6( 70Count:Weight 3/1100Site / tipGrossWeight5DescriptionSiteGrossWeightDateDateCollected 21 Weighed 72Dateg edWei h edDescription _/Net WeightltoGrossSSOtherCSInitials)MNAftllJoel~ZConne547DateLoaded 7Count:~~CSp O br7C.~i njiilis G-YJU-1 //ate-25)areConnextoConnex425ZDate '~DateCollected / ~l Wei gh ed ~`7-01~~ Ticket #Connex#26 1-,A ISiteGrossWeight/VJ061__Tare Weight7-ZE ~'7Descriptiono bTare WeightNetTareWeigh ttoConnex~fCount :Net WeightGross toConnex&Connex#DateLoaded7J 2~gtCSWeigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaTicket #(,AM 1 Z7GrossWeight _a(I_ Tare Weight IqNetWeigh tFCA/ \i 5Tare toConnextolDateCollected`Descrip tio nGrossWeightTare WeightNetWeightTare toConnex,VAn~I t,CollectedDate /- 5Loaded G--BDR `HM-'C o u nt:'SS CS-~-`~ Other3Net Weight~"l qq~Gross toConnexIn iti l's L"DateLoaded,~~~Coun t: /V/J~75DescriptionGrossWeightTare WeightNetWeightTare toConnex _\CHTWConnex#05"? ~11-1~Net Weight _DateLoaded ~~~~Gross toConnexCount :6i'J12-0DateWeighed~BDRSSInitiI Is,10Site~OtherGross to ~~Connex7- 2-~_Connex#Net WeightDatem i Z19DateWeighedDateWeighed ~~1SiteTicket #~_n(1~~,W I " t,D es cri p tionSiteTicket#DateCollected_____GJC onnex#BDRSSCSOther~initials,Weigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaDateCollectedTicket # (,, j r\- 0DateWeighed50DescriptionSiteGross~~Weight 16NetWeightCount : _ MTare WeightInitials2Gross toDateDateTare toConnex152 -?lConnex / 53CollectedWeighedPAiSiteGrossWeightJUw A cThtj614 NetTare to..~ ./Connex V2~Ticket#WeightGross toConnexConnex#Date7-- /-Y 7LoadedkSDescriptionsTare WeightNetWeightSStherCount:J ':q2„li L lDate'e-4e2 DateCollected____ WeighedConnex#q7-O? -lSC, . mE-fAt, ~lsSiteGrossWeightNetWeightDescriptio n .1'Z-10Tare Weight 3 1 '1 Net WeightTare toConnexGross toConnexInitials201~8' ~ J711Connex#HTWCSWeigh TicketDebris Removal and Containerized HTW Removal, Gambeii AlaskaDateCollectedTicket #Description-Site GrossWeightDatec~ 19\3 Ticket # (;P,InitialsGrossto--~Connex Connex# 2, ~~ jl/V5LAWeigh TicketDebris Removal and Containerized HTW Removal, Gambell Alaskacket #DateCollectedYI'q-() 1k rn Z~`DateWeighedDateLoadedHTWDescription c./ i 14 /A)C- . JSite-14&GrossWeightNetWeight;L,-7.=~"TareConnexc____~ATicket #DateCollected7dTare Weight-O C--Net Weightto Gross toConnex7-~~GrossWeightTare WeightNet WeightTicketSite#NetWeight67Tare Weight' L) 1Tare toConnexNet WeigInitials A Cto~vZS50~Connex# 2 3 Z 7- --DatLoade~-Count: Jht-6-2)Gross toConnex2q ~3z 7 I/DateLoaded_~61Ll la - ,Vi, .~-A~7C onnex#C BDR + HTWCount: 16' ' u (CSOtherDate C~ I -I _C'DateCollectedWeighedC6b(GrossWeight--GrossConnextoConnexDescriptionInitialsDateWeighed-~~DescriptionB'CS(6 A-, :Other'5-60,_15ISiteNetTareWeight~~~†Count :° lJ~.l Connex#DR Y HTWCS--SSOtherInitials /1/1.7CiK\N,, .,jh TicketDebris Removal and Containerized HTW Removal , Gambell AlaskaTicket #C')...SiteGrossWeightDateCollected~1 rv\qi)5qjNetWeight~~MTicket #SiteDescriptionDateWeighed-1- -Ciq,MI,f1l~&t~Tare WeightNet WeightTare toConnexGross toConnexDateCollected ~ .-~VDateLoaded-/Lt Connex#.0(52-5'-_-)v12DateLoadedCount :QI--~J_RHTWSS CSOthercrossWeight6NetWeight1JTare toConnexGross toConnex/~,--~Connex#20 5.-S~'CWDateCollectedDateWeighedql-aTicket #SiteGrossWeightTare WeightDescriptionC..~II! Vl ( ~~d Net WeightABq9 2-)m~~CInitials~DDateLoaded-fSHTWount : ~~ SS CSOther~Tare WeightNet WeightTare toConnexGross toConnexInitialsCiNetWeight(iInitial sDescription`-99BDR1/ HTWSS CSOtherS Count :CDateWeighed_~~ I Connex#10Z c7(4-Weigh TicketDebris Removal and Containerized HTVV Removal, Gambell AlaskaTicket # A JCollectedDateLoaded UWeighed5PAA 0 q CX6SiteDescriptionMle-( S Count: 0A-Gpl LBD HTWSS CSOtherGrossWeightTare WeightNetWeightTare toConnex~'Ticket #G L M1SiteGrossWeightI1 7Eq4 $- C"_DateWeighedreC- s)Tare toConnexGross toConnexSiteDescriptionGrossWeightTare WeightNetWeightTare toConnexg_lRCount :HTWSS'OtherInitials/(11t%/DateLoadedCount :Net WeightICS;yC14,52-550Connex#Date ~_ .Weighed †Coy72 .05155O/DateLoadedrNet WeightC /a'M 'L70Connex#rTare WeightDateCollectedInitials iGross toConnexDescriptionNet-C..(Weight lTicket #DateCollectedNet Weight _InitialsGross toConnex ! 7 g~ Connex# '~qBDRSSOtherCS,'rMSG0(Wt.TicketDebris Removal and Containerized HTW Removal , Gambell AlaskaTicket #21DateWeighedq 6(~ -,~''`)Description CC )Site 00GrossWeightDateCollectedl 6 INei ~~~~l~'~. JWeightTare WeightDate'Loaded q'-3 ,Count :-'5o/ ---NetWeight1O-Tare to Gross LO 'ConnexConnexf ~' Connex#GrossWeightTareNet eo IWeightNetWeightVWeight5140_ t~1/-HTWCSGDWSSOtherInitialsSDateWeighedIDateLoadedc~~rDescriptionSiteGrossWeightNet;_M5TaretoGrosstoSSOConnex#2p2,ConnexConnexDateCollectedTicket #[)&0d S Count:uInitialsLoaded - (?DescriptionWeightCSJ2~ `7Z-7Z-ASite q ' ,1BDRSSOtherDateDate' ~G1 DateCollected WeighedTicket #~ 34C~BDR_)HTWSSCSCount :OtherTare WeightNet Weight-22-)Tare toConnexGross toConnex120InitialsConnex#2 ZS5O , lWeigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaDateCollectedTicket #Site 6 )GrossWeight .~J~TareDescriptionCN /Tare toConnexTi ket #DateCollectedDescription--7DateLoaded~~:Count : ) …j A/`T .5 -z-Gross toConnexSSROtherM3C-'w J5 3263 /InitialsConnex#DateWeighedC0/~~".G5J/ ( ._Net WeightWeightNetWeightSitel _DateWeighed ___DateLoaded0/L.Count : 1 8BDRSSHTWOtherGrossWeightNetWeightTare WeightTareConnexTicket # -DateCollectedSiteDescription7Net Weightto Gross to-7 Connex/6/GGInitials~~I '7 73Connex#DateWeighedGrossWeightTare Weight J Net WeightNetWeightTare to Gross toConnex Connexf15C26-D Ili -32-62>DateLoadedCount : _8I + G '7BDRSSOtherInitialsConnex# 7.05415C_-34Weigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaNTicket #b(/11 2-7/SiteDateCollectedDescriptionDatet&Tq-'tf^1-~? 1.GrossWeightBDRSSOtherr~ Tare WeightNet ~(1c ;o 5Weight l"'T`~ -9-17D ateLoadedCount :/C,:~YyInitialsTare toConnex3263Gross toConnex3Connex# ! 9 ~~ ^7atliket # AM Z7SiteDateWeigheDescriptionCount :lGrossWeight_Tare WeightNetWeight~Tare toConnexInitials /f I.I2t~3~6w ._ Gross toConnexConnex#"DateCollectedTicket #SiteDescription__" _ _"DateWeighedGrossI-0'C ` CDate ILoadeR1566Weight-F?NetWeightDateCollected"'Count :04/ 65c7Tare Weight -37HNet WeightTare toConnexGross to.r Connex`Initials~.,~' 6Connex#QS3Z63Weigh TicketDebris Removal and Containerized HTW Removal, Gambell Alaska\ NlTicket #~~Site46GrossWeightf -7if~NetWeightTicket #'.Descriptioni &) /~:)o [Tare Weight-7Net WeightL1-`~Tare toConnex,'` i cDateCollectedDateLoadedDateWeighedDateCollecte d 'GrosstoConnexCount :BDRSSOtherV206 5630Initials ~_15(32-- Connex#DateDateWeighedLoaded_SiteGrossWeightNetWeight--Ticket #(4 (3o/ ) j --J/L 5 0(` ~,7 1 1/-? kMZ!KZ-TareConnexGrossWei g ht -/l~p(. 9to~DateCollectedDescriptionBDRCount :(a)/ L,Gross toConnex~(-'~'~ n~T-115Z'InitialsC onnex#DateoadedDateWeighed3OHTW_SS~S1OtherK 9MNet WeightTare WeightSiteNetWeightDescriptionCount? I~~, ILTare WeightNet WeightTare toConnexGross toConnexq -'q lV~BDR~S JSS'Other tInitials7OConnex#20 5qZG3AWeigh TicketDebris Removal and Containerized HTW Removal, Gambell Alaska'cket#~~~'/vIDateCollected°- lZ9DateWeighedDateLoaded)4 L$SiteDescription~BDRHTWCount .:-;/SSOther L'CGrossJWeight /Tare Weight Net~l~ /NetTareWeight_ l L--Ti'ket #toConnex(~J 1GrossWeight• t_ INetWeightDescriptionTare Weight~~~.InitialsrGross toConnex7~~Date/ "/ r l Z CollectedSiteWeight~~t-~DateWeigheY, ~,Connex#-C A)T- SO( (2~UDateWeighedDescriptionGrossWeightTare WeightNet WeightTare toConnexGross toConnexu-4~~JimS'SiteNetWeightBDRSSOtherNet WeightInitials/'[ 5 C,0% 7(d.7Ticket#-10-98DateLoadedCount :Tare to - s~ Gross toConnexConnexDateCollected~za ~5 6 30+~C onnex# =5 -10 .q~~dy~DateLoaded `Count :BDRSSOtherCInitials /14 .5.~~Connex#0,/Lo766~y°Weigh TicketDebris Removal and Containerized HTW Removal, Gambell Alaska~.Ticket #DateCollectedSiteDateWeighed'?DescriptionqI30 1DateLoaded-( o~LCount : _lSSR(J)OtherGross Weight/,530Net Weight ~ i 2Tare WeightNetWeightTareConnextoGross toConnex (S 363Initials A'S-Connex#~~4#2-Q567667/llTicket #6-6A )-/ 'l 2 7DateCollectedDescriptionSiteGrossiJ..Weight- .~ Tare WeightNet IWeight\ Ticket #(GrossWeightNet\aWeightQ-2DateLoadedSo t!-BDRSsOtherCount : '1Net Weight I V S IGross toTare toConnex6 A /)I Zn 5SiteDateWeighedConnexDateDateCollected1 /Weighed16-31KInitialsConnex#. / ,.1 l `C tl~ZcDate C--~Loaded~~"DescriptionCount :BDR~~(~ SSOtherTare WeightTaretoConnexiNet Weightf-`1 /qGross to~wOConnexHTWConnex#'CSInitials_gq~1 2O5ro766~ JaWeigh TicketDebris Removal and Containerized HTW Removal, Gambell AlaskaTicket#CollectedDateLoadedWeighed ~~Site I L' DescriptionGrossWeightTare WeightNet Weight ~5NetWeightTare toConnexGross to ~~~ConnexTicket #r A iOSiteGrossWeightBDRSSOtherCount :Date ~Collected. 0 -q~HTWCS40Initials <Connex#DateWeighedDateLoadedDescription _~A)1 1 Ii ?_Tare Weight/ Net WeighttoGrossCInitials t r2 q ~l / 3 `toConnexConnex#DD~sTicket #~~Date3z"1 CollectedJDateWeighed~'6 - R" DateLoadedHTWSiteDescriptionCount : AIMSSCsOtherGross~qWeight _q )6oNetWeightC; `6rOTare Weight 395 ZaNet WeightTare to Gross toConnexConnexInitials ANN;q 76 0Connex#ZO 1 6 zZCWeigh TicketDebris Removal and Containerized HTW Removal, Gambell Alaska3 2~Ticket #Date/ _Collected `6j 'tjDateWeighed-6 -q q DateLoaded''I--- 77hrNBLC)&KSDescription C..OTSiteCount:6MGrossWeight7000LlNet WeightGross toTare toConnexNetWeightTicket #Tare WeightGf*,41 3LConnexDateCollected-~GrossWeightDescription~/620Z--rG'1T'OO Connex# 2GrossConnex-1 0Tare tooG,(-UWeightConnexAny 317Initials ~~Count: ~~ ~A' SSR CSOtherNet WeightNetTicket # C7 q eclztlDate~'†'_%ateWeighed Loaded -___&C-01SiteC RDR~ HTWSS CSOtherBDR-~ HTWSS CSOtherInitials Sty~((2- '~ 00C onnex# (qL/-/ 75q (f-1 A,V/CAppendix CWaste Manifests and Certificates of Disposal99A607 08/23/991 . Generator's US EPA ID No .NON-HAZARDOUSWASTE MANIFESTManifestK .R . O .O . O .O .0 2 2 2 82 . Page I•("` f .60lof 13 . Generator' s Nome and Mailing Address:FPMDIST AK( -ER (GAME)US Ala4YPO B( 350664. Generator's Phone ( FT5.YAT1tSRT(fj'Transporter1AK 99703-0066 (9M)353-7063CompanyNameTransporter2A . Transporter' s Phone. A . D .9 .8 .1 .7 .7 .3 .0 .0 .5)Iorthl ar>Id Services7.6 . US EPA ID NumberCompanyName8 . US EPA ID Number(206)763-30010B . Transporter's Phone.A -D-0-6 .1-6-72S .12Resource Recovery9. Designated Facility Name and Site Address 10 . US EPA ID NumberRABAW0 BEL'YC2JM(253)383-3044C . Facility's Phone(206) 623-40004 TH & IBSSEATTLE, VA 98106.X .E .M .P .T ..11 . Waste Shipping Name and Description12 . Containers13 .TotalNo . TypeQuanta14 .UnitWt Volla.IN-ICU TASTE SOLID ( PBTIOLEDI CORAQIAT° SOIL)Gb.ENERA c.T0RIX -1C1A TASTE SOLID ( I3iPTT DIOIS).d.E . Handling Codes for Wastes Listed AboveD . Additional Descriptions for Materials Listed Abovea) 162939 -00 - - PETIOLSOI COITAII1ATED SOIL, 1ABAICO CEDTIIICATIOI 10 . 9!-1121 01101 ( 22) b) 162!40 - 00 - - 1CIA KI PTT 010IS , I.ABAICO CBITIIICATIOI I0 . 99-1120 -a) b)15 . Special Handling Instructions and Additional Information6UE ATOR ' S CBITIIICATIOII : I hereby declare that the contents o! this consigneent are fully and accurately describedabove by the proper shipping nue , and are classified , packaged , urked , and labelled /placarded, and are in all respectsilt proper condition for transport via air , road , rail and urine vessel according to applicable international andnational regulations .16 . GENERATOR 'S CERTIFICATION : I certify the materials described above on this manifest ore not subject to federal regulations for reporting proper disposal of Hazardous Waste .SignaturePrinted/Typed NameTANSP0RTERMonth Day Year17. Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed NameSignatureMonthDayYea,18 . Transporter 2 Acknowledgement of Receipt of MaterialsSignaturePrinted/Typed NameMonthDoyYear19 . Discrepancy Indication SpaceFAC120 . Facility Owner or Operator : Certification of receipt of waste materials covered by this manifest except as noted in Item 19 .Printed /TypedNameSignatureMonthDayORIGINAL - RETURN TO GENERATOR MYear11/1?/bbnLUs'D .rfo9 9A607 O ' : - 31 . Generator' s US EPA ID No .NC N .HAZARDOUST-WASTE MANIFEST3 . Generotor'Manifest.K .R .O .O .O .0 .0 .3 3 1IG it'.`R•d'•1Name and Mailing O .ddressOS ARP ( ENGtNk.EIUNG DIST AK C~a'CiA-fi>t1-‚r'Et ((A14 ~i .L)PO H)X 35C ~64 . GoneratoV Phone'Z. ^ NAi. NSRIe 11'5, Transpartei 1 Comi . . tYName---AK 99703-0066 (907) .!5* --/L)636 . US .EPA 1 . ! .umberNo rthl . u)d Services _W A .U .9-ff.3 .O A SS . U i eV.. ID .tiu'.sber7 . Tronsponci 2 CompoA‚ r lameJ .A .L)-O .6 . 1 _6_Re sour- :e Rc c_crv10 .9 . Designated Facilit ' N , me and 5i-e AddressUSe. Tronspon .rs Phonc.2 .8 .1 .2(253) 383-30 .44'A I' p .r .berRABANC ) RI ' . ti : LTNG4 TH & LAI '%ZSSE A'I'!'ly, w : -1 _981081 1 . Waste Shy aping t , -and Dts . _riplio '1o.NUN-MA 1 kST? MID {PSTROLSIJA CO)1T1U(INATSu 5J1L}NONACRA V%' SOLI D t g?1'Y U1:Glfs ;C.d.s iar Mate rials Lasted Abov.tD . Additional Doscrif'a) 1629 ;13-oO Y6TiiOl,cUt GJNTMI1NA'l O SUIL, dAbakCQ IV.IIF : .: .' . . ! . Y9 .1121illHOi ( ~ !) b j '6,-O (1 - fCBA .MP1" DRUM, PA61v)CO ',RTIF' L 19-1120 -nTaal p ._ . _ ..15 . Special H Indlinr‚raio and Adaitiond1 InlormolionOFNERAT0l'S CF ' .i).1"CATIUK : I lletelly declart: that .the coatents ,-f tt ., .'inslgnaent are fl.i ly and accur~ ; ,y describedstore by the gnper shipping ncee ,ii nd are clae'3U. ied, paciUged ,~ .arlri, ud label led / plal:arded, and art a all tebpectsin proper condi.t.ion,for Transport via air, road , rail and ' aariir; wedAccording to app icaple iuterr . . anal addna.tional regut , tir :'s .1 6 . GRNERAT )R 'S CL-k, . . .:ATION. Ice pity use rrsm edals described o bo. . an th,s one, .1TPremed/T)1 7 . Tr onsporte r 1 Ack ,oedN/AV16 . Tr. snsportc r 2 Ac, .rated /T1 ped~ ..-a . .v of R. ceipi of M aterials._---s . 'lea o federal reaulat o s !or rep Los (al `'.C%cJ.5 Spec'I I Hanat ; g lnstrucoons and Additional Informationdeclare that me contents of this c0a nmeni ar-. fully and accurately de‚ .eAbed above by16 . GENE iATOR'S t‚c,TWICAT)0N: I ttoreayproper shipping ii me and an. clautlled. Packed. marked . and labeled/plararded, and era in ail rospeas in proper condition for Iransporraccort ng to applirablo International and national government regulation.III arr a targ. . luantity generator . I cor ity that I have a program in place to reCu. a the - alumo and toxicity of waste generated to the legree I have detorminod to beecono nicatly r : -4= e and .hat 1 have selected the practicable method of treatment, .Jto : : go r r disposal currently available tome wttrdt ' nimizes the present and futurea gooo teeth effort to minimize my wait )eneration and sclCct the bestthreat o hum :,, . ;ualm and ;he environment, OR, if lama small quantity generator. ,w tste nanagr .nt method twt is avallA Dle to me and that t can afford .Pnnt' :d / TYp4 ‚t ' lame I''j ril:TPANSPA-4FMonth Day Year1-0 o- GolT1 i . Tran : porter 1 A . tinowledgement of Receipt of MaterialsPrint/ / yf . ::d Name 1 idTs1H. Tran- ,portt> - 2 +, cl, nowledgement cif Rec eipt of Materialsr'~Month DayYearI 1 0 I•i`i.14 \itYearrr .f Print Typ. :. .' 7ffrneMonth Day19. Disc epancy ,r 0 ration SpaceFAC2U . Facie ty Owr. er . .r Operator : Certific ation of receipt of hazarCOUS ma ~ tals_ : . _~ red by this manifest except as note sLEPA FonwPrini!d/Type[Namea .e.f Pr.v.oue . atecn. „. .e.a.„..>oo- .2la.r2TRANSP0' : ^,T 0',- ; NO . 2Item 19 .mournuay.ca+‚ FCR 24 HOURi RE'CJ 66 1itMl*V r iUtt, CALL (90 /) 211-90o'1 , ,()99A60708/17/99Form Approved. OMB no . 2050-0039 . Expires 9-30-99ase print or type (Form designed for use on elite (12-pitch) typewriter )Generators US EPA ID NoUNIFORM HAZARDOUS ('WASTE MANIFEST AKw 00003228ManIf Docum.nt No.2 Pa ge 1of 1IG 3Information in the shaded areasis not required by Federal law3 . Generator's Name and Mailing AddressA. State Manifest Document NumberUS ARMY ENGII G DIST AK C IEKA-OD-ER (G 1, )PO BOX 350664 . Generator's Phone ET WATZISRIGHT AK 99703 -0066 (907)353-7063B . State Generator's 105 . Transporter 1 Company Name 6 US EPA ID NumberC . State Transporter's IDD . Transporter's Phone (206)763-3000Northland Services WAD9817730057 . Transporter 2 Company Name 8 . US EPA ID NumberE . State Transporter's IDF . Transporter's Phone 253383-3044WAD061672812Resource9 . Designated Facility Name and Site Address 10 . US EPA ID NumberChem Waste Mot of Northwest17629 Cedar Springs LaneArIi on , OR 97812G . State Facilitys IDH . Facititys Phone( 541) 454-2643ORD08945235312 Conta iners11 . US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number)N a.E13 .TotalQuantity14 .UnittNolNo .T17BA16436P1TB2560PHAt.IIDOQS IASTE , SOLID, I .O .S . (0001) 9 IA3077 PGIII BIG#(171)R1.Waste No .0001RT b.HAXAIDOQS VASYK , SOLID , LO .S . (D008) 9 113077 PGIII S1GI ( 171)0RQD001C,d.J . Additional Descriptions for Materials Listed AboveK . Handling Codes for Wastes Listed Abovea) 004133 -00 - - LEAD CORTUIIAT° SOIL - DI101 ( i) b) COU33 -00 - - LEADCMTAJIIAT° SOIL - DI101 (7)a) b)15 . Special Handling Instructions and Additional Information16 . GENERATOR 'S CERTIFICATION : I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeledtplacarded, and are in all respects in prope r condition for transportaccording to applicable international and national government regulations .If I am a large quantity generator , I certify that I have a program in place to reduce the volume and toxicity c1 waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and futurethreat to human health and the environment: OR, if I am a small quantity generator . I have made a good faith effort to minimize my waste generation and select the bestwaste management method that is available to me and that I can afford.Pnnted/Typed NameTSignatureMonth Day YearSignatureMonth Day YearSignatureMonth Day Year17 . Transporter 1 Acknowledgement of Receipt of MaterialsPrinted /Typed NameNSPR18 . Transporter 2 Acknowledgement of Receipt of MaterialsTPrinted/Typed NameER719 . Discrepancy Indication SpaceFtY20 . Facility Owner or Operator : Certification of receipt of hazardous materials covered by this manifest except as noted in item 19SignaturePrinted/Typed NameMonth DayEPA Fpm‚700-22 (Rev. 5-U ) Previous editions am ob .obtsORIGINAL-RETURN TO GENERATORYear1 ;:f : 13p Philip Services Corp-LL-11/18/ 99THi; 10 :23 FAX907 272 9005P .05?OR ‚24 HC14L2 F,~DStCC ,NC'Y. &a4-ZPONSC 1Wr'1LAtKXT1.ON, . . CALL ( 907) 2,?-.1-9001 '1 -1 991t607 08/24/99,t'lo,.tte dt,rt ,w tv .e . (Fore ' dnsyncd la NR * nn ad .,, (12‚t>‚rcht tvo .wrrt., I~/UNIFOAM HAZARDOUS I t3enerator$US EPA tD NotiF xrn Approved . OMB no. 20 003ti. Expires fiwLrawatf7ot:urnsnt 2?,UL Page'WAS TE MANIFESTa~iv~Xxm,~…g= r1~~~~rr.~r--}7jenara o r s N am . and Ma iS mg A ddres I JS A14MY P)iG? RE RING DIST AK CE )A-(.`O-Fr, (CftHI LL }ofr.mar ra1 tnrormaloom in the shades 3 .is not required; by Fwrarai taw-PO 210X'355-06643enQra or's Phone f'3' rt+'PixNS 1%V 1130 Q~'Z-&7tKri 1`907 .3353-70ta35 . Transp. rter71 Company Name 6 US EPA 1C Numbert~7'.X13C . Stsba~~.~aretpcrlas'}tS;U~SIGiA' ; ;aumberE . St1*:Tiaws it. .a)b'$ r ; h l attd Serve c~us _transp -nor 2 Company NameRest urce ttc!covew1 f AM13 1 5'7 2j='~9 . Design dots Facility NamF and Site AddressF . t :r†spert ::'s l s ,o~e . . I10 . U3 S' A lQ \umaer G. St$w F..ae t'sto ..113 -3csaaChe Wasto tiglt+t; of Not t1i sc_sti 176< 9 C dar i;Fr. i nq5 1.flEtrZr 1 1 nyt.un09 9"8I .i 1 . US DC T Dascnption (Including Propty Shoving Name . Hazard Crass ink :J Ni.. n r/0 I r~FL 1t__12. Containers 13 . ts .1.Total. Unli West. rto‚No . T 7e 0uantit wWdlA'1teU06S MkSt3 , 50i.IC, 1 .3 .S . ID008}_9 7113077 PG!1I 1DGO1iM‚L1-a' tGt(( ~i16436T b . !AZA900IiS lpt~1?!, S4LI,1, 11 .0 .5 . 1D003' v 9/l307'; I{T (t ;! (I 110~~41(f711+~I 'Nah, ‚K Nanditng .Code ., 'tu‚Wasuas UstedAboveJ- Addhle nal Dies,: ;poems lot M aterials Uste 6 ADaveC i1L33-t.7 - - WO COfI!l1i176,l9}`‚SQAr ('CCDCr, . !'CD'.} - Dili01 {3b } ~l : A1b33-80_560.PCB . ssr' 1 t, leCDts,'JI DQsEXCD1a,'crczws , PeCNI, PeCDht ; .?C.DOt, .ratsI_- :DTt41'_(31}15 Spec at Handling lnstruc ,. ions and Additional Information10 . GENE FFATOti ' S C RCAr10N : I r.raey d.eI de that V* contents of this cons nntt :n ; err ;ally and aecuratey do scntxa attovm by? t -lam ',,all respects in propCr Cwndltlort br transpomprop . st‚iDtt n nema and ar m ciasshfed, paDnid, enarXted, and lab .lad/placard .aCCD1' tag to rppowbte intt ;tranonai and natiorul government ra)ulatiants . tf'tl tan a larva quantity gcneator. I corny Mai I have a p+o9ram in platy to radt 1 tna fa;r‚ns and touchy ct wta-e q .n. ratad 10 tr,* dograe I have daiatmined to tscon: lleally DracI cable and blot I haw r aledt tl ttte Dractieabla method o f lr.atr : ar* . ;te .qa . tx disposal curre ury a eIis i . la m. watch rnmimizas t e Dresent ann R,hu: OR, if t am a amalt quantity g .netatAr i l3tY mad. a good win elton to minimus my wash gen e ration and sated trio bethreat to nunwn haatth and the environmenttamed &1C management matnpd M al is awla bie to me and that I cam of orrl.Print id / Typed Name 1r`~of L41= C1 t,.S y e .- .rGm)oTsign.>LTran : porter i ACknowle‚~gament cf Re. :eipl of Materials,G-r~ l tX~JPr I id/Typed Nameig5 ' Sn"reMonth Day Yg ~r ae~ruMonth Day 1Trait porter 2 Acknowla .ige m e nt Of fiae:e . pt o f M ate rta~lsit j~tepancy lndicatton 5pacaFel1 20 . Faei qty Owner o r Cipera: oTi nn ed/Typed?""0SPA /,. ..,, .T.Oa(F- "111)in Iterr 19Cert tht :anon of receipt of nazar dJS maien ;llp r:1x od by Mot ma 'west except\ as..notec,o 9'9_n' /Month Dayf' . ..hr . .era.+ta .n atr.+w7Tf.4NSF :OI~i'ATIOP" NO . 2‚**FOR 24 HOUR EICY RESPONSE I)(NATION, CALL (907) 272- 9007 '')99A607 08/17/99Please print or type (Form designed for use on elite (12-pitch) typewriter )UNIFORM HAZARDOUSWASTE MANIFEST4Form Approved . OMB no . 2050 -0039 . Expires 9-30-99I Generator's US EPA ID8NoManlf.u Doa,m . rtt No .3 . Generator's Name and Mailing AddressB . State Generators ID4 . Generator'sPhone5 . Transporter 1 Company Name 6 US EPA ID NumberServices7 . Transporter 2 Company NameResource Recovery9 . Designated Facility Name and Site AddressC . State Transporters IDD . TransportersPhon. (206)763-300078 . US EPA ID NumberE. State Transporbrs ID1 WAD061672812F . Transporters Phons 253383-410 . US EPA ID NumberG. State Facility's IDChem Waste Hg at of Northwest17629 Cedar Springs LaneArlingtonRH . Facilitys Phone978125511 . US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number)ArlHASA1D0US /ASYH , SOLID, 1 .0 .5 . (DOOS ) ! 1A3077 PCIII 1ZC$ ( 171)N a.ERQRATInformation i n the shaded areasis not required by Federal law .A . State Manifest Document NumberUS ARMY ENGINEERING DIST AK CEPOA-a>-FR. (CAM,)PO BOX 35066Northland2 Page 1of 1G!!04541 454-264312 . Containers13 .TotalNo . TQuantity14iUnitWtNolI.Waste No.D00120BA18342Pb.0RC,d.J . Additional Descriptions for Materials Listed AboveK Handling Codes for Wastes Listed Abovea) 001133 -00 - - LEAD COffUMUTIM SOIL - DI101 (1)a)15 . Special Handling Instructions and Additional Information16 . GENERATOR 'S CERTIFICATION : I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified , packed, marked , and labeled /placarded, aald are in all respects in proper condition for transportaccording to applicable international and national government regulations .If I am a large quantity generator , I certify that I have a program in place to reduce the volume and toxicity c' waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method of treatment ., storage , or disposal currently available to me which minimizes the present and futurethreat to human health and the environment ; OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and select the bestwaste management method that is available to me and that I can afford .YFTRAPrinted /Typed NameSignatureMonth Day YearSignatureMonth Day YearSignatureMonth Day Year17 . Transporter 1 Acknowledgement of Receipt of MaterialsPrinted /Typed NameNSPORT18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameER19 . Discrepancy Indication SpaceT20 . Facility Owner or Operator : Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19Printed/Typed NameSignatureMonth Day YearLYTEPA Form 1 700-22 M*v . %-U) Previoua . dmoni w, oe,o,,t.ORIGINAL-RETURN TO GENERATOR11f1!/DD1!LLvi' .`silam._*RE 2 4 -0MtR MgMGE3XT I2I5 T]!TI O* 4ATi :w : t,; :i1 .L (9O7 )'- 272-9OQT was()J9PFit` .7~'Plua .C print or type ~for' rid for use on elite ( 1 2-pnrh) typewriter .)'IDEPA o1 Generato r s us NHAZARDOUSA UNIFORIAWAST E MA NIFESTiLttro ~Ar '. oowm .rx tvo.t,1 niikWk~'4 77A.P- J7 708/2 } '')9proved . OMB r! - 2050-0039 . Expires 9 .30.99Inform . on in the shaded areasis not ri 1 :Iired by Federal taw,3 Gone- s Na and Mailing Address -U1 . ARHX `'DGBI,'-j2ZM DIST AK GY A - M-FR, y C AM F LL ) .P(1 BOX ?x)66.4 . Generator s Phone !7. ` for 5K 99 0 -{)066 (%1 .7~- ">6.US EPA II P j r,,ber5 . Transport, it I Company NamirNorth ? AW i-4tv1 c= :7 . Transport, or 2 Co.rripany Narr iPƒsoin -sa.j t( Rt 1'7 ?,~11.7 _ . .US EP -. IC fwr:-berWAt"X)f161 . 171,L.'s:QV-elz~9 . Designate d Facii tv Name anc Site Address 10 . US EPA ID ri . ,nber.Ctx m i fasts I4mt of Northwest17629 Cdr Spr1rrjs LarnArli nc M= .,11 . US DOT I )esct . : ti, : ;; (InUuding Proper Shipping Name, Hazard CLasa and ID Number)0NHAE JDOUf i4XSTg, SOLID, J .O . ;i . (DOO* ) 11U13077 PGIII .( DOO .aJIRGI(171 iRAT015 . Special dandling !ttstructiors and Adeitional InformationCab016. GENERA rOR'S CERTIFICATION : I hereby declare that the contents d 1Ns ~Igr .ment a :a lurly and accurately dasalbed above byproper sr pping name and are staSSllied , pet cod. martcod , and labeleWplecarded , and are in all jespects in proper concitlon br transportaccording to applicable international and national government regulationsIt I am a ergo quantity goneratt ‚ r. I certify that I lave a program in place jq reduce ti•ui vo(fne , and toxldty of waste venerated to the degree I have determined to beeconomic ally practicable and that I have a .teaed the practicable method of treatment , sicrag2 , o disposal alrrontty avail ible to me which minir :tizas the present and futurentreat to human hr.afth and the environment : OR . If t am a small quantity generator, I have cram a good faith effort to rdrrmize my waste oc+nerallon and select the bestwaste me iagem o nt .me'noo that is available to. Imo and that l can afford.Printed , Typed Name ltd v ~t r, tr,Xi Goth r17 . Tr a n spg rter t :>cknowied9cment of Recei it of MaterialsPrinted, Typed Name,.AI-YWQ-18 . Transpr . rter 2 Acknowledgement of Receipt of Ma t erialsPrinted , TYP d Name~Q~~?a19. DiscreF envy Indic ..tiCn Space20 . Facility Dwnar or Operator: Certification of receipt of hazardous materia ls covered by this manifest ex cept as noted in hem 19SignaturePrinteq Typed Name//7SPA Fe. .n a7aa.22 / acv . ace)Month Dav rYepr,TRANSPORTATION NO . 2i .rI- Y urt L 4tX.RJtC CISCJO.aC, w r ~A\i7A 1 i. ~aa r.2 itr--A S(ase print or type (Form designed for use on elite (12-pitch) typewriter )UNIFORM HAZARDOUSWASTE MANIFEST)‚ ‚‚ ., .t 7v r I t i t-T1.I r99A607Form Approved . OMB no . 2050-0039. Expires 9-30-991 Generator's US EPA ID No Maniw! Document No .AK 00003228( GAMS3 . Generator 's Name and Mailing AddressResourceGENInformation i n the shaded areasi s not required by Federal law .B . State Generators ID6 . US EPA ID NumberC . State Transporter's IDNorthland Services NAD9817730057 . Transporter 2 Company Name2 Pa ge 1or 1A . State Manifest Document NumberUS ARMY E NGINEIItING DIST AK CE2' Oltl-MFR ( GAJ 1.L )p0 BOX 350660066 ( 907 ) 353-70634 . Generator 's Phone FT WATNSRIQ ' AK 99703 5 . Transporter 1 Company Name06/17/99D . TransportersPhone ( 206)763-30008 . US EPA ID NumberE . State Transporter's IDWAD061672812F . Transporter's Phone 253383-30449 . Designated Facility Name and Site Address 10 . US EPA 10 NumberG . State Facility's IDChem Waste Mgt of NorthKest17629 Cedar Springs LaneArlington OR 97812 ORD089452353H . Facilitys Phone11 . US DOT Description (Including Proper Shipping Name , Hazard Class and ID Number)-W-,a( 541) 454-264312 Containers13 .14 .I.UnitWaste No .No . TypeTotalQuantityWtNoI,13RQBA17749PRAT b.0RC.d.J . Additional Descriptions for Materials Listed AboveK. Handling Codes for Wastes Listed Abovea) 004133 -00 - - LEAD COITh1IIR° SOIL - DA01 (!)a)15 . Special Handling Instructions and Additional Information16 . GENERATOR' S CERTIFICATION : I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified . packed , marked, and labeled/placarded. and are in all respects in proper condition for transportaccording to applicable international and national government regulations .If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity c' waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method of treatment , storage, or disposal currently available to me which minimizes the present and futurethreat to human health and the environment ; OR, it I am a small quantity generator, I have made a good faith effort to minimize my waste generation and select the bestwaste management method that is available to me and that I can afford .Printed/Typed NameTASignatureMonth DaySignatuereMonth Day YearSignatureMonth Day Year17 . Transporter 1 Acknowledgement of Receipt of MaterialsPrinted /Typed NameNsPoTYear18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameER19 . Discrepancy Indication SpaceS1r20 . Facility Owner or Operator : Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19SignaturePrinted/Typed NameMonth Day YearEPA FFonn ‚700.22 (flow. ts ) Pr.vlou, s ftons we oe.wefrORIGINAL-RETURN TO GENERATOR11i17/ vi t,i) t'br"'E DFtr_ 2t rfC L ` . I C-Y 1SYONSE INF012HA'J'L09,CA‚(7)2-?901G.)4371607yDPkxtsc p an t ro rypu "1FMrA ` d i.y ttell Inr' iw mt f.waP (12-jitch) typ.writ*r .)1 Generators US EPA ID No .Fa m Approved . OMBf4P‚‚rife.? DowUNIFOA M HAIARDO U SWAS" E MANIFEST N aO 0OW3228A. t ;tate Manifest Document NumbeiL AKMY E K :I krcliR IN(, D) : S" 1' AK CF130A--rt dq typewriter. Generator's US EPA ID No . AAentiaal tfoa,ntwtt~No .RNHAZARDOUS1~ 1UN IFOWASTE ; MANIFESTAIKR000Q03228 L Lm2 Pt: ge 1of1Information in the shaded areasis not required by Federal law .3 . Generator: Name and Mailing 4ddressUS AR? y . MM E RING- oxsr AK (EOA- O-1cR (r:PJff4..,L )PO BO% 350664 . Generator: Phoner wAT'tisRTc f r AK 99"1)3-0066 S9O71 -1h .ƒi5. Transporte 1 Company Name a ; US EPA ID Number,CA=Ic es ifAP19R1773~'w48 . US EPA ID Number7 . Transports 2 Company Name-fY- !110 . US EPA ID Number9 . Designatec Facility Name and Site AddressChew W liste log t of Northwest17629 - :edar Springs Lane_ y OR 97812hr 11nc7 cont 1 . US DOT D ascription (lnCluding Proper Shipping Name. Hazard Class a†7! I1,1 `lumoe: )aENEHAZHD005 mere, 501.10, N .G .5 . (D0081 i 11L3077 P6ITl. (DOtla 1RQ(fGI(171 1RAT015 . Special h andlin :j Instructions and Additional Information16 . GENEAAi DR'S CEpr1FICATION : I hereby oeclara that the contents d this consigninant are fully and accurately described above byproper shi ping t-ame and are classified, packed, marked . and IabeleGtplacarded, arid- re it all respects In propercondiion for transportaccording o applicab . ‚e Ii 4ernariotal and national government regulations .It I am a L rge quantity peneralot, I certify that I have a program In place tc reduce the v it do and lo,ddry of waste gtxterated to the de,. .- I have determined to beec.onomla Iy pracacable and that I have selected the practicable method of treatment,stora a ‚ ‚'r disposal currently availainle to me which ml : d'e Las the present and futurethroat to h ,man health and the environment ; OR, If I am a smell quantity generator, I have -n-de r, good faith effort to minirruze my waste g .mr,radon and salad the bestwaste mar agement method tha t i s available t o me and that I can afford..Printedf yped I : - U.aLhAC' tF+ vi?`-IL K~17 . T ra n spo ter I Acl,tr owledgem ento f Race pt of Materials' ~Pr int d / "Sped K .-ileMV !-f- /f wc~Montn Day Yeare j~ y r18 . Transpo - ter 2 AL knowied9emert of Receipt of MaterialsPrin ted ty ped 14,Styrtr r .'te0RMonth19 .,; Discrep + racy Indication Space.Facility t /yrtel;i; Operator : _eru6cation of receipt of h azardous mate r i als -o e.rel$lgnaturePrinted /19PA Form 1700-22 (low . Nr!pr- ‚ iota' bone ors 0b~&Day YearI//1 ~7 99Z-TRANSPOR' : 4:"i.:- / ,10 .2t .ept as noted in i r n 1 9 .%/C :~Month Dayyear99A607e print or type (Form designed for use on elite (12-pitch ) typewriter )UNIFORM HAZARDOUSWASTE MANIFESTForm1 Generators US EPA ID NoAIQbD0000322806/17/99Approved . OMB no . 2050-0039 . Expires 9-30-99MartMast ~~(G&MD7~‚Page l1ARMYF3iGII'ffitIIIIGAK DISTC'30A -M-ER (.L )PO BOX 3506699703-0066 (907) 353-70634 Generators Phone ET iAINS'RIMN AKB . State Generators ID5 . Transporter 1 Company Name 6 . US EPA ID NumberC . State Transports 's IDD . Transporters Phone E . State Transporter's IDNorthland Services iQ~D9817730057 . Transporter 2 Company Name 8 . US EPA ID NumberF . Transporter's Phone (253)383-35WResource Recovery KAD0616728129 . Designated Facility .Name and Site Address 10 . US EPA ID NumberG . State Facility's IDChest Waste Mgnt of Northwest17629 Cedar Springs LaneArlington , OR 97812 ORD089452353H . Facifitys Phone(541) 454-264312 . Containers11 . US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number)NaERATORInformation i n the shaded areasis not required by Federal law .A . State Manifest Document Number3 . Generator's Name and Mailing AddressUS2of~t13 .TotalQuantityNo . Type14 .UnitI.Waste No .WWoISOLID,10RQ1A16830Pb.C,d.J . Additional Descriptions for Materials Listed AboveK. Handling Codes for Wastes Listed Abovea) 004x33 -00 - - LM C0iIY h1M' BOIL - DI101 (11)a)15 . Special Handling Instructions and Additional Information16 . GENERATOR'S CERTIFICATION : I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled/placarded, and are in all respects in proper condition for transportaccording to applicable international and national government regulations .If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity c1 waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and futurethreat to human health and the environment ; OR, it I am a small quantity generator, I have made a good faith effort to minimize my waste generation and select the bestwaste management method that is available to me and that I can afford .Prlnted/Typed NameTASignatureMonth Day YearSignatureMonth Day Year17 . Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed NameNSPOT18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameSignatureMonthDayYear20 . Facility Owner or Operator Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19Printed/Typed NameSignaturerMonth DayYearER19 . Discrepancy Indication SpaceFATEPA Fare $7V042 (pw . F-U) Prwlow editions w. ob oy.,ORIGINAL-RETURN TO GENERATORbb _11t.u^uar- :.*‚%F HOUR EF iCY RESPONSE TMMON , =l~T,L (907 ) 27a.-9007 ‚ ‚ `08/24 /99;r r.PIctise Dnnt ip tqW . (For m deigned for use on otne ;12- p.tch) rypowntcr i Form Approvod . OMB no . 2050-oo39 . Expires 9-30-99ilenthad. ooc†n,.rt tner.uo( s US EPA ID No .y ?age 1 Information in the shaded areUNIFORM'. HAZARDOUS 1 . G''G lMa7 r t 1 is not rs+ quired by Federal lavAKI 000003 228WA'$1 'E MANIFESTI3 . Generatc rs Name and Mailing Address3 ARM ,U , ENGY E RT13G DLST AK CEPOA-s t,erol reerigr n. fell epoft's e‚ape r Inperel at retard- west,Frinf .d,rTYF -d Nome:7t i-~V9T 17 Tro :ports r 1 Acktto ‚ l lydyem en+ of Ittrcr pt o f Mor erialsrt.X ~YF1 :A I OtinredlTyp ‚ d Nome y..+~GLRlyv_-oT:r naturer+Il~r'.r,tIMe‚‚rh OarV-., O- .AA*.. e.0 ' 18 . Tro o porter 2 Ackno_iedoement . d Race:pt o f Mof VialsTff.d 'Typ rd!`\jaipnatur.' 1/1J Mon,n`Do'g ~ .'~ 1P pixreponcy indocolion Space20 . foal,ry Cl .r se e . Op.ro/ar : Cerfifconon of r .seep ' of att, netenois cc-red by :,'h mani{est except as noted in Item 19 .Seed naty r eI 1Pnwi .d / I yp ,d Nome.TRAPIs."OPTFR ?i2To' d9006ZLZL06d .A03 saw L n .,+ las d L L L 4d d6I : ZO00-OZ-u1--PNON-HAZARDOUSWASTE MANIFEST1 . Generator's US EPA ID No .Manifest2 . Page 1R R 0 0 0 0 0 3 2 2 8 Dnufn'1No7of 1ors Name Moiling Address3 . GeneratlAE RING DIST AK CEF%- 0 -FR (GAH3ELL)PO BOX 350664 . G enerat or's Phone ( F "SRI( T AK 99703-0066 (907) 353-7063US EPA5.llor~hlai1Services7. Transporter 2 Company NameNumber. Transporter's Phone6 . A D 9 8 .11 78 . US EPA ID Number(206)763-3000B . Transporter's PhoneResource Recovery ADO 6 1 6 7 2 8 1 29 . Designoted_Facili Nome and Address 10 . US EPA ID Number~~TH4 TH & LADSSF'ATrIE , NA 98108(253)383-3044C . Facility's Phone(206) 623-4000XEKPT12 . Containers11 . Waste Shipping Name and Description13.TotalQuantityNo . Type14 .Unitt Vola . 11TEIIIL WT tEGULITED By DOT ( SCw IKYAL)GENERAT0Rb.Id..c..D . Additional Descriptions for Materials Listed AboveE . Handling Codes for Wastes Listed Abovea) 162942 -00 - - SCM WILL, IARAICO CEITIIICATIOI 10 . 99-1119 - 01101 (24)a)15 . Special Handling Instructions and Additional InformationGDKUT01 'S CEITIUICATIOI : I hereby declare that the contents of this cansign .ent are fully and accurately describedabove by the proper shipping nane , and are classified , packaged, carted , and labelled/placarded , and are in all respectsin proper condition for transport via air , road, rail and urine vessel according to applicable international andnational regulations .16 . GENERATOR'S CERTIFICATION : I certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste .SignaturePrinted/Typed NameTRANSP0RTMonthDayYea,17. Transporter 1 Acknowledgement of Receipt of MaterialsSignaturePrinted/Typed NameMonthDayYearMonthDayYearMonthDayYear18. Transporter 2 Acknowledgement of Receipt of MaterialsSignaturePrinted/Typed NameE19. Discrepancy Indication SpaceFAC20. Facility Owner or Operator : Certification of receipt of waste materials covered by this manifest except as noted in hem 19 .TYPrinted/TypedNameSignatureORV NAL-RETURN TO GENERATOR99A607 08/23/99~,~)Manifest. Per . 12NO J HAZARDOtbC 1 . Generator's US EPA 10 NoKrK .R .0 .0 .0 .0 0 3! . 2 & ),'1117`1 7 of 1WA STE MANIFESTcnerator s lame ~nd Mailing Address,l-I}US ARl~C E I RING DIST 'AK C o*-co :.im GAr` ~, )PO BOX 35066 Ie, t,aonoro tor' s phone ( FT N&Ili(SRIG'1‚!rI' AK 99703-0066 (907) 353- 70635 . Transporter Company Name. .Northland ServicesUS. E?:: ID Hj6.nberjI .A .)7 .'0.1,7 .7 3.sn.._ ._. US EPA ID Nil-,bar7, Transportor ! Company NomeReBOtrc s Rec a=yAA. Transporter'sASPhone(206)i__763-3000L Tnsnsporter's Phone, ,.A .D ,001 ,6 -7 2 B 1 2 l (253) 383-30449. Designated -oc;lity Name andSiteAddress)0 . US EPA lD Nw,mI rC. Fccility's PhoneRAERNM RECYQ..4 1'H & C .ANDE RSJMLE, WA .,9b108(206) 62 .1-4000IA.UnitWT Vol1ATBi LAL IqT p1;GULA!&[ BY DOT (SCQAP KTAL)E . Handling Codes for V aster Listed AboveD . Additional I escriptions for Mo,crisls Listed Abovea j 1629 ( 2 -00 - - SCUP K.ETAL, QABhI1CO CEITIFICATI01 10 . 99-1114 - Q141 124)15 . Special Ho idling h i .'ructions ant; Addiiona InformationG1L71BYATOp'S CSETIY.ICATI01 ; I hereby declare that the contents of thIT rx- ;rlgn.ent are fully and accurate y describedabove by . Lhe proper sb'pping nan ,and ire classified, pactaged , e4rtewii, ,,pd labelled /plac ;rded, and are 'n all respectsla proper condition for transport cola -air, road, rail and term. vaafrrl :wording to applicable lnterfnat~onal andnational :equlations .. t ce a `ST~Qr. n s h malifest are not d to federal regvlMl16 . GENERATC R 'S CERTIffCATIPrinted/TyF ad Name.17'•r.., .:P'ere;nt a f'Mnrerial,printed/TyF ed Name it I r .004_14`/. AfAA'I Si9na18 . Transporter 2 Ackn' ' edgement , )f Receipt c ‚f MoteiolsPrinted /TyFed19. Dlscrepon q Indication 'Focefor reporting props dispoml of Haxordov3 Wwte .Sifitnon+%Nom,_ _ _riSignotv,e-2i20 . Facility Owi er or Operator. Cerfiiieation of receipt of waste materials covered by thi murtiep except as noted in b- :m 19.Y RESPONSE INFORMATION, CALL---F'CIt 24 HOUR EI'( 907) 272-9007 ---99A607 08/23/991 . enerator's US EPA ID No .NON-HAZARDOUS-WASTE MANIFEST3.Manifest) R 0 0 0 0 0 3 2 2 8ftul4nl c82 . Page 1of 1Generator's l~j~pykpAG DIST AK CFF'0&- -FR (GAH~LL)P0 ID 35066W flISItIGf' AK 99703-0066 (907) 353-70634 . Generator 's Phone( FTUJs . _jransransporter7. T2A D 9 8 .11 7CompanyResource Recovery9.Number6.jai d mSeiYvN?cesrteNameADAddress4 ZH & LAIRSSEATTLE,A . Transporter's Phone0 0 58 . US EPA ID Number061(~) 763-3000B . Transporter 's Phone6 .7 .2 .8 .1 .210. US EPA ID Number(253)383-3044C . Facility's Phone(206) 623-4000VA98108XEMPT11 . Waste Shipping Name and Description12 . Containers13 .TotalNo . TypeQuantity14 .UnitWt Vola . IATEIIAL JOT IEGQLATED BY DO! ( SCUP IETAL)GENERAT0Rb..c.d.E . Handling Codes for Wastes Listed AboveD . Additional Descriptions for Materials Listed Abovea) 162942 -00 - - SCUP IETAL , UBAICO CEITIFICATI01 10 . 99-1119 - DI101 (25)t)15. Special Handling Instructions and Additional InformationCDEUT01 'S CRITIFICATIOI : I hereby declare that the contents of this consiguent are fully and accurately describedabove by the proper shipping nue , and are classified , packaged , urked , and labelled / placarded, and are in all respectsin proper condition for transport via air, road , rail and urine vessel according to applicable international andnational regulations .16. GENERATOR 'S CERTIFICATION : I certify the materials described above on this manifest ore not subject to federal regulations for reporting proper disposal of Hazardous Waste .SignaturePrinted/Typed NameTRANSPORTMonthDo,Year17. Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed NameSignatureMonthDayYearSignatureMonthDayYearMonthDayYear18. Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameER19. Discrepancy Indication SpaceFAC20. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest except as noted in Item 19 .TYPrinted/Typed NameSignatureORIGINAL - RETURN TO GENERATORe - -FOR 24 HOUR f24: R( 77CY R ESPONSE INFORHATIObf r CALL ( 907) 272-•900799A6071. toNOI J-HAZARDOUS09/23/49r1 US EPA ID NoWA STE MANIFEST--eb O 0 o t.xManifest~~ ~ nd3 . Genertgs I qW-- MCsI1lCt. t{YfG DIST AK G POA-C0-FR ( GAHFl1;w.,Sa)PO . ~0X 35066`1AX 49703 -0066 (~,O7) 353-7063(FWINSRIQITA. Genrroro / s Phone5US EPA iD Nu bemie. NOr~[iL8:7c3mservl605A. Tmnsporter 's PhoneA D98';I 773005e.(206)763-3000EPA f1 Num',,arU5WADO6, .1 67 281 2(253) 383-304410. US EPA 1 Npmknr(206) 623-4000IEXEMPT)a.12. Containers 13 .Tota lU nitNo .Type,Quantity Wit/volNATBA AL NOT REGULATED 8T DOT ISCal3 WAL)O'0' C'E . Handling Codes for V. ates Listed AboveD. Additional C,scripitons for Mote ;i c'h listed Abovedi !b2942 00 -PSCI P 'AL, a At .ANCC Cb'NTIFICATIOA N0 . 99-1115 • t. M i (2511115 . Special Hot dying Instructions and Additional InformofionGEL ATOP 5 CE'?TIFICATION : 1 hereby declare that the cooteLLS of this consigavent are tu11Y and accurate'( describedabove by ne prnpec shipping na .e,and are classified, pactaged ,ailKtld, tad label led/placacded, and are 1 all respectsin proper condition for transpozL via air, road , rail and aarin4°resiel according to applicable lnternat_oral andnational equlatlons .16. GEN ERATO VS CERTIIIC{ .TION : I conify the matatiols described abe a on this rnan`i(ettPri d/Typ d Name&&A tt v S of O V7Sig.rrr rot sub! - d to federo l reg ulation for reporting propsw lispo oI of Hozordan Wove .DayYearMonth DarYearmonthrc17 . Transporter i Adkn v r i dpemenr o f Receipt of Mat erialsPrint d/Typ td Nome 4'.4'Q/cGa/4,QDSignoiu.11-A.18 . Transporter ? Acknov iedgement : Receipt of Mot oriolsdSignatum`Name'-Printed/ Typ ,1t . Disereponcy Indicw 'e•• tpocr1;ail''-20. Facility Owr or or Oporater : Certification of nrceipt of waste materials covered by thi- me n far' except as noted in hem 19... . I K L, I Qy,_MonthpayYearIN11-(,1g9ace99A607NON-HAZARDOUS08/23/991 . Generator's US EPA ID No .ManifestWASTE MANIFEST K .R .0 .O 0 0 0 3 2 2 8t" .'Kny"C192 . Page 1of 13 . Generator's Name and Mailing AddressUS ARHY ENGINEERENG DIST AK CEPQA-CO-FR (GAMS . )PO BOX 350664 . Generator's Phone( FT 1AINS UGH'T AK 99703-0066 (907) 353-70635.Transporter1CompanyName7.Transporter2Resource6 . US EPA ID NumberA . Transporter's Phone. A . D . 9 .8 .1 .7 .7 .3 O 0 5Northland ServicesCompanyNameRecovery8 . US EPA ID NumberB . Transporter's PhoneA . D 0 6 .1 6 .7 .2 8 1 29 . Designated Facility Name and Site Address 10 . US EPA ID NumberRAHANW RF>rYCL NG4 TH & LAIRSSEATITE, WA 98106(206) 763-3000(253)383-3044C . Facility's Phone(206) 623-4000.X .E .H P T12 . Containers11 . Waste Shipping Name and DescriptionNo . Type13 .TotalQuanta14 .UnitWt vola' IITBRIAL WT LEGULATKD BY DOT ( SCRIP IBTAL)GENERATb.c.0RE . Handling Codes for Wastes Listed AboveD. Additional Descriptions for Materials Listed Abovea) 162962 - 00 - - SCRIP IBTAL, UBAICO CK1TIFICITIOI W . 99-1119 - DI101 (26 )a)15 . Special Handling Instructions and Additional InformationGBIODZITOI'S CBRTI ?ICITIOI : I hereby declare that the contents of this consignaent are fully and accurately describedabove by the proper shipping nue , and are classified , packaged , urked , and labelled/placarded , and are in all respectsin proper condition for transport via air, road , rail and urine vessel according to applicable international andnational regulations .16. GENERATOR'S CERTIFICATION : I certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste .SignaturePrinted/Typed NomeTANSPORTERMonthDoy Year17 . Transporter 1 Acknowledgement of Receipt of MaterialsSignaturePrinted/Typed NameMonthDayYearMonthYear18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameSignatureDay19 . Discrepancy Indication SpaceFAC20. Facility Owner or Operator : Certification of receipt of waste materials covered by this manifest except as noted in Item 19 .YPrinted/Typed NameSignatureORIGINAL - RETURN TO GENERATORMonth Doy Year99A607• NOI J - HAZARDOUSWASTE MANIFESTs06/2 3/i91 . Generators US EPA ID No.Monffen~ .K .R .0 .O .o O .O .3 ,2 .2 8 jer.WnY'I°93 . Crnerator's Jome and Mailing AddressUS ' ARHY 2 GIN1 RING L1ISl'.?QA-CD-FR:AX (f( t'8F' LL, )PO k1QX 35066A.Genarotors none ( F2' W AIINSRIGHI ' AK 997O3-• o066 (907'13`3-10636.. US EPA ID NumberA . Tninsponer's Phone 'A D 9 1 7 7 ..3 0 0 5I 8.7 . Transporter CompanyfNomeReeourca RecoveryI10.9, Designated I acuity Name and Site AddresshAIiANCC RECYCLINGU9 ID NumberA D O 6 1 6 7 2 8 3 2. US EPA !0 Numbert (20606 :~-3000B . Trtmsporices PhoneM(253)383-3044C. Focilifyh Phone44 rlli & LANDiERSS12 TILE , WA 96108(206) 62 -400012 . Cantainers11 . Wostc Ship )in9 Nave and DescriptionNo .;Type i~IIlIAYH JL 907 UGJLATE BY Q0T i SCULP METAL)1tt13 .la .Total UnitOvanti Wt Vcl•C1rl1E . Handling Codes for wastes Listed AboveD . Additional C escripncn6 tar Materials Listed Abovea ) 1t2342 00 - SCRAP liisPAL, flAEANC0 Ci LTlf1C)T1ON K0 . 99 -1119 - ?igill Itf)a;15 . Special Mar dung Inuruerfons and Additional InformationG11 J.AT(lu S CiiYTt iCATION : I hereby deciac~t4hai the co4Lants 91. ;hi . :a/:f~tgneent are tuU f cud accuratecaacrlbedabaire by he p ap ehippi2g naae , and are classified, packaged , ilarkea , and label led/placaf•ded, and are , all reapectain proper condl'toli 1017 tr ospoit via alt, road , tall and marine K•aasci ::cording to appli :able interoai: . nil and+j,vnational ogula tans .16 .GENERATO !'S CE RTIHLATI ON : I comfy nc . mororioh described abo.e an thn non- fs re .o' '* ea to federal ra ularions for reporting proper .irposol of Hazardous wost ..DayYOGIPrinted/Typ, d NomeN F..=-14,LF =-14,4L4= 10,C s/$ 6• p - Sign y - -, MonthT 17. Trays r sner I Ac kn ow ledgement o f ReceiptRPrimed /Typ rA.dp 18. Trn spo rt e rofMaterialsA~NomeSid__nature.~MonthAchno • ted‚g emo m o f Receipt of MaterialsR printed /Typ ~d Nom I .Tear''Si. _ - ,..ourrERDay..ahrhA .d19. Discrepancy Indication : .aceFAC20. Futility Own tr or O•saratar: CertiFcotion of nrceipt of waste tnefer41$ covered by,tl)it m. n : st except of noted in her 19.SignatureTRANSPOPTr_rl # .er..FOR 24 HOUR ICY RESPONSE I NFORMATION , CALL (907)99A607 08/23/99Reltrcar'OXUPAIRy''a3 2 2 8 f^'D6ZUrfilnt&oyr~q ~ f e0. 2 .NON-HAZARDOUSWASTE MANIFEST3 . Gener sfEGa9Mof.911W DIPO BOX 35066FT WJNSRIGHT4 . Generator's Phone ( )5 . filmm"g} a7 . geget&C:%~C+pegAD$1&dP'i9 . immuW "I{Ti. :Z41S22RSiteAD qP Sj rt1e3 0 0 5lDd4"'Ib*2Address8110 . US EPA ID Number2. Transporter's PhoneB. Transpo rt er's Phone(206) 763-3000(253)383-3044C . Facility's Phone(206) 623-40004 TH & IAm sSEATI1E , VA 98108X E M P T11 . Waste Shipping Name and Description12 . Containers13 .Total14.UnitNo . TypeQuantaWt Vola . IATE1IIL 10T REGULATED BY DOT (SCAM IET11L)•0 .1M 1 .2 .4 .6 .0Pb.C.d.E . Handling Codes for Wastes Listed AboveD . Additional Descriptions for Materials Listed Abovea) 162942 -00 - - SCALP EM, LABIICO CELTIFICATIOI 10 . 99-1119 - DIli01 (27)t)15 . Special Handling Instructions and Additional Information _GBIIIIT0I ' S CIRTIIICATI01 : I hereby declare that the contents of this consignunt are fully and accurately describedabove by the proper shipping nue , and are classified , packaged , urked , and labelled / placarded, and are In all respectsIn proper condition for transport via air, road , rail and urine vessel according to applicable international andnational regulations .16 . GENERATOR 'S CERTIFICATION : I certify the materials described above on this manifest ore not subject to federal regulations for reporting proper disposal of Hazardous Waste .SignatureMonthDayYearPrinted/Typed Name17. Transporter I Acknowledgement of Receipt of MaterialsSignaturePrinted/Typed NameMonthDayYearMonthDayYea,MonthDayYearIf 18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameSignature19 . Discrepancy Indication Space20 . Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest except as noted in Item 19 .rPrinted /Typed NameSignatureORIGINAL - RETURN TO GENERA'Op• `F0 24 I OUItt l WEIV-71 M-MPONSE IN)?0RMATI(I:;', CALL (907) 272-9W799A607()8/2.3/49N etarcWCU!aPPIUOda3 . .2 2 . 8. GhoeumAn3fii.nNO N-HAZARDOUSW{STE MANIFEST3 .1 Geerdt 's nPO BOX 3506601ST. . .Oa.C2YClA-ZS'V)CA1)0° l lk) . 71 -}, '. } •3 . : . (1fJav~rY,13 . Speciol r .ndlinf Instruetions a,d Adda:ona InformationGbt18WTl'i 'S C2T1lfCAT3-N4 : 1 hinebp dee)are LhaL khe c uteatP at .414 .rtRligh%e b t are Wit is •Ccvzat : ly describedd ore b• the proper zh4j;)iaq gue,asd are c14101iId Services lM A ll 9'8 ;~ 7 `7 3 .0 P .58. US EPA ID Num6gbr7 . Transporter ! Company NameResource Recovery. A . D . 0 ;'G ,1 .6 , 7 .2 .8 .1 , 29. Designated acuity Nami and Sits AddressBABA) CC R .'YCLM-!10. US EPA 10 Number4 TH & L .ARS11I1 , WA 93108(206) 62:1-400011 . Wove Shipping Name and De . aiptionKATE ; ILL E1 aRGUlrATK1) BY DOT (SC&AP METAL)0. Additional C ezeriptions for Materials Listed Above11 162942 -00 - - . CW JET", "LKCO C†YTIFICCATION 1O . 0-111 :+ - BIRO! 131)15 . Special Ha dling.-,hIr fictions and Additional informationGƒiBY.AYOF S :CERTIFICATIONI Lerebti declare that the contetits al to 9 :oL ':ignaent are tally and accurately describedabove by . he proper shipping naae , and are claeaitied , pactaged , wu ted , and label led / placarded , and are . a all respectsin proper condition for transport via iii, road, rail and aallne .,ew according to applicable international andnational -agulitions .16. GENERATO .S CERTIRCATION : I certify s he mate rials described above on this menlfest ore not rbiea so federal regulations for r eporting proper Jisposo l of Ibzordmrs Wean.Primed/Typ :d Nomefj.p Vf-It+V V. ,LI4 - OF` 1/517 . Transporter I Acknowledgement of Receipt o f MaterialsPA ted/Typ :d Name L l4 ~4. .5,.~/I)5-'R,-C-Oh •eAy li)L >!18 . Transporter 2 Ackn owled gement c l Receipt o f Mai erio s20 . Facility Owr x or Ow,,, or: Cerlilicotion of oxeipr of waste materials corured b y this moo fro except as noted in Item 19 .TRANSPOR"rL ;z. t!199A607NON-HAZARDOUSWASTE MANIFEST3 . Generator's Name anilin1 . Generator's US EPA ID No.DManifestK .R 0 0 0 0 0 3 2 2 8Address(08/23/99mo2 . Page 1p4l ?f 2Jc of 1)GAM _--• L .US ARMY W06II RING DISP AK (P0A--00-ER n*tRtrPO H]X 35066AK 99703-0066 (907) 353-70634 . Generator 's Phone( ET WIHSRIQ5.Transporter7.Transporter1CompanyName6 . US EPA ID NumberA . Transporter's Phone(206)763-3000Hor~hland Services A D 9 8 1 7 7 3 0 0 52CompanyNamej Resource Recovery8 . US EPA ID Number8. Transporter's Phone.ADO 6 1 .6 7 2 8 1 2C . Facility's Phone9 . Designated Focili Name and Site Address 10 . US EPA ID Number4 TH & LAMMSSSOWME , VA(253)383-3044(206) 623-400098108XEMPT.12 . Containers11 . Waste Shipping Name and DescriptionNo . Typea13 .TotalQuanta14 .UnitWt Vol. IITSIIAL WT 1ZCUL ATƒ BY DOT (SCRAP IIETAL)b.C.d.E . Handling Codes for Wastes Listed Above0 . Additional Descriptions for Materials Listed Abovea) 162!12 - 00 - - SCRAP IKTAL, LABAIC0 CBYTIIIC &TI01 10 . !9- lII! - Dit01 (32)a)15 . Special Handling Instructions and Additional InformationGU KIII0t 'S C12TIIICATIOI : I hereby declare that the contents of this consignsent are fully and accurately describedabove by the proper shipping nue , and are classified , packaged , .arced , and labelled / placarded , and are in all respectsin proper condition for transport via air, road , rail and [arisie vessel according to applicable international andnational regulations .16 . GENERATOR 'S CERTIFICATION : I certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste .SignaturePrinted/Typed NameTRANSMonthDayYearDayYear17 . Transporter I Acknowledgement of Receipt of MaterialsSignaturePrinted/Typed NameMonth18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed NameSignatureMonthDayyearMonthDayYear19 . Discrepancy Indication Space20 . Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest except as noted in Item 19 .Printed /Typed NameSignaturer tPlr ;INAL - RETURN TO GFNER4SOP11/17iaat1J L.1.u : uu rt112E 3PONSE INFORMATION, CAM, (90.1)99A607s %.#w%L~W a`~Manifest.K .R. .0 .O .O .O .0 .3`'! 2 BWR STE MANIFESTA1O8 / 2 3/99Ti1 . Generolors US EPA ID No.3 . Generafer's Name and Mailing AddressUS AM FNGINkERING LliSir AK -CO--FA-~(PO BOX 35066..L)14,. Generator's Phone ( FT WAIZI5RIG1[)' Afi 99703-0066 ( 90 .7.) .35`3-'10636.North la nd ServicesUS EPA ID Nvrrl,er7, Transporter 2 Company NameM .A .D ;9 .8 ,1 .7' .3 3 .0 O 58 . -US-EPA I NumberResource RecoveryA .D .O .b :='1 .61,7 2 S .1 29 . Designated =aciliry Name and 5tu : AddressRA13N X RECYCLING10.a. Transporters PhoneBUS t~r-_17. Transporter I Acknowledgement -,f Receipt of Ma terialsSignal"QwRpPrinted/ TyF ed Naner18. Tra nsporter 2 Acknow t aaement of Receipt o f Ma teri a ls~S;ynafv mar! -Pr6,tes1/Tve ed Na r .e_~i1F19. Oil-pa/c, Indicori ., r SpaceAFII-------_. _ . . . .; Certi'icotion of receipt of waste materials covered b1 tI' mono ^ auepl as noted in M-m 19 ..fI- 20. Facility Owe per or Opo' otorTY.,blept„ payr(:is aI :nD .,IaC;t' D .' M',NON-HAZARDOUSgoo1 . Generator's US EPA ID No .WASTE MANIFESTManifestDo um nt No .- R .R .0 .0 .0 .0 .0 .3 .2 .2 S G .A .)i .2 .82 . Page 1of 13 . Generator's Nome and Mailing AddressUS ARHY ENGIN LNG DIST AK C P0A-CD-ER (GAIMd,)PO BOX 350664 . Generator's Phone( FT Iffy-MSR.IC TI' AK 99703-0066 (907)353-70635.Transporter1CompanyNameNorthland Services7.Transporter26 . US EPA ID NumberA. Transporter's Phone. A . D . 9 .8 .1 .7 .7 .3 .0 .0 .5CompanyNameRe ouI ce Recovery8 . US EPA ID Number(206)763-3=B. Transporter's Phone. A . D .O .6 .1 .6 .7 .2 .8 .1 .29 . Designated Facility Name and Site Address 10 . US EPA ID NumberRAW" REMCLM4 TH & I J4I SSEATTLE, VA 98108(253)383-3044C . Facility's Phone(206) 623-4000.X .E .H .P .T ..12 . Containers11 . Waste Shipping Name and DescriptionNo . Type13 .14 .TotalUnitQuantaWt Vola.IATBIIAL LOT 1BGQLAT EO BY DOT ( SCRAP IETAL)G b.ENERA c.T0R.d.D . Additional Descriptions for Materials Listed AboveE . Handling Codes for Wastes Listed Abovea) 162942 -00 - - SCRAP IETAL, 1ABAICO CERTIFICATION NO . 99-1119 - DIRO1 (35)a)15 . Special Handling Instructions and Additional InformationCE'IE1ATOR ' S CERTIFICATION : I hereby declare that the contents of this consignment ire fully and accurately describedabove by the proper shipping naee,and are classified, packaged , marked , and labelled /placarded, and are in all respectsIn proper condition for transport via air , road, rail and marine vessel according to applicable international andnational regulations .16 . GENERATOR 'S CERTIFICATION : I certify the materials described above on this manifest are not subject to federal regulations for reportingPrinted/Typed NameTRNSF,RTERproper disposal of Hazardous Waste .SignatureMonth Day YearSignatureMonthDay YearSignatureMonthDayYearMonthDayYear17 . Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed Nome18 . Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed Name19 . Discrepancy Indication SpaceFA1T20 . Facility Owner or Operator: Certification of receipt of waste materials covered b5' this manifest except as noted in Item 19 .YPrinted/Typed NameSignatureORIGINAL - RETURN TO GENERATOR11/17/ 98 W.D 10401 k- A.1(49 9A607NON-HAZARDOUSW),STE MA IFEST3 . Goncraror' sNameovi!081 -21• GcncroTors US EPA 10 N6 ./Ma nifest 2. Pc .ye 1Docume n t No.• K-R •0 .4 .0 .0 •I• -3 • 8 ~ - alMoilingAddress1 . _1 ;4 4US ARMY I2iGINJ;3 RZA1G 1)IS'r AK tmvoA-{X)-1'R ;t Ghll~tlE:Li )POBOX3,066,A . Gereroiers Phone (WAI1iS12ZGH.r A{ 99703--006 (902'1)353-70635 . Transporter I Company`NameNorth 1 . Ind Services7 . Transporter 2 Compon1/ omerReam :e Etec vez9 . Des. gneied Fociliry Nome and Situ Address6 . L15'ePI. ID NumberA. Transporter's PhoneIk • A .13 9'7 .3 .0 .0 .5B . US EPA IDh'vmf.er.B. Trnnsporier's, PhoneyICI . A :0 .0 .6-1 .6 . 7r.2 .A .1 .2110. US EPA ID Number(206)763-3000C . FuclliWs PhoneRASUGI, I XafC,'TJ.NG4 711 & L1 NDi BSSEAt1 rL :, WA `4 810811 . Waste Ship ping Nome and Descriptiona.1(Al'E!IAL NU1' .iRGIJLATEi) BY GOT iSCIAP NETALIb.C.d.fp. Additional >escriprio;+ : for Mater als Listed Abort. a1 16294 : -Osi - SCRAP LTAL, R1t ANCO CgltTOICATION 00, X9-1115 . Di1,0i (35)15 . Special Mc ndling Insrru Zion and Addilioncl InformationiCE)1K AIOI 'S CRds' .FICATIOR I hereby declare that tGe conl .E:nls ct thla cmianaent are tut if and accuratr , ly deacrlbeoabove DY the props: shlpp . ag naie , and are classified , pactag d, airted, and labelled /placiirded, and are in all respectsin prope r condition for transport via air, road , rail and tarTne vessel according to applicable International i`idnational regulations .16. GENERATI )R'5 CERTIFICATION : I eenify the materials described oba ." on obis reael l ea ort nrr si eject t o Iede rol tegvtatien , for te paning props d isposal of Mavardout Wane .Printed / Ty 'ad Naroe17 . Trcnsportef..#Signo+u.e1 Acknc -i_dgemeni of Re ceipt .sf Ma terialsPrime /Ty Pod Namel+ .4.,018, Tre nsporrc 2 Ackr, Dwl edgernenl of Receipt of MaterialsSignaturVA,dosed /Ty red NomeI19, Discrepant F Indiccr-oi . Space20 . Focaity O .. ner or Operator : Certification of receipt of . ..onto materials ces•ered by +hia m r ifes' except as noted in Item 19 .Printed /Ty )ad NorneSENT BY : RABANCO ;2063327611 ;NOV-9 - 01 12 :04 ;PAGERABANCO54 SOUTH DAWSON STRE1 TSEAT rL Z , WA 98134(20M)3S2-7700 FAX(206)763-1234CERTIFICATE OF DISPOSAL. November 9, 2001OSCIAttn : Diving PortudesBill of Lading :99-1119 ( see attached)This is to certify that NON-DANGEROUS WASTE as defined on the above referenced Bill ofLading was shipped by US Army Engineering District Alaska, CEPOA-CO-FR from Gamble, AK .The scrap metal was received by Regional Disposal Company and disposed of at RooseveltRegional Landfill, 1800 Roosevelt Grade Road , Roosevelt, WA 99356 . The above described :NON-DANGEROUS WASTE was managed in compliance with all Permits and Laws Regulatingthis Facility .Final Disposition : Subtitle D and WAC 173- 351 MSW LandfilltdSignatureFor Regional Disposal Company2/0SENT BY : RABANCO ;2063327611 ; NOV-9-01 12 :04 ;SUMMARY OF LOADS HAULEDPAGE :INVOICE *9924043-K1KD;m(71) Industrial Waste - Seattle11/09 / 99 112118635,64029,14011/11/ 99PAGE112252541,22029,04011/12/ 99 112296238,00011/12 / 99 112305111/12 / 99 112319239,10041,62029,38028,80011/12 / 99 112323811/12/ 99 112325641,12042,00029,26028,96029,2206,50012,1803 .2506 .0909009008,6204 .31090010,30012,36012,16012,7805 .1506 .1806 .0806 .390900900900900Total :37 .450NSIU 299074CAXU 2590422NSIU 20115333/3SENT BY : RABANCO ;2060327611 ; NOV-9-01 12 :09 ;PAGE213RABANCO54 SOUTH L)AWSON STREETSb:ArrL.E, WA 08134(2061332-7700 FAX (20(I 7W-1234CERTIFICATE OF DISPOSALNovember 9, 2001OSCIAttn .' Divina PortudesBill of Lading :99-1120 (see attached)This is to certify that NON-DANGEROUS WASTE as defined on the above referenced Bill ofLading was shipped by US Army Engineering District Alaska, CEPOA-CO-FR from Gamble, AK .The RCRA Empty Drums were received by Regional Disposal Company and disposed of atRoosevelt Regional Landfill , 1800 Roosevelt Grade Road , Roosevelt, WA 99356 . The abovedescribed NON-DANGEROUS WASTE was managed in compliance with all Permits and LawsRegulating this Facility .Final Disposition : Subtitle D and WAC 173-351 MSW LandfillSignatureFor Regional Disposal Company~aSENT BY : RABANCO ;2063327611 ; NOV-9-01 12 :09 ;SUMMARY OF LOADS HAULEDPAGE :DATEPAGEINVOICE #9924044-K1TILT#GROSSTARENET NETONSTRUCK # CONTAINER #`(71) Industrial waste - Seattle11/09 / 99 112124739,18029,5409,6404 .82090011/11/ 99 112259911/12 / 99 112313239,08037,72029,44028,8809,6408,8404 .8204 .420900900Total :14 .0603/3SENT BY : RABANCO ;2063327611 ;NOV-9-0112 :12 ;PAGERABANCOg4 SOUTN r7AWSON STRE[rSEA'ITLE, WA 98134(2061332-1700 rAX ( 20(i) 763 1234CERTIFICATE OF DISPOSALNovember 9, 2001OSCIAttn : Divina PortudesBill of Lading :99-1121 (see a _ hed)This is to certify that NON-DANGEROUS WASTE as defined on the above referenced Bill ofLading was shipped by US Army Engineering District Alaska, CEPOA-CO-FR from Gamble, AKThe Petroleum Contaminated Soil was received by Regional Disposal Company and disposed ofat Roosevelt Regional Landfill , 1800 Roosevelt Grade Road , Roosevelt, WA 99356 . Theabove described NON-DANGEROUS WASTE was managed in compliance with all Permits andLaws Regulating this Facility .Final Disposition : Subtitle D and WAC 173-351 MSW LandfillSignatureFor Regional Disposal Company2!3SENT BY : RABANCO ;2063327611 ; NOV-9-0i 12 :12 ;SUMMARY OF LOADS HAULEDPAGE :1DATETICKET #GROSSPAGEINVOICE #9924045-KTARENETNET TONS(34) Petroleum Contaminated Soil Disposal -- Sea tt11/09/99 112133636,28028,9207,3603 .68039,00028,98011/11/ 99 112246510,0205 .01011/11/ 99 112265943,52028,86014,6607 .330Total :16 .020TRUCK #CONTAINER #900900900MSIU 2992352NSIU 299327 ;CMCU 20578443/3Date : 11 /07/01 CERTIFICATE OF TREATMENT , RECYCLING , AND/OR DISPOSALLC)This is to certify that the following waste material was received , managed, and treated in compliance withall applicable Federal and Washington State Laws and regulations .vFacility :BURLINGTON ENVIRONMENTAL TUC . 734 SOUTH LUCILE STREETGEORGETOWN FACILITY SEATTLE WA 98108EPA ID : WAD0008129D9Generator : 32944Manifest :- US ARMY ENGINEERING D1ST AK EPA ID :GAM02-99Line ProfileWasteReceipt # :N0AXRD00003228GTW-40524 Date Received :'-n11/10/99Material DescriptionFinal Treatment/Treatment/Disposal Description Disposal FacilityFinal PSC Final Date/ManifestPgLn DateShippedIA162785-00HAZARDOUS WASTE, SOLID, N .O .S .( 0008)M111 STABILIZATION /CHEMICALFIXATION /CEMENTCHEM WASTE MGMT OF NORTHWEST15969-KNT1A12/29/991B162781-00WASTE TARS, LIQUIDM061 FUEL BLENDINGCONTINENTAL CEMENT CO . L .t .CSYSTECR ENVIRONMENTALSYSTECR ENVIRONMENTALSYSTECH ENVIRONMENTALSYSTECH ENVIRONMENTAL25213- GTW25252-GTW25270 -GTW25271-GTW25310- GTW1C1A1A1AIA12/03/9901/06/0001/17/0001/18/0002/15/001C162783- ODHAZARDOUS WASTE . SOLID, N .O .S( DO08 )M111 STABILIZATION / CHEMICAL CHEM WASTE NGMT OF NORTHWESTFIXATION / CEMENT15969-KNT1A12/29/991D162782- 00ENVIRONMENTALLY HAZARDOUSSUBSTANCES , SOLID, N .O .S . (LEAD)M013 SECONDARY SMELTING KINSBURSK) BROTHERS ,INC .25196-GTW1C12/10/99Name :Wanda GrondahlncISignatureTitle : Certificate Production Specialistz0wNOW.- z xwxvzi• -FM 24 ucta II1XPC MATICN, CALL (907) 272-9007 ,( y 99A607 C43 I17j99'~AJU NIFORM HAZARDOUS l . Generatcr'$ JS --FA 'CNoLis'JFarm ADprWOC . -'M3 no , logo-Ccze .aMWde .t Dooum•ni N o .Page ! n/ormetton n.Me' 3hadeo areas i9 0l ' .OUKed Dy edaral 'ew.3~t, l0 2WA TE MANIFEST A322a0/A Stag.tytltMlget7 • Generators Name ano Ma liag Addreea.A-a,,-FR (G L)U9 Al MY P~iG MST AX tPO W X 35066T AX 99703-CC66 (907) 353-70634, Generator' s Phone F'T VMI =d . U5 ~PA .C NumoerNAMS177300SS . Transporter 1 Company NameNcrthland'Sexy icesRecoveryDesignated Facility Name and S lie Address3lL C:31CIl~L331GPC~ii 734 South Ltlci la StroatA 98108rSeattleIIaX81290913 .TotalIT v.! Cuantit2 . Containers11 . us DOT Description (Including Prayer Shipping Name, Ma3erd Claea end 10 Number)a1!9 j!3rSOLID, l ; . S. (boosIJ4 iiT.Inal(i.IL 1{.fL :...J.--14 ,I UnIWWoip)11 IL!! 601 1 PMIr rt~sntNumber~8, JS EPA !C Numtrer}tlCL61572S1210 .US PA ;O :Number7. Transporter 2 Cornpirw Name9.oiros 3-30-Ao1A1t D a iS99 '9II( DCC1 )t3i( ;3O)!1 9 ` CH 4458c . a YA3~ , 30 0,,Or3, (Kill 9 IA307 241 :1 51(111 }UK375d.ISOC.71 Et i ATCR'e CERTtFICATlONaiby seders that The oentsn * of ty!ia consignment are fully and aecurataly deacrtbed boa tryproper shlpDing name and Are clasaltied, pecked , marked, and tabsl d/placarCed and are In all respects in proper conCldon for,ranaponeaccrding to apoileabls lntarnellonal and nedeiie! govemmsnt reguladone,It I am a large quantity generator, I eenity flat 1 haee a program in place to ;educe the volurne, end ioxICNy of waste aeneAlted to ale degree I have Cetermirad woesconomlcally preedeabte and that I lava salOgod the prectleao1e method of treatment, storage , or dlspoul OUrrentry available to me wNch mWmlzee the present and lulurethreat to human nsalth and the environment ; OR, it I am a small quantity generator, I have made a good itlth effort to minlmlze my waste generation and Ielect the bestwaste mahaCernant method that is available to me and 0-at I can afford .Primed/Typed Nart) e 1 V j44up = Vg So`!T17 . Transporter I Acknowiedgement of Rece t of MaterialsPfIntep/ Typed NametPrint Type d N #sMoron , Day YearSigma re0a 19 . Transporter 2 Acknowledgement0flecelpt oI MaterialsaMonthSignature19 . Discrepancy indication Spacea1r720 . Faclity Owner or Oper ator : Ca rtiflcattan of, eceipt of hazardous materials COver s d by this manifest except as noted in Item 19Printed /Typed Namet:PA lame 17eyf (Ray , II•M ) Pievtau. .dhieee enƒeei wSignatureDayYea,/(1 r n Iqu.~OAIQINAL- RETURN TO GENERATOR11/07/ 01 WED 16 : 01 FAX 5414543279 Chem-Waste Arlington, ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812 .US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/17/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM03 .Profile Number : C04833CWM Tracking ID : 34756401Process : CHEMICAL FIXATIONTreatment Date : 11/19/99I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above -described waste was managed incompliance with all applicable laws, regulations , permits andlicenses on the date listed above .LYNN MLYRILLRECORDS MANAGERCertificate # 6835712/09/99Q00211/07 / 01 WED 16 : 01 FAX 5414543279 Chem - Waste Arlington, ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/17/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM03 .Profile Number : C04833CWM Tracking ID : 34756402Process : CHEMICAL FIXATIONTreatment Date : 11/19/99I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .LYNN MICRILLRECORDS MANAGERCertificate # 6835812/09/99lj 00311/07/01 WED 16 :01 FAX 5414543279 Chem-Waste Arlington, ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/10/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM04 .Profile Number : C04833CWM Tracking ID : 34739601Treatment Date : 11/16/99CWM Unit # : 1*0 thru 20*0I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .LYNN MtRILLRECORDS MANAGERCertificate # 9385711/07/01Cj 00411/07/01 WED 16 :02 FAX 5414543279 Chem-Waste Arlington . ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/15/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM05 .Profile Number : C04833CWM Tracking ID : 34747201Process : CHEMICAL FIXATIONTreatment Date : 11/17/99I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .LYNN MU(RILLRECORDS MANAGERCertificate # 6836212/09/99X100511/07 / 01 WED 16 : 02 FAX 5414543279 Chem - Waste Arlington . ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/09/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM06 .Profile Number : C04833CWM Tracking ID : 34731901Process : CHEMICAL FIXATIONTreatment Date : 11/10/99I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .LYNN MT RILLRECORDS MANAGERCertificate # 6724511/18/99Z00611/07 / 01 WED 16 : 03 FAX 5414543279 Chem - Waste Arlington, ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/10/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM07 .Profile Number :CWM Tracking ID :Treatment Date :CWM Unit # :C048333473940111/16/991*0 thru 10*0I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .0LYNN MtIRRILLRECORDS MANAGERCertificate # 9386011/07/011Q00711/07 / 01 WED 16 : 03 FAX 5414543279 Chem - Waste Arlington, ORCWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/09/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM08 .Profile Number : C04833CWM Tracking ID : 34731801Process : CHEMICAL FIXATIONTreatment Date : 11/10/99I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .0 aLYNN MUUILLRECORDS MANAGERCertificate # 7119002/09/001100811/07/01 WED 16 :03 FAX 5414543279 Chem-Waste Arlington,OR1J009CWM OF THE NORTHWESTFederal EPA ID : ORD08945235317629 CEDAR SPRINGS LANEARLINGTON, OR 97812US ARMY ENGINEERING DISTRICTATTN : MANIFEST SECTIONAKR000003228CEPOA-CO-FRGAMBELL AK 99742CONFIRMATION OF DESTRUCTIONChemical Waste Management, Inc . has received waste material from USARMY ENGINEERING DISTRICT on 11/09/99 as described on [StateManifest or Uniform] Hazardous Waste Manifest number GAM08 .Profile Number : C04833CWM Tracking ID : 34731802Process : CHEMICAL FIXATIONTreatment Date : 11/10/99I certify, on behalf of the above listed treatment facility, that tothe best of my knowledge, the above-described waste was managed incompliance with all applicable laws, regulations, permits andlicenses on the date listed above .LYNN MU$RILLRECORDS MANAGERCertificate # 7119102/09/001Appendix DDaily Quality Control ReportsEnvironmental Quality Control/Qualit~• :Assurance ReportIo41 ,ContractDACA3__e•37 -D 331 :,D .O . 0004UPC,Prcleet T :t-,Debris Rcrnov3i and Containerized Hazardous and Toxic Waste RemovalCCC R .rort99-0i1L)atc or Ti,nc PeriodT:n1;9Weather C .,Temp Lc,.,, _Wind Srcrd •__-nliLoc ; :icn and TcamGambcli, AlaskaContractorTemp HiConditions Pt :y cliyOil Spill Consultants, Inc .Quality; cncns._.t.CoPerformed This Date 'r- : rJe inspections . results, derc,encies ots•:r- .cy, and acv ;n 1Prepara : : f soo JiUched a,cUbsiinitial~,seooluct,ed check!ntFollow-U :.WasYes 0 NoField Sarp ; , s ., ., rci .• ".gHasfic : :_ . .Type cf x, :Yes C1 Not%le :ho . Ma ::,x Ouar .tty of sam ;. ; _sResuiaNoneHave Don C , . :y C :-' ves been achievedlN,AYesOHave Samples Geen Collected for Laboratory Analysis?EPA Test blcthod.T,Aatrx'q; .. 7f TestCcc-'.iy ::f SamplesSC t .p t ; es a :.d r,rsa :•n ccHave req_.,ea -. .achieved) lUAHave a,pr ..p : Y-, _ . .`'aNd :d: •y tuts bee' OrJEr^ .7 _ 'a :r,x SrrACS, r•',E!hO dE!hOd blanks, 5U r rajat. .:s ence,c ;•_ .s _"CS et .'Have OA a-d CC _ : ics been cc ::ected in the spec.1e d quantity? N/AYesoYesDYasDHave sa::•- :__`YasDr:y!JNoOYesand pac`'N :ANoDNODNODNotHealth andWorker prxe,. . : 's..:cdLevel A 0 Level 8 l7 Level C I] Level D e N/AQWas any v:J :-. . . . . . . _- .uct^J vdhin a ccn'rcd scacclYes Q Noe:;.`Was an?v.cr} : c _ crd ct d vr .in a^ r^_3 (;c :e•-. .-c ; to be imredlate!y dangerous to life and re :Ith'rYesQNoeWere apprc .c : Jc-- a^ :ail o . p;r_ec .:res used cn wcrkers and equipment as requ,red7Yes 0 NoeSafety Cor : crs : -' de ar y nf:actions W approved safety plan, and include instr,;ctions from Governmen t personnel. Specify corrective action taken-)The COC receive d a detailed briefing on terrain hazards and instructions in ATV operation .Wont Acti • :t;P4dcnned This DateReference•C • . cVi Sr r :Locale S,teu~Ate. :, .Locatorae .' rr•eJ or,n ;issanca Jf sites 2,3,8 10 12, 13CARalC .:an.t.tyContractorsurvey of sites onlyMobil iza t ._r N :,C C .__7r Unpacked vehicles from conr. ex . Started soup of fcld cflceStarted sutsistence arrangements . Made arrangemert ; nor, :.°', cc .n pleteOAR ofr,,;e and phones .Manpower and Equipmentebor ClassificationProject ktt : :3gcrCAC System MnrJCUCrSuperintc _Archeolc y.stOperatorLaborersNumberMan Hours1111I ;Equipment Type4 wheelerCJt 4CC lCJCCr1.•~cNed1 . • .,P . ; 'r. . ;,Number21211Hours Used223400Total Hours : 29'vial Hcr :rs .trlstr,Ctin .ts::(jcr -‚re Goverament to the Contractor (Include narnes . reactionssVerbaland rcrnn :'s j0 Written 0NoneWork Progress t< c : : ere any Contractor caused delays or potential finding of fact?Are zero any Government caused ways or potential finding of fact?Are !'ere any u-.fcreseeable or weather related delays?Yes ONo eYes 0No eYes QNo eRemarks (Include ?.' t visitors to protect a A miscellaneous remarks pertnent to work )The three connexes containing Philip's tools, materials, equipment were not cffloaded with the other containers .Northland (the shipper) was contacted and verified that they were on the barge and had neglected to offload them.Arran en,e : its were made to have the connexes delivered by the ne> t available barge .I certify thZt t ; 1.c : . : . , _' ; :s C_-1 . !_i e and cc : reel and that all rr, aterals and equiprrcnt used p.rforrned anal tests conducted during this period were In strictCompliance .s 2 - . . . _c ; p.Jr•s and sredfc3tions except as noted aboveQuality Control r. . . r . : ; .r Signaturet/rilDate.. rEnlironmcntal Quality Control;Quality Assurnncc Report(r 4!5 .1- : : :Continuation Slice[Oovernn 'nt G . 3I t, &ss~,rancc Comments., ., ,:ConcurYcNo OJ c~ rJ S i ; ~% TOCM SIgnaturcA 2Supcr. :-Cr's Initial DateEnvironmental Quality Control/Quality Assurance Report(E]t 4I3-l. titContract Number ! Delivery Order Nianber :UPC/Project Ties:DACABS-I1.a-0O1010.0 . 0004Debris Removal and Contalnertzed Hazardous and Toxic Waste RemovalCQC Report NumberDate or Time PeriodLocation and Team1 .00271719 !Garnball, AlaskaContractorHeather ConditionsTemp Low 40 Temp HIWind Speed15 knotsConditions60Ptycldy00 spill Consultants, Inc.Quality Control Inspections Performed This Date (kldude inspections, results, deficiencies observed , and Corrective action.)Preparabry 0 s.o attached anctaRInitial 0 a.m arched checklistFollow-Up 0Was the deficiency tracking list updated this dateYes DField Sampling and TestingHas field testing beenperformedthisType of oat Method/Matrix Quantity ofdate?Yessamples Results0NoNoNoneH ave Data Quality Objecti ves been achieved? N/AY.O NoOY.sO MOMHave Samples Been Collected for Laboratory Analysis?Type of Test EPA Test Method/AAatrix Quantity of SamplesNoneHave required amount of OC trip darks and rinsates been achieved?NIAYs0MOOHave appropriate OC laboratory tab been ordered ? (matrix spikes. me t od blanks . surrogates , reference standards, .)etcYsONotHave QA and OC samples been collected in the specified quantity ?WAY.sp NoOHave samples bee n property labeled and packaged ?WAY.5D MOOHealth and SafetyWorker protection levels this date : Level A O Level 8 O Level C O Level 0 0 WADWas any work activity conducted within a confined space ?YesDMOOWas "work activity conducted within an area determined to be immedo sly dangerous to life and health ?Yes0NoOWere approved decontamination procedures used on workers and equipment as required ?YsOMoOSafety Cormrera : (Include any infractions of approved safety plan, and include instructions from Government personnel . Speci fy corrective action taken.)_Emergency communications procedures were covered at the safety meeting . The radios were tested for range and blindspots. Available on-island emergency services were reviewed as well as the posted location of emergency contactnumbers.Work Activities Performed This DateReference (NAS D S/Tech Spec S)Mobilization (HAS D 0011)Activity&LocationQuantityContractorSetup of the field office for contractor and OAR, Serviced vehicles and equipmentManpower and EquipmentLaborC1asslkaeonPr>)ect tote perCOC System kAansgerSuperin .4.ntArcheologistOperbrLaborersNumberManHours1110110EquipmentTypeNumber Hours Used2201320114 wheelerCat 42e loaderArgoPlPickup kup10Total Hours :1300Total Hours : 24tnstruWons Given by the Government to the Contractor (Include names. reactions , and remarks.)OAR not an siteVerbal O Written DWork Progress Are there any Contractor caused delays or POW" fir" of fact?Are two any Government caused delays or potential finding 01 fact?Are there any unforeseeable or weather related delays?Yes 0Yes OYs 0Remarks (tr dude any visitor b project and miscellaneous remarks pertinent to work.)Started coordinated with Village of Gambell for possible location for contractor ' s operating area .I certify that the above report is complete and Carrot ! and that all materials and equipment used . work performed and tests conducted during this period were in strictcompliance with the contract plans and specifcatierns except as . oted above .QualityControlManager3ignatursI/Dab7NoNoNoEnvironmental Quality Controt/Quality Assurance Report(EP 415- 1 .302)Continuation SheetGovernment Duality Assuranc e CommentsConcurs with the OCAdditional comments or exceptionsreport?Yesi/o,tee Nor a S/ -tFOAR signature 47ZIa-,-ka,14f- Oat .7~ss7Supervisor' s Initial Date0Environmental Quality Control/Quality Assurance Report(FR 41S-l-)02)UPCJProject Title:Contract Number / Deliwxy Order Number :D.brrb Removal and Contaln .rtzsd Hazardous and Toxic Waste RemovalDACASS - 97-O-00101D.0 . 0004COC Report NumberDate or Time PeriodLocation and Team99.003718199Gam bell . AlaskaWeir ConditionsTemp Low 40_10 krX isWind SpeedContractorTamp MConditions6oPtlv cidyOil Spill Consultants, Inc.Quality Control Inspections Performed This Data (Include inspections . results, deficiencies observed, and corrective action)Preparatory 0 ... .uadnd eh .cklbt.ckaatInitial0 ..o anachad chFollow-Up0yea 0 NoWas the deficiency tracking list updated this dateField Sampling and TestingHas field testing been performed fl s date ?Type of testYes0Metuod/Matrix Quantity of samplesNoResultsNoneN/AYssO MooHave Data Quality Objectives been achieved?BeanCollectedforLaboratoryAnalysis?YssONoƒHave SamplesType of Test EPA Test MethodAItatix Quantity of SamplesNone?WAYesONo0Have required amount of QC trip blanks and rinsates been achieved.)YesOMOOHave appropriate OC laboratory tests been ordered ? ( matrix spikes, method blanks . surrogates . reference standards, etcWAYesD1400Have QA and QC samples been collected in the specified quantity ?N/AYssO No0Have samples been properly labeled and packaged ?Health and safetyLevelA0LevelB0LevelC0 Level 0 ƒ wA0Worker protectionon levels this daft:Yes 0 MOOWas any work activity conducted wilts a confined space ?Yes 0 1400Was any work activity conducted wi8in an area determined b be immediately dangerous to life and health ?Yes 0 Moowere approved decontamination procedures used on workers and equipment as required ?action taken.)Safety Comments: (hdude any inlractians of approved safety plan. and include instructions from Government personnel . Specify correctiveThe causes , effects , and preventative measures required to counter Hypothermia were discussed at the mornings safetymeeting . Specific items addressed included the need to stay dry and the effect of wind on body heat loss . Appropriatetypes of clothing for different conditions were outlined .Work Activities Pedonned This OafsReference (NAS 1) S/Tech Spec 9)Mobilization: Mobilization (NAS ID 0007 )QuantityActivity & LocationEquipment inspection and maintenance was performed on delivered equipmentField office and Communications systems setup were completed today.Manpower and EquipmentLaborCiassUlcathonManHoursType4 wheelerCat 420 loaderArgoNodwellPickup111010110Total Hours:30ArcheologistOper80%EquipmentNumberPrat ManagerCQC sysiern fWSuperimmendentContractorNumber Hours Used22003261010LaborersTotal Hours : 29Instructions Given by the Government to the Contractor (kclude names . reactions. and remarks .)OAR not on siteVerbal 0 wrttan 0Yes 0Yes 0Work Progress Are there any Contador caused delays or potential /fading of fart?Are were any Government caused delays or potential finding of fact?Are them any untoreseeabie or weather related delays?Yes 0NoNoNoRemarks (include any vision o project and miscellaneous remarks pertinent to work .)In a survey of the access roads throughout the site it was noted that while the roads on the east and west sides ofTroutman Lake were very good , all routes through the village were over very loose gravel . It was also noted that thegravel conditions at the North Beach made the location unsuitable for contractor ' s primary operating area as proposed inthe work plan . An alternate location will have to be identified.1Environmental Quality Control/Quality Assurance Report .(1:R 41S-1-M)Continuation Sheet' certify that the above report is complete and coned and that aN materials and equipment used . wont performed and tests conducted during )his period were in strictpliance with the contract plans and spealicatlons exact as noted above .Quality Control Manager signature--_ Z&4Government Quality Assurance CommentsConcurs With the QCAdditional comments or exepbonsreport?aj,~eOAR Signature-,~~"-003Nc r7yesoNOQ~~ 9t -s-2Su perv Isors inltla1Date-Environmental Quality Control/Quality Assurance Report(ER 41 S W- ) n)Contract Number / Delivery Order Number 'UPC/Prgset TitleDACASS-97-0-001t)ID.O . 0004Debris Removal and Containerized Hazardous and Toxic Waste RemovalCQC Report NumberOat. or T)me PeriodLocation and Team99-004_719/99Gambefi , AlaskaWeather ConditionsTemp Low 38Wind SpeedContractorTemp HiConditions33Ptv cldvOil Split Consultants, inc.OuaOly Control Inspections Performed This Date ( include inspections . results . deficiencies observed . and corrective action )Preparatory 0 No leached checklistin"Follow-Up0 eve naach.d checkkt0Was the deficiency tracking list upd ated this dateField Sampling and TestingHas field testing been perlonned this date ?Type d testYea 0NoYes D NoMethodl?MtiixQuantity of SamplesResultsNoneHave Data Quality Objectives bee n achieved?WAYesoMooHove Samples Been Collected forLaboratoryAnalysis?Y .s0 MooTyped Test EPA Test Methodl lie ix Quantity of SamplesNoneHave required amount of QC trip blanks and riroates been achieved?NIAYeiDNODHave appropriate QC laboratory lest been ordered ? (matrix spikes . method blanks. surrogates , reference standards .eke)YiDMooHave OA and QC samples been collected in the specified quantity?N/AYeeDMooHave samples been prop" labeled and packaged ?NIAY0110 MooHealth and SafelyWorker prclection levels this dab : Level A D Level B 0 Level C 0 Level 0 0 WADWas any work activity conducted within a confined space ?Yea0MooWas any work activity conducted within an area determined to be immediately dangerous to fife and health ?Yes0NoDWere approved decontamination procedures used on workers and equipment as required ?Yes0MooSally Comments : ( Include any infractions of approved safety pan . and include inspections from Government person ne . Specify corrective action taken.)At the safety meeting the techniques for safe operation of ATVs over difficult terrain was discussed . Specific areasaddressed included operation on slopes, rocky terrain, and soft mud . Later in the day, hands on instruction with fourwheelers and Argos was provided to the CQC who was not and experienced ATV operator .Safety meeting covered : AN OP ERAT I ONWork Activities Performed This DateReference (HAS ID ?/Tech Spec 9)Activity&LocationQuantityContractorMobilization (NAS ID 0007 )khvestigated the local availability of rental equipment,Coordinated with shipper on delivery of missing tool/suppy containers80%Staging Area Setup ( NAS ID 0009)Started reviewing potential alternate staging areas5%Manpower and EquipmentLaborEquipmentClassUcation Number ManHours TypeProject M.n.ger4wheelerCQC System Manager 1 9 .5 Cat 426 loaderSuperintendent19.5ArgoArcheologistNumber21211NodweltOperator19 .5 PickupLaborersTotal Hours :28.5Instructions Given by the Government to the Contractor (Include names , reactions . and remarks .)Hours Used193400Total Hours :26Verbal 0 Written 0OAR NOT ON SITEWork Progress Are there any Contractor caused delays or poor" findingoffact?YesDNoAre there any Government aused delays or potential finding d tact? Yea 0 No 19Are there any unforeseeable or weather related delays?Yes 0 NoRemarks (Ynduds any visitors to project and miscellaneous remarks pertinent to work)certiy tut the above report is complete and coo,ect andthat all materials and equipment used. work performed and tests conducted during this period were in strictompliance with the contract plans and specifications except es noted above-Quality Control Manager Signature ry~ ' ',r-'/ZA-Oat,IEnvironmental Quality Control/Quality Assurance Report(ER 4 15-1 .302)Continuation SheetGovsmment Quality Assurance CommentsConcurswithAdditional comments or e xoeptions.theQCreport'syesOAR NOT ON SITEQAR Signature.-/.c,JDate ,- Supervisor's Initial_DateNoEnvironmental Quality Control/Quality Assurance Report(ER 4111-)0:(Contract Number / Delivery Order NumberDACASS-97-0-0010ID. O . 0004COC Report NumberDate or Time Period7/1019999 .005Weather ConditionsSSTamp Low 3f Temp HI$ -15 oats ConditionsSunnyWind SpeedUPC/Prolect Title :Debris Removal and Containerized Hazardous and Toxic Waste RemovalLocation and TeamGambell, AlaskaContractorOil Spill Consultants, Inc.Quality Control Inspections Performed This Date (Include inspections . results. deficiencies observed . and corrective action )Q see as dl .d ch .cktlatPreparatoryInitial 0 see attacMd checkfatFollow-up 0yes 0Was the deficiency tracking list updated this dateField Sampling and TestingHas field testingType of testNobeen performed this date? YesMethod/Matnx Quantity of samples Results0NoN/A1400NoneHave Data Quality Objectives been ac hie ved7Have Samples Been Collected for Laboratory Analysis?Type of Test EPA TestYes(YesO NoƒMethod/MatrixQuantity of SamplesNoneWAYssONoDHave required amount of QC tnp blanks and rinsates been achieved 'YesOmooHave appropriate QC laboratory tests been ordered 7 (matrix spikes . method blanks. surrogates . reference standards . etc .)Have QA and QC samples been collected in the specified quantity?N/AYesDNo0WAYesD No0Hare samples been property labeled and packaged?Health and SafetyWorker protection levels this date : Level A Q Level 8 0 Level C Q Level D 0 N/AQYesQNoOWas any work activity conducted within a confined space ?Yes 0 mooWas any work activity conducted within an area determined to be immediately dangerous to life and health?Were approved decontamination procedures used on workers and equipment as required )Yes0MOOSafety Commen ts : (Include any infractions of approved safety plan . and include instructions from Government personnel. Specify corrective action taken )Safety meeting covered: WILD LFE HAZARDSWork Activities Performed This DataRettxence (HAS ID S(Tecfl Spec a)Locate waste sites (HAS ID 0011)Manpower and EquipmentLaborClassificationProject ManagerCOC System ManagerSupwwftr dartArcheologistOperatorActivity&LocationQuantityContractor40%A reconnaissance was conducted of Site 10 (the trail system) and Site 4 (the mountain top)The contaminated soil and most items of HTW and debris described in the delivery orderwere identifiedNumber111EquipmentTypeNumber4wheeler210Cat426loader110Argo2ManHours10NodwellPickupHours Used200101100LaborersTotal Hours 30Total HoursI aOvdions Given by the Government to the Contractor (Include names , reactions . and remarks .)OAR not on siteWodt Progress Are there any Contractor caused delays or potential finding of fact ?Are lbere any Government caused delays or potential finding of fact?Are there any unforeseeable or weather related delays?Verbal300 Written 0Yes 0NoYes 0Yes 0NoNoRemarks (Include any visitors to project and miscellaneous remarks pertinent to work .)During the reconnaissance of Site 10 and Area 4 with four wheeler and Argo it was noted that the light-duty improvedroads shown on the contract drawings as the "Air Force Trail" and the " Army Trail " were little more than commonlytraveled tracks in the tundra . The boulder field at the top of the mountain (Site 4) made many areas impossible to reachby ATV .1 certify that the above report is complete and corned and that all materials and equipment used . work performed and tests conducted during this period were in strictcompliance with the contract plans and sexcept rhotey above/Quality Control Manager Signature:" c ~~Date iIEnvironmental Quality CoatroUQuality Assurance Report(ER 415-1 -3021Continuation SheetGovernment Ouaiky Assurance CommentsreportsConcurs , mtt eu OCAdditional comments or excepbonsYes$NoOAR NOT ON SITEDat.799-0052OAR Signature ASupervisors InMs1Oat.0Environmental Quality Control/Quality Assurance ReportiER 4151-RC)Contract Number I Delivery Order Number UPC /Prgec1 TideDACA$S -97-0-00101O .O . 0004 Debra Removal and Contaln .rtzed Hazardous and Toxic Waste Removalr :QC Report Number Date or Time Period Location and Team-0067111199Gambell,Alaska.athKConditionsTemp Low 40 _Temp HI51Wind SpeedCalm knMConditionsContractorCloudyOil Spill Consultants, Inc .Quality Control Inspections Perform ed This Date (k)Uude inspections, results . defic,enaes observed. and corrective action)Preparatory 0 iwe attached checklistInitial 0 see cached cMCklistFollow-Up 0NO INSPECTIONS TODAYupdatedthisWas the deficiency tracking listdateYes0NoField Sampling and TestingHas field testing been performed this date ?Type of testYes 0 NoM ethod / titatnxQuantity of samples ResultsNoneHave Data Quality Objectives been achieved?Have Samples Been Collected forType of TestN/ALaboratoryEPA Test Method/AfatrixYesOAnalysis?YesOQuantity of SamplesMOOMooNoneHave required amount of QC trip blanks and rinsates been achieved?N/AYesOMooHave appropriate QC laboratory tests been ordered ? (matrix spikes , method blanks . surrogates . reference standards . etc .)YesOMOOHave QA and OC samples been collected in the specified quantity ?N/AYesONo0Have samples been property labeled and packaged?N/AYesO MooHealth and SafetyWorker protecton levels this dateLevel A 0 Level a 0 Level C 0 Level D 0 N/AOWas any work activity conducted within a confined space ?Yes0NoCWas any work activity conducted within an area determined 10 be immediately dangerous to life and health ?Yes0MOOWere approved decontamination procedures used on workers and equipment as required ?Yes0MooSafety Comments : ( Include any infractions of approved safety plan, and include instructions from Government personnel Specify corrective action taken )e safety meeting was used to cover the types of PPE that would be used on the project to deal with the variouspotentially hazardous conditions that might be encountered . Methods of controlling the spread of contamination werealso discussed .Work Activities Performed This DateReference (NAS ID 1t/Tech Spec a) Activity & Location QuantityContractorMobilization (NAS 10 0007) Continued investigated the local availability of rental equipment80%Continued to coordinated with shipper on delivery of missing too(/supply containersManpower and EquipmentLaborClassificationNumberEquipmentTypeManHoursProtect ManagerCOC system ManagerSuperintendent1144ArcheologistOperatorLaborers14Total Hours '12NumberHours used4 wheeler28Cat 426 loaderArgo1200Nodwell10Pickup10Total HoursInstructions Given by the Government to the Contractor (Include names reactions, and remarks)8Verbal 0 Written 0OAR NOT ON SITEWork Progress Are there any Contractor caused delays or potential finding of fact'Are there any Government caused delays or potential finding of fact'Are there any unforeseeable or weather related delays?Yes 0Yes 0Yes 0NoNoNoRemarks (k)dude any visitors to project and miscellaneous remarks pertinent to work .)I certify that the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this period were in strictipliance with the contract plans and specifications except as /Rtted aboveQuality Control Manager SignatureIEnvironmental Quality Control/Quality Assurance ReportIER 415.1 .302)Continuation SheetGovernment Quality Assurance Comments^.oncurswithXmonal comments or exseptlonstheQCreportsYes'RNoOAR NOT ON SITEQAR Signature ALO yL_""_""'wwe 7- 1 5 ?799-0067Supervisors Initial oat .0Environmental Quality Control/Quality Assurance Report(ER 41t-I-O )Contract Number / Delivery Order NumberDACAU-97 .O-0 010/D. O . 0004UPC/Project TreeDebris Removal and Containerized Hazardous and Toxic Waste RemovalDate or Time Period7112/99COC RepoR Number9„007Location and TamGambol! , AlaskaContractor50Foooy a .m . Sunny Porn Oil split Consultants, Inc.Weather ConditionsTamp Low 40__ Temp HIWind Speed Calm ConditionsQuality Control Inspections Performed This Date (k+dude inspections . results . deficiencies observed . and corrective action )Preparatory 0 s .. amch.d ChecklistInitial 0 see sRached ch.ckastFollow-Up 0Yes 0Was the deficiency tracking list updated this dateField Sampling and TestingHas field testing been performed this date ?Type of test Mettwd / MatnxNoYes 0 NoQuantity of samples ResultsNoneYesoHave Data Quality Objectives been achieved ? N/AHave Samples Been Collect ed for Laboratory Analysis?Type of Test EPA Test Method/MatrixQuantity of SamplesNooY .sD NomNoneHave required amount of QC trip blanks and rinsates been achieved?N/AYesOetcHave appropriate QC laboratory tests been ordered 7 ( matrix spokes . method blanks , surrogates . reference standards .N/AYesDHave QA and OC samples been collected in the specified quantity?WAHave samples been property labeled and packaged ?MOOiY .sO NODNo0Ys0 MooHealth and SafetyLevel A 0 Level 8 0 Level C 0 Level 0 Cg MIA[ :)Worker protectoon levels this date:Yes0MooWas any work activity conducted within a confined space ?Yes0No0Was any work activity conducted within an area determined to be immediately dangerous to life and healthWere approved decontamination procedures used on workers and equipment asrequired?Ys0MOOSafety Comments : ( kldude any infractions of approved safety plan . and include instructions from Government personnel Specify corrective action taken )Safe work practices around operating equipment was discussed at the morning safety meeting . Specifics included theuse of one and only one spotter, correct spotter hand signals, and the need for personnel on foot to be cognizant ofequipment movement areas was also addressed .Work Activities Performed This DateReference (NAS 10 a/Tech Spec S)Setup Staging Area (NAS ID 0009)Manpower and EquipmentLaborCtassIk anonProject ManagerActivity&LocationQuantityReceived approval for use of area south of runway for staging areaRented Cat 966 loader from city Moved 9 empty connexes to staging areaNumbercoo System Manager1SuperintendentArcheologist1OperatorLaborers1ManHours101010Total HoursEquipmentType4 wheelerCat 426 loaderArgoNodwellPickupCat 966 LoaderContractor20%Number2Hours used2010214010730Total HoursInstructions Given by the Government to the Contractor ( Include names , reactions , and remarks )Verbal 031Written 0QAR NOT ON SITEYes 0Wok Progress Are there any Contractor caused delays or potential finding of fact?Are there any Government caused delays or potential finding of fact?Are there any unforeseeable or weather related delays?Yes 0Yes 0NoNoNoRemarks ( Include any visitors to project and miscellaneous remarks pertinent to work .)Persons unknown broke into Argos and siphoned gas from four wheelers during the night . No serious damage . Reportedproblem to Bert, the Village Liaison contractor . Moved two empty connexes to the lodge to use as garages .COC and Superintendent noted VASIs at both ends of the runway, as well as AWOS and other navaids . These navaidsare in debris, removal Site 8 . Contacted FAA office in Nome for utility locates underground electrical lines providingpower to naaids . Received faxed sketch (attached .)1Environmental Quality Control/Quality Assurance Report(ER 415.1-302)Continuation Sheett certify that the above report i s complete and correct and Meat all materials and equipment used , work performed and tests conducted during this period were in strictcompliance win the contract plans and specifications except as notedGovernment Quality Assurance CommentsConcurs with we OC report''Additional comments or exceptions .YesWio DQAR NOT ON SITEOAR Signatu& Do, 7-15 - 79Supervisors InitialDoeCUf. .CILiLa7I0\. N 5 %ftU PSt annLaLCLos~1JT,--) D-DP\`"s(, -~T0Environmental Quality Control/Quality Assurance Report,ER 411-1-MContract Number / Delivery Order Num berUPC/Pro ect TitleDACA85-97-0-001010.0. 0004Debris Removal and Contairwrtzod Hazardous and Toxic Waste RemovalCOC Report NumberDate or Time PeriodLocation and Team99-ooa.9"V7- r 3Gam bell , AlaskaWeather ConditionsTamp Low39TempitContractor48Wind speed Calm ConditionsFoocv a m Sunny om . Showers ever .ng 041 Spill Consultants, Inc .Quality Control Inspections Performed This Date ( Include inspections . results , defic iencies observed. and corrective action)Preparatory 0 .. * aeacta. d ch.cUistInitial0 see amcMd checklistFollow-Up 0NO INSPECTIONS TODAYWas the deficiency tracking list updated this dateField Sampling and TestingHas field testing been performed this date'Type d testYes 0 No tMYes 0 NoMethod/MatrixQuantity oil samplesResultsNoneHave Data Quality Otiectives been actneved'N/AYeso NodHave Samples Been Collected for Laboratory Analysis?Type of Test EPA TestYesoMethod /MatnxNoƒQuantity of SamplesNoneHave required amount of OC trip blanks and nnsates been achieved ?N/AYesoNodHave appropriate OC laboratory tests been ordered 7 (matrix spikes, method blanks , surrogates . reference standards . etc l Yeso NodHave OA and QC samples been collected in the specified quantity?NIAYeso1400Have samples been properly labeled and packaged?N/AYesoNodHealth and SafetyWorker protection levels this date .Level A O Level 8 0 Level C O Level D ƒ N/AOWas arty work activity conducted within a confined space 'Yes0NodWas any work activity conducted within an area determined to be immediately dangerous to life and health?Yes 0 NodWere approved decontamination procedures used on workers and equipment as required?Yes0NodSe" Comments ( knctude any infractions of approved safety plan, and include instructions from Government personnel Specify corective action taken)The safety meeting addressed the definition of "Level D" PPE . The needed upgrades discussed included hearingprotection for activities where the noise reached a level that would interfere with normal conversation, full face shieldsduring use of cutoff saws and drum washing , and the various types of gloves that Would be used for different tasks .Work Activities Performed This DateReference (NASIDs/TechSpecs)ActivitydLocationQuantityContractorMobilization (NAS ID 0007) Kelly Ryan barges with missing tool connexes arrived late in the eavening Mobilization 100%Three containers offloaded and moved to the south staging areaSetup Staging Area (NAS ID 0 (09) moved 8 additional empty connexes from the north landing site to south Setup now 60% completeStaging area The Cat 980 from the barge was used to moved the previcusy deliveredtool connex from the north landing area to south staging areaManpower and EquipmentLaborEquipmentClassifcetion Number ManHoursTypeProtect Manager4 wheelerCOC System Manager113 Cat 426 loaderSuperintendent115ArgoArcheologistNodwellOperator115PickupLaborersCat966LoaderTotal Hours .43Number212111Hours Used3004007Total Hoursinstructions Given by the Government to the Contractor (Include names . reactions . and remarks)41Verbal 0 Written 0QAR NOT ON SITEWork Progress Are there any Contractor caused decays or potential finding of fact?Are there any Government caused delays or potential finding of fact'Are there any unforeseeable or weather related delays'Yes 0Yes 0Yes 0NoNoNoRemarks ( include any visitors to protect and miscellaneous remarks pertinent to work)The Cat 980 Loader from barge used to move previously delivered tool connex from north beach to operating area atsouth got stuck in the soft gravel in town . The CAT 966 was used to pull the loaded machine out . The incidentunderscores the difficulty of travel and equipment operating in and around the village .1Environmental Quality Cuatrol/ Ouslity Assurance Report(ER 415 .1 7O2tContinuation SheetI certty that the above report is complete and correct and that all matenals and equa merit ruedd wont performed and tests conducted dunng this period were ~n strictcompliance with the contrail plans and specifications except as noted aboveOuallty Control Manager SignatureJ~^ rDate2z 1~ J 1Government Duality Assurance CommentsConcurs with VV DCreport'sYesrtoAdditional comments or exceptionsOAR NOT ON SITEDAR Signature99-()OR- 4z~~kDataS "1 Sup .rvlsor's Initial DateCEnvironmental Quality CoetrollQuality Assurance ReportiER 41 "- 302)Contract Number / Delnvery Order Number 'UPCIPrgect TitleDACASS-974).OO10/D .O. 0004Debris Removal and Contalnertzed Hazardous and Toxic Waste RemovalCOC Report NumberDate or Time Period1 9-0097114/99Heather ConditionsTemp Low 43_Temp HIWind Speed I ConditionsLocation and TeamGarnbell , AlaskaContractor48Rain a m . Clear w/foo p mOil Spill Consultants, Inc.Quality Control Inspections Performed This Date ( include inspections . results deficiencies observed . and corrective action )Preparatory D see attached checklistfrutial 0 see aaeched checklistFollow-Up 0Was the deficiency tracking list updated this dateField Sampling and TestingHas field testing been performed this date?Type of testYes D No aYes C] NoMethod/Mat nxQuantity of sampleswResultsNoneHave Data Qua lity objectives been achieved'YesO No0N/AHave Samples Been Collected forLaboratoryType of Test EPA Test MethodUaianxAnalysis?YesQQuantity of SamplesNowNoneHave required amount of OC Onp blanks and nnsates been achieved ?NIAYOSO160(:]Have appropriate QC laboratory tests been ordered 7 (matrix spikes . method blanks. surrogates . reference standards . etc .)Y.Q NODHave QA and QC samples been collected in the specified quantity ?N/AYesOMooHave samples been properly labeled and packaged ?WAYeiQNo0Health and SafetyWorker protection levels this date .Level A 0 Level 8 D Level C D Level D a N/AQWas any work activity conducted within a confined space ?Yes 0 NowWas any work activity conducted within an area determined to be immediately dangerous to life and health? Yes 0 NowWere approved decontamination procedures used on workers and equipment as requredy Yes 0 NooSafety Comments . (Include any infractions of approved safety plan . and Include i nssn.ctions from Government personnel . Specify corrective action taken)The safety meeting covered the requirements for level D PPE . Hard hats , steel-toe boots , and safety glasses werenandatory when ever any persons was "on the clock ." The only exceptions were when personnel were on break indesignated break areas . Helmets and eye protection were established as mandatory while using ATVs . The prohibitionagainst carrying passengers on four wheelers was also emphasized .Wort Activities Performed This DateReference (HAS ID A/Tecn Spec e)Activity&LocationQuantitySetup Staging Area (NAS ID 0009) Started unpacking tools and setting up shop in the staging areaContractor80% CompleteManpower and EquipmentLaborEquipmentClassicationNumberManHoursTypeNumberHoursUsedProjectManager4wheeler48CQCSystemManager111Cat426loader10Superintendent111Argo26ArcheologistNodwell10Operator111Pickup10Laborers38Cat966Loader12TotalHours41instructions Given by the Government to the Contractor ( Include names . reactions . and remarks)OAR not on siteTotalHours41Verbal 0 Written 0Work Progress Are there any Contractor caused delays or potential finding of fact?Are there any Government caused delays or potential finding of fact'Are there any unforeseeable or weather related delays?Yes DYes 0Yes 0NoNoNo aRemarks ( Include arty visitors to project and miscellaneous remarks pertinent to worn)Three laborers from the local- hire crew put on today and two additional operator/laborers arrived late in the dayI certify that the above report is complete and correct and flat Bit matenals and equipment used , work performed and tests conducted during this period were in strictompliance with the contract plans and specifications except as rioted above3uailty Control Manager Signatur e-ay-Date 1L ~11Environmental Quality Cototrol /Quality Assurance Report(ER 4111-702)Continuation SheetGovemm.nt Quality Assurance CommentsYes4TNo 0Concurs with the QC report?Additional comments or exeptions .OAR NOT ON SITEQAR SignatureZL _,.~/1YSGJ~ Dat.7 -4 y Supervisor ' s Initial DateOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate :1999Time :~-~L! /Briefing Location :Activities Planned :6-k" '/.Briefer :Topic :~' tTopic :Briefer :Topic :TopicTopic :AttendeesZQCOh ~,r~ ~Site Health^and Safety Officer :j%}rDate : ~T1999Environmental Quality Control/Quality Assurance ReportIER 411.1 .'k-1Contract Number / Delivery Order Number :DACA85-97.O-001010.0 . 0004CQC Report Number010UPG'Prolect Title:Dat e or Time PeriodDebris Removal and Containerized Hazardous and Toxic Waste RemovalLocation and Team7115199low Conditions. wnp Low46Gambell , AlaskaContractorTamp HIWind Speed Calm Conditions48Cloudy a m Rain a m -Clear ;/Tog o mOil Spill Consultants, Inc .Q a1ty Control Inspections Performed This Date (Include inspections, results . deficiencies observed , and corrective action .)Preparatory0 se. ,ttich*d ch.CktbtDebris Collection (NAS I .d . a 0013 ) Inspection e xclud e d weighing debrisIn"0 see Attached checklistFollow-Up 0Was the deficiency tracking list updated thi s dateField Sampling and TestingHas held testing beenType of testYes (7 Noperformedthisdate?YesMethod.Matrix Quantity of samples ResultsQNoNO FIELD TESTING TODAYHave Data Quality Objectives been achi eved ?N/AYp0 No0Have Samples Been Collected for Laboratory Analysts?YqQ NoƒType of Test EPA Test MethodMatrix Quantity of SamplesNO SAMPLING TODAYHare required amount of OC trip blanks and rinsates been achieved? N/AYaD NoDHave appropriate QC laboratory tests been ordered 7 (matrix spikes, method blanks, surrogates, reference standards, etc)YesQ NoDHare QA and OC samples been collected in the specified quantity?N/AYeeD NoDHare samples been property labeled and packaged?WAYesO mooHealth and safetyWorker protection levels this date:Level A Q Level B Q Level C Q Level D ƒ NIAQWas "waft activity conducted within a confined space?Yes 0 NoƒWas anywork activity conducted within an area determined to be immediately dangerous to life and health? Yes 0 NoƒWere approved decontamination procedures used on workers and equipment as required? Yes 0NoƒSelety Comments : (Include any infractions of approved safety plan, and include instructions from Government personnel. Specify corrective action taker.)The safety meeting stressed four wheeler and Argo safety . The correct PPE for these vehicles as well as techniques foroperating them safely was discussed .or in the day, an overview of the hazards to travel posed by terrain and local traffic was given to personnel whoarrived at the site that day . The hazards peculiar to the diffent areas, village, beach, tundra , and mountain top werediscussed in detail .aM SAFETY COMMENTS :04440Vfu .5k rc r e -r-C'/' o c o )S T7"Ig- .r~TQ~E _IPryors Cc %, i .E:nsironnicntal Quality Control/Quality Assurance Report(ER 41 5 -1-302)Continuation SheetWork Activities Performed This DateReference (NAS ID f,Tech Spec I) Activity S LocationQuantitySetup Staging Area(NAS 10 0009) Continued to unpack connexes and set upwork shop and break areastio% set upLocate Waste Siles(NAS ID 0011) Toured Sites 10 (the trail system and tundra)and Site 4 . (the mountain top) with the CZARCCC . Archeologst . and Contractor's Project Manager50%Manpower and EquipmentLaborEquipmentClasslfkaUon Number ManHours TypeProtectManager144wheelerCOC System Manager 1 1 Cat 428 loaderSuperintendent115ArgoArcheologist14Nodwetloperator226PickupLaborers444Cat968LoaderT otal Hours :106ContractorNumber4Hours Used5E120201I10I270Total Hours:Instructions Given by the Government to the Contractor ( Include names, reactions , and remarks.)none.Verbal 0 Wrfnen OWork Progress Are there any Contractor caused delays or potential finding of fact?Are there any Government caused delays or potential finding of fact-)Are there any unforeseeable or weather related delays?aYes ONoYes ONo aNo aYes ORemarks (Include any visitors to project and misccllaneo• .;s remarks pertinent to work)The QAR, Contractor's Project Manager and Project Archeologists arrived on site today . The QAR inspected the wontarea . In the evening a reconnaissance of Site 10 (the tundra and trail system) and Site 4 ,(the mountain top) wasperformed by the QAR, Contractor's Project Manager, the Project Archeologist, and the CQC . Difficult travel conditionswere noted with respect to wet tundra and rocks . The Project Archeologist noted a human skull fragment at Site 4B . Itwas left in place pending further coordination with local government organizations.I certify that the above report is complete and correct and that all materials and equipment used, work performed and tests conducted dining this period wets in strictcompliance with the contract plans and specifications except as noted above .Qratfty Control Manager SignatureGovernment Quality Assurance CommentsConcurs with the QC report?YesZNo OAdditional comments or exceptions :&#J'fofo~ of GQov-,v za 1-. Lt. E-r r &4=n z;),2p ira-tr .'-+-& Twits7V sr sotic-o1 c- i eLA> t.uo.-S we trM,1-4v U,-% T1T tQ.f t t.AN>~iC'G°.ftPJ~'f't Qw /~v .~1~ v t> • C cg~• .Lr~~'S F~~rr r> ; tt~fPe'OE=c'z j' 1DZsC~th c'I re+ Ptz~i~ . r %a Z .r?,~hy _ -ro Axa}gvrS -4r+t> cK5CC' 'ro ZAA C-o s fjn.n> I /V w ~7' ~ Tu, 4-A.7-)1~~ t k vG …sT 1Naez~~TbZ,Q q r ..s c'.'TO s rrvt ..-u ri 4h~AAR slg natuS t v A-ztiL.1 n . . r iNoI -or-0L~OvLaGY! p .t~ r>7a$."'J .w AS ADJQZSS~b /t-+.'t1t1cO U'aWC ()? Yr1 ESc_) - t_ r-cre c .ro`ra 4 u L %f~vC i S 4w~ art; d s C-r f .t .:6Date2SIG Z .i-/-4.1.0_ -t IV Tbt !-yw t7-W~o c utL t ,ti 7yt 4 + C .7-y$r- 97QRJ i~T r ..~T A_ e:CJCLL tf.I- TEST vE~Fr(r jTSupervisor's InRWOatsOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location :Gambell, AlaskaDate : 7- 1999 Time :Activities Planned :Briefer :: C~ C'j, Zr-xBriefing Location :(rt/it/hUDTopic :Topic :Q uriBriefer Ae 'azTopic :r4 aTopic :Ia&::-Topic :Topic :Attendees214kvIS7~rl~ .~~cMiSite Healthand Safety Officer :_1~ ~/ /L 'Date :1999HOT WORK PERMITContract: DACA95-97-D-0010, D .O . 0004Project : Debris Removal and Containerized and Hazardous and Toxic Waste Removalocation : Gambell, Saint Lawrence Island, AlaskaType of Work :C1, t 7-2rc ,f t ~ yr_ f-(.,1- . hHeat Producing DeviceFire Guard : C•Location : tZ1a 5 T /5 A c T,,! f---7 TimeA> el,Scheduled Work Date :TheChecklistSuperintendent :BelowOZOperator :Start: /1'oo~/ /WasReviewed-Date : 7SHSO :_Time Finished :,'Date : __COMPLETE IMMEDIATELY PRIOR TO WORKHot Work ChecklistNIAYesNo1 . Are all flammables and at lest 50 ft away?[]02 . Is the operator fully qualified to operate the equipment?†0Q04 . Has emergency communication procedures been checked?(~05 . Is and ABC extinguisher present and is it in working order?Li06 . Have the tools and equipment been inspected for safety?ƒ07 . Is the correct PPE being wom?ƒ0ItemHas the Fire Guard been identified and briefed to observe the area for 1 hour after work iscomplete?8. Has the area been checked for flammable or explosive vapors? 009 . Have containers been checked for explosive! flammable residue or vapors?(drums and tanks)0010 . Are torch hoses purged before lighting (torches only)? 00011 . Are nozzles and hoses in good repair? (torches only) 0[0COMPLETE AFTER WORKTime Start: 4Ue rt 'Time Finished : r7t? r't -rSuperintendent : "~ ~/ `4 Date : 7 giHSO :- ---Fire Guard Released :Date:('4LOCAL RESIDENT HAZARD ABETEMENT PLAN FOR DEBRIS REMOVALContract : DACA95-97-D-0010, D .O . 0004'roject : Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island, AlaskaType of Work : Collecting metal debris and Construction Debris StockpilesHazard Description : Stockpiles of Metal create a potential hazard to area residents travelling on ATS,especially in low visibility . Some work areas are adjacent to heavily traveled roads . Stockpiles adjacent tothe road may create a hazard to ATV traffic. ATV traffic may be a hazard to work crews collecting andhandling debris .Stockpile PrecautionsThe site for each proposed stockpile will be inspected for traffic hazards prior to construction .No stockpiles will be constructed on ATV trails or within 10 yards of a regularly traveled trails .All stockpiles will be at least four feet high to provide a visible silhouette above adjacent terrain .Stockpiles shall be marked by four evenly spaced stakes minimum , of 2 .5 ft above terrain minimum, withorange or yellow flagging 2 ft . long minimum , one stake placed at each comer .Drums , planking , signage , or metal planking may be utilized as a suitable as outer warning markers along theaxis of travel if heavily flagged or painted with fluorescent marker paint .Precautions for heavily Traveled Areas .In areas adjacent to regularly traveled roads the following precautions will be implemented in addition to theabove .A warning sign will be staked on the road edge, 50 yards from the road in either direction from the nearestarea of work activity or stockpile .Personnel working within 10 yards of the road will wear fluorescent visibility vests .Personnel will be especially briefed of the hazards of passing traffic .Oil Spill Consultants, Inc .David L . ReinProject EngineerINSPECTION CHECKLISTContract: DACA95-97-D-0010, DO . 0004Project Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island, AlaskaFeature of Work : Debris Removal CLIN : 2Inspection : InitialRelevant Specifications : SOW 1 .3 .1, SOW Table 2, 02050, 01130, 01450Submittals : Work Plan, Health and Safety Plan, Environmental Protection PlanInspection ChecklistItemYesNotNotObsrvd1 . Is the proper PPE being worn?0'00002 . Is the work being conducted a safe manner?3 . Is metal scrap being removed to a sufficient depth?004. Are haul routes being maintained in a manner safe for vehicles?5. Are appropriate lifting and tie-down methods being used?D6 . Are excavated areas being restored?009 . Are all flammable materials kept away from hot work areas .D000Q'10 . Is refueling of saws and equipment performed in a lined area .0D11 . Is metal scrap free of dirt, wood, and other foreign matter prior to weighing .0012 . Is debris being weighed and weights recorded against the correct ledger?00Comments:0007. Are personnel on foot cognizant of vehicle haul routes?8 . Are loads being numbered and recorder as to the area originated?0SAFETY INSPECTION CHECKLIST FOR CONSTRUCTION EQUIPMENTCON TRACTOR :i T 'PE OF EQUIPMENT .`/EQUIPMENT ` UMBER .CONTRACT V1JMBER :7, 0DATE O~ NSPECTION :~ ~ :E'REVISION.92 , 385-1-1CORPS OF ENGINEERS SAFETY AND HEALTH REOLIRE N IENTS NtANLAL . EIMREFERENCES ARE IN PARENTHESES .INDICATE ANSWERS BY PLACING "X'* IN PROPER COLUMN .YESI NIANOMOTOR VEHICLES :" ECTER 8S A \IECH.~'tC .\O FOUW TO BE M SAFE OPEItA TT`~ •iOTOt .EHiCLE SHALL BE FL .CEO ; ' SE It, ICE L'TIL ; T Ii .S BEE' .SP0GCOMOrflONI \ cnicie has ocen cncCKea 10 insure tnat the euu ipment ana accessories are in sate operating conditions andfree of aooarent damage mat could cause failure . . niie in use . t IS A 021tc1_ . Lienis : f I3 .A .041 All .enicles or combination of .enicies ooeratec crn•ecn the sunset and sunnee shallhate the following nehts :, ,a . T ..o heaaliehts. one on each side of the front :b. At least one red tatllieht and one red or ameer stoonent on eacn side of the rear :-c . Directional signal Rents - both front and back . a:.aJ. Three emergent x flares . retlectf . e markers . or eaunaient eortaole ..amine device .3rat:c a• stem : ( 13 .A .Ue i Service nraKes and manuatl . -ooeratco - a kirte =rakes I1 eacn cnicie snail have. :n working orocr :t I3 .A.UbfXa . A ,Decoometcrb . Fuel gagec . An auatble .% amine :c, ice ; hom and or aacKuo at= IJ . A \.Inusnield couippea . .Itn an aucouate .% indshicfu . .Ircrc . Defrosting and aetoeetng devicef. .adequate rear \ few mirror or mirrorse . Cabs. cab shields . and other protection to protect :he -art . er from the elements and falling--!'-yor shifting materials5.h. Nonsiip surfaces on stepsi A oower- operated starting deviceand doors ; atcr% ziass ' An . cracked or broken glass shall betilass . i IS .A .U7) Is \% indshteld . . .Inuo ..s%~---replaced .:I13 .A .u81o mailersa. Structuraily adcuuatc for the ..ei nt ura . .n `b . Loikine uevicc or double safct . s% stem pro , taco anti .% orking'Safer cnains and or caoles''J . Trailers .kith po ..cr brakes equipped with break-a•% a' oe \ ice .. With will effectively lockAuo brakes in event of separation'Dumb trucks : 118 .A .IU1a. Equipped with a holding device to prevent to pre \ ent accidental loaenne of body dunngmaintenance or inspection''b . Hoist levers can be secured to prevent accidental starting or tnopine"8 Emergenc y equipment: i I S .A . I I I Minimum for vehicles of I I : :on or o .er operates on public highways ._,hall be .khat is reautrea by state la%% but not less than :a. One rea flat not less that 12 -- square w rah stanoari aria three reflective mark ersb . Two .kneel chocks or each unit of a combination of chiclessc. At least onelOB2AC:C fire extinguisher into oroocri \ rated for flammable cargoes)REMARKSLSERE%ERSESIDEINSPECTED AND CERTIFIED BY t>IGNA rURE OF MECHANIC . lSPA Form 33 (Revised I %tav 19961IF;PPROV D BY : ISI_1-\ECESSARYIlN rU OF COMPANY OFFICIALIy-t~~1\IACHINERY AND MECHANICAL EQUIPMENT :.D TESTED S•U \IaCi/i'ttV Oft \IEC1 U\IC LL EOi.'P'IF'T SH -LLL BE Pt ACED rv SERVICE LNTTL IT HAS BEEN M PECTED . 'k CO' (1` ETEYT PERSON.ND CERTT7M TO E*% SOE OPERA TIING CONDMO'iINDICATE .\NSW ERS BY PLACING "X" IN PROPER COLUMN .YESI cquipment rccwremcnis . , : b .A .U7)a . Seats or ecuai protection provided for each person required to floe equipmentI o When operated on ine ntgmvav- headlights . ta)IlighLs. brake lights . eacxuo tights. antium signals visible Irom Irons and rear must be providedWith winosnields%snail be equippca w ith power wiper and detoggin iv detrosting cc\icesd . Sen ice cr xc s . stem . parking brake sv stem . and emcrgencv I manually opcratea rromNO v i- i -e . At a minimum . one do cnemleal or carbon-diox ide lire extinguisher w lth a rating .o!5B :C ItaesedI chareca . and ready for use)Reverse signal (BACK-L P) alarms i 16 B U I I3 t ;uaruine t Ib B .031 s rccuired for ire foiiowlne :a . All bets . sna ;ts . pulleys. sprockets . spindles . drums . tI neeis . Chains. orother rec :crocatine . -ataune . or moving parts of equipment..aces inciuU)ng e-\naust p .pcs or other lines5 . Hot surc . Charging skip snail be provided with guards on both sides ano open epos of skip area.i . Platforms . . atwaiks . sides . handholds4 Fuci tanks iocatea not to aludw spiiis or o' crilow-s to run onto engine. exnausL or c :ectncai equipment416 B 041Eshaust or discharges uo not cnoanccr "%orxmen or obstruct view or oocrator i Ib B .U51n )catbelLs comply wrtn 49CFR 5"1 i Ib B 08)Fallingooiectorotecuvcstructures iFOPS) I1b .B .1I)(athroughc)3 Rollover Drotective structures (ROPS) I Ib B . 121 la through e)q Is glass installed in operator S Comoarimcnt safer' class' (16 B .IU)10, Points requiring lubncauon during operation shall have fittings so located or euaraed to DC accessiblewithout hazardous exposure . H6 .1313)I I . Whenever long-Ded ena-Dump trailers are usca : t 16.B . 15) provide a roll-over warning desice: the de. iceshall have a continuous monitoring disp(a% at the operator station to provide the operator with a quick andeasily-read indicator and audible warming of an unsafe condition .f_vREMARKS : LSE REVERSE SIDE IF NECESSARY)INSPECTED A'D CERTIFIED BY . i StG`A I LRE OF MECHANICIAPPR D B JIpa rUU.RE OF COMPANY OFFICIAL~VV1--~~I\i' i Form s3 iReviscU I \Iav I9QAISAFETY INSPECTION CHECKLIST FOR CONSTRUCTION EQUIPMENTONTRACT NUMBER:C O NS64 STYPE OF EQUIPMENT :EQUIPMENT NUMBER :DATE 0 IN SP CTION :CONTR .,kCTOR :,~'- U) -fit, L t/ -L CORPS OF ENGINEERS SAFETY AND HEALTH REQUIRE`IENTS MANUAL . EM 385-I-I . REVISION 92 .REFERENCES ARE IN PARENTHESES .INDICATE ANSWERS BY PLACING "X" IN PROPER COLUMN ._YESNONIAMOTOR VEHICLES :\ 1) ')OTOa %tH1CLU S)tLLL aE ?L%CtO t`r SERVICE L'*. rr HAS BEEN M'SPLCTtO SY % NRC) l\WIC 4.O rOC$O TO It M SArt ortMTT!Q Co, vrno-41 . Vchicie has been checked to insure that the equipment and accessories are in sate operating conditions andfret of aoparent damage that could Cause failure while in use . t 1 S_A .021(c)2 . Lights (I 8 .A .04) All venicles or combination of vehicles operatea berwccn the sunset and sunrise shallhave the following Iithts :a. Two headlights . one on each side of the front :b . At least one red taillight and one red or amber stooitg_ht on each side of the rest :c . Directional signal lights - both front and back` ariad. Three emergency flares. reflective markers. or ccui%afent oortable wamtnt device.Brake S%-Stem: t I3 . . k .US i Service nr:KCs and manually-operated trsiane orv :cs4. Each tchicic shall have. in wort:ine oracrt I3 .A .ubia. A speedometerb. Fuel cagec. An audible warning device thorn and or backup aiarmid . A windshield equipped with an adequate windshield wiperc. Defrosting and dcfoeging device-rf. Adequate rear view mirror or mirrorsg . Cabs . cab shields. and other protection to protect the-driver from the elements and fallingA_At_tY_ZINCor shifting materialsh. Nonslip surfaces on stepsi . A power-operated starting device"C,S . Glass : i I8 .A .U7) Is windshield . windows . and doors gala`" glass ' .any cracked or broken glass shall bereplaced .6. Trailers: ( IS .A.U8)a. Structurally adequate for the weight drawn'_b. Locking device or double safety system provided and working'c. Safety chains and or cables'.,tomd . Trailers with power brakes equipped with break :-a%%ay device which will effectively lockup brakes in event of separation?7 . Dumo trucks : 1 I8 .A.10)a . Equipped with a holding device to prevent to prevent accidental lowering of body duringmaintenance or inspection?b. Hoist levers can be secured to prevent accidental starting or tripping?S. Emergency equipment: I l8.A . I I) Nlinimum for vehicles of 1 1 : ton or over operated on public highways .shall be what is required by state law but not less than :a . One red flag not less that 12- square with standard and three reflective markersb. Two wheel chocks or each unit of a combination of vehiclesc. At least one 2.4 : I OB :C fire extinguisher ( t%v s prooeriv rated for flammable cargoes)A)CREMARKS : i USE REVERSE SIDE IF NECESSARY)INSPECT ED A ND CERT IFIED BY : I SIGNATURE OF MECHANICINPA Form a3 (Revised I May 19961APP OWEDY : )SIA i TURE OF COMPANY OFFICIALiMACH [NERY AND MECHANICAL EQUIPMENT :NO II ACHNEAY OR \tECKk\IC U IOC? tEvT SH UL BE Pt.CEO IN SERVICE UNTIL IT MAS SELM INSPECTED k%D TESTED IN % CO'PETEYT PEKSON &NO CUITV (ID TO It, N S .FE OIEU TrKGCDF,DITIONINDICATE .ANSWERS BY PLACING " X" IN PROPER COL UMN .5.6.Cquipment requirements : i Ib .A .Ui). Scats or equal protection provided for each person required to ride equipmentab . When operated on tnc .highwayheadlights. taillights. brake lights. backup lights. andturn signals visible from front and rear must be providedc. With icinashicids : shall be equipped with power wiper and detogginvdefosting devicesd . Service br Eke system. parking brake system. and emergency (manually operates fromdrivers s position Ic. .at a minimum. one dn- chemical or carbon -dioxide fire extinguisher with a rating of 5 8 :C nagged . charged. and ready for userReverse stenat I BACK-LP) alarms 116 . B .011Guaraine (16 .B .03) a required for tnc toilowing .a. All belts : : ars. shahs . Pulleys. sprockets . spindles. drums tly\sheels. chains . orother rccicrocatine . rotating . or moving pans of equipmentb. Hot sunaccs including e'.haust p .pes or other linesc . Charging slap shall be provided w ith guards on both sides and ooen crass of skip aread . Platforms . : :twalks . iteos . handholdsFuel tanks tocatea not to avow spills or oscrtlows to run onto engine . exnausL or cicetncal equipmenti 16 .8 .04)Exhaust or discharges ;o not cncangcr %%orKmcn or obstruct view of oDcrafor 116 .8 .031Scatbe is comoty with 49CFR 571 f 16-B US)I.2.3.4.7.Falling obicct Orotectrs c structures i FOPS) 1S.9.10 .Rollover protective structures CROPS ) 116 .8 .13) la through it)Is glass installed in oocrator s compartment saiexv glass '? ( 16 .13 . 101It .Whenever long-bed end-oumo trailers arc used : ( 16.13 .15) provide a roll-over warning device : the dc%iceshall have a continuous monitoring display at the operator station to provide the operator with a quick andeasily-read indicator and audible warning of an unsafe condition .YESNONIA`_/I) l a through ciPoints requiring lubrication during operation shall have fittings so located or guarded to be accessiblewithout hazardous exposure . 116 .8 . 13)REMARKS : (USE REVERSE SIDE IF NECESSARY)INSPECTED AND CERTIFIED BY ISIGNA FLRE OF 'MECHANIC)3`PA Furm 83 (Revised I Ua . 19961A PPROVED 8Y : iSIGN ..kTLRE OF COMPANY OFFICIALiCONTRACTOR :SAFETY INSPECTION CHECKLIST FOR CON STRLCTION EQUIPMENTCONTRACT NUMBER:TYPE OF EQUIPMENT :i" 7~ oaa/•x as 1 Q sEQUIPMENT NUMBER :~r (~ tci 4C L~~ - ~JDATE OF ( SPECTION :2-79CORPS OF ENGINEERS SAFETY AND HEALTH REQUIREMENTS MANUAL . ELI 385-I-I . REVISION 92 .REFERENCES ARE IN PARENTHESES .INDICATE ANSWERS BY PLACING "X" IN PROPER COLUMN .MOTOR VEHICLES :tYESNONIAtM'IOTOn %EHICLE SH . LLL BE PL.+CED N SElt %ICE L"TIL IT HAS BEE`d rrSPECTE o BY a VECKANIC k"O FO4.'!+ O TO BE N SAVE OI'ERATiNGCo"o rriO'I1 . \ chicie has been cnccKC(l to insure that the equipment and accessories arc in salt operating conditions andtree of aoparent damage that could cause failure while in use . r I S . .A .0211c)2 . Lights : 118 .A .04) All venicics or comotnation of vehicles operates Denyeen me sunset and sunrise shallhave the following lights :a. T %% o headlights . one on each side of the frontb . At least one red taillight and one red or amber stoongnt on each side of the rear :c . Dirccuonai stenai lights - both front and back - a.:aJ . Three e :ncrgenc\ ; lares . reflective markers . or ccui%aicnt ooriable earning device .i3rake r stem : i 13 A .U5 i Serv ice nraKes and nar.uail% - opr :area : :rune DraKes.Each'ensue shall have . :n wonane oracr :t I3 .A .Ub)4a . A ipccoomctcrb . Fuel gage'betJt~_LA`c . An audible warning device thorn and or backup atarmid . A +vmdshield equipped with an adequate w indshield \r, toere . Dctrostine and defogging deviceekI . Adequate rear view mirror or mirrors~-_e . Cabs . cab shields . and other protection to protect the-driver from the elements and fallingor shifting materialsh . Nonslip sunaces on steps~'_i . A Dowcr-operated stantne_ device%Glass: i 18 .A .U7) Is \~indshicld . %%inaowsana doors satcry grass ' .An\ cracked or broken glass shall bereplaced .6 . Traders : t I S .A .U81a. Structurally adequate for the weight drawn'b . Locking device or double safety system provided and working?C . Safcn' chains and or cables "?d. Trailers with power brakes equipped with break - av%a\ aev'icc %%hich will effectively lockup brakes in event of separation?7.Dumb trucks. t 18 .A .101a . Equipped w i th a holding device to prevent to prevent accidental lowering of body during5.I'~Jv'-Imaintenance or inspection"b. Hoist levers can be secured to prevent accidental itanine or tnopine'8 Lmergcncv equipment: ( IS .A .I I) `linimum for vehicles of I I _ :on or over operated on public highways .shall be what is required by state law but not less than :a. One red hag not less that 12 " square with standard and three retkcave markersb . T""o wheel chocks or each unit of a combination of vehiclesc . At least one 2A :IOB : C fire extinguisher (t ..- n prooeriv rated for rlammable cargoes)ti1C;REMARKS : i LSE REVERSE SIDE IF NECESSARY)1INSPECTED AND CERTIFIED BY . iSIGNA CURE OF MECHANIC(SPA Form 33 ( Revised I May 1996)' r TURF OF COMPANY OFFICIAL( .APPROVED BY : SI CMACHINERY AND MECHANICAL EQUIPMENT :•O %1 .CH1'E0Y 01l .IECKk%IC u EOE'7%R,.T SH kIL BE Pt /CEO (rv SERVICE U T IT HAS IEEN rNSPECTED 4%D TESTED aS k CO%7ETFYT PEISON ANOCEATLFMED TO BEIN S of E OfERATTNG COKDIT10.*4INDICATE ANSWERS BY PLACING'-X" IN PROPER COL UMIN .I .2.3.Equipment recu(rcmcnts : t ib A .U71a. Scats or c=oal protection provided for each person required to ride equipmentb . When operated on the hienwav_ headlights- taillights. brake lights . backup lights . andtum s(gnais visible from front and rear must be providedc . With %%inoshiclds : shall be equipped with power wiper and deioegingidetrosung dcyucsd. Scr.tce braise system . parking brake system- and emergency ( manually opcraeca fromdnvcr s position Ie . .at a minimum. one dr.. chemical or carbon-dioxide lire extinguisher %%ith a rating of tB :C tagged . charged . and ready for userReverse signal t BAC}:-CPI alarms ( 16 .8 011Guarotne t 16 .B .031 is reauircd for the to(lowlne :a. All belts . _ :ars . shams . puileys. sprockets, spindles drums . ilh .%hcels. chains . orYESNO`/AVL_~~-!!other reC :Dr0cating . rotating . or moving parts of equipmentb Hut sunaees including c\haust p .pes or other lines.c . Charging sap shall be provided %%ith guards on both sides and open ends of skip aread . Platforms . zzovalks . iteos. handholds4.5.6.7.8.9.10 .Fuel tanks locatca not to allow spins or o%erIIowys to run onto engine. exnaustL or clcctncat equipment(16 .B .04)Exhaust or discharges uo not endanger %%orKmen or obstruct view or ooerator ( 16 .8 .01Seat belts comoty with 19CFR 571 ( 1O .B .US)Falling object protcctt'e structures I FOPS 1 ( 16 .8 .1 1) (a through ciRollover protective structures CROPS) ( 16 . ( a through e)Is glass installed in oocrator s compartment safety glass ? ( 16.B . 101Points requiring lubncatton during operation shall have fittings so located or guarded to be accessiblewithout hazardous cxcosurc . 116. B . 13 )JI1,i,ii/LWhenever Tong-bed cno -aump trailers are used : ( 16 .8 .1 S1 provide a roll-over warning device : the de' Iceshall have a continuous monitoring display at the operator station to provide the operator with a quick andcasily-read indicator and audible warning of an unsafe condition.REMARKS : (USE REVERSE SIDE IF N E CESSARY)11 .INSPECTED .ANDCERTIFIED BY : (SIG`APUREOF'MECHANIC)3'PA Form 113 (Revised I >tar 190(.1APPROV ED BV : ,SlGAtLRE OF COMPANY OFFICIALi> .aFETt 1\.SPECT ION C HECKLIST FOR CONSTRU CTION EQUIPMENTCO . TR aCT Ll RCONTRACTTYPEEQL"OFNTE0NUMBERS ENT NUMBER .I D AT OF)NSPECTION .CORPS OF ENGINEERS SAFE T Y .AND HEALTH REQUIRENIENTS MANUAL . Ell 385-I-1 . REVISION 92 .REFERENCES ARE iN PARENTHESESLY ESNO IINDICATE A NSWERS BY PL .ACiNG • X•- IN PROPER COLUMN .MOTOR VEHICLES .f•-0MOTOR \EHICLE SH\L . aE PL+C‡C ;\ tEQ~'CE LNTIL IT HAS SEEN trspEC-fE0 By + \IECH .'IC %\0 r0C .D TO 6E M SAFE OPEMT1 4C COr+01110%I chine nas oeen cnecxea ;o insure .r.at :ne equipment and accessories are in sate open tine conditions andtktree of aooarent ua .:.ace :pat could cause :ailurc tt^lit ;n use _ t 13 .v02)(c)2 . Llents : I I S .A .t)4I .ati \enicies or cerloinauon of \ C .^.Ic ;es operatea centeen ine sunset and sunnse shallha\c the tollo\\ine nehtsv~] . r'.\o neaonents, one on each side of :he front :b . .At :east one rt- : ;i~iI2ni anti one rea or amoer stocltf_nt on glen side of the rear:___c D ;rec :tonal s ;er.a : tights - noth front aria back : aria.j . Three Lmvicenc . : .arcs . retlecti%e martcers . or eeui\alent oonaoie \\ arilne device.!X:~C1ke _n stem : I I S A .u ! ~Crt Ic : .- .'ax s aria r1anuall\ -rneraIea '=: x ;rat orakes"aacn \,niCie snail na'e . :n %nrkine orocr( I S .a .U0 i] . A ) : e :corncler-I-LR5 F .:ei eaorAn auoinle '% arn ;r.e Je' :cc ; ntrn a^u or r 1ckap afar ri i'\ inusnlciC cc : ;:re : : '.t iIn an a ;c,;uate tt inasr ielt a perDe :rosiinc anti :o e'nc ue\ it e.Adeauate rear '.Ie'.% mirror or mirrorsV'z . Cabs . cao snicks . ;no otncr protection to protect the-\iriver from the elements and fallingor snit tine mater :aish . Nonsilp surfaces on stees, . A oo…cr•opcratea s=ine_ device-.-Glass : 1 I S . A . U i 1 is w musnicla . .\ ;noo1\ s . aria doors safety Mass .' .an\ cracked or broken glass shall bereolaced .b r railers : I I S .A US Ia.Sir ic,urail\ auc0 ..ale ;or me ••\e :gnt- I ran 'Licking .:cvicc ir Qouoie sa ;et\" S'\ stem oro' ice- aria %%orklne1OC-j. . Sa :etn c'rains anti Jr ceoles',/ .r ra ;lers %iin power nrakc s equipped \v it h break- a\\a\ .fe\\ ice \\ n ic h \\11 1 etfectiya v lockuc orakes in event of separationDumo trucks : I13-A . IUIa. Equippea with a holding device to prevent to pre\ent accidental Io\\enne of body duringtx_maintenance or inspection"b . Hoist levers can nc secured to prevent accidental stanme or tneelne'S Emergency equipment : I IS .A . III Minimum for vcnicles of I I : : on or o%er operated on public highways .I,hall be wnat is rccuirea by state law but not less than :a. One rca flag not less that 12- iquarc \\ ith standard aria three rerlecti \ a markersb T .\o \\neel chocks or each unit of a combination of \ehicIcsc A ; least one 2 .A IUB C 1 .re ettineulsher ttx%n oroocri\ rated for flammable cargoes)REMARKS . . i" SE RE\ ERSE SIDE i s \LCES SARY iyniINSPECTED .AND CERTIFIED BY , ~, IGNA f LRE OF MECH ."aNIC I l APPROVED BY . (SIGNA rURE OF COMPANY OFFICLaL I I\PA Form 33 (Re%tsed I \13v tYdhieMACHINERY AND MECHANICAL EQUIPMENT :•0 %I+Lt4I RY nR \ILC 1 , VC S: c7l :T~ff~T tH -,LL BE Fl ICED rv SERVICE L"TII . IT HAS SEEN NSPECTED 4'D TESTED I~ COSPETE`rT i'E .3O d • O CEITIr:', SAFE OIER.ATT .G C0%DITTONINDIC .a i E VERS BY PLACING "X" IN PROPER COLUMN .I_rnri%cr s position)c . kt a minimum . one do cr :emtcal or cartwn-dioxide tire extinguisher %%ith a rating of 53 C :aeecd. : .'a.reed . and ready for userReverse sienat IBACn•L?I alarms , I (3 B UI1i;uaraine i to B 03) a rccutrca :or tnc tonowing .a A 1 t,- : :S . _ea:s . smarts . puilevs . sprockets. spindles, drums . 0, s.herls . cnains. orJtne : :cc :c :oca : :r.Z . -Jba inc . or moving parts of equipmentslut > r.ac~s .ac :uJ ;r.c e\ .^.aust n .pes or other lines,, Shat? ;'_ -~ :o Gall be cro'wcu %%Itn gurus on both does and open CADS 01 skin areave/b".3.910 .11 .,`-~G~_vPatterms ;_ :'.'a .~s- cs . ^anuhotds.tNIA=~sna li be equipped with po% er wiper and detog„ tneide fr ostine de' icesJ . Sen ;ce cral::c s\ stem . parking crake s._ stem . and emergency imnnually operates fromNO-% ;sicle from front ants :ear must Dc provided;in3YESLjuIpment ;cc uiremenu : ; . 0 A t1'1'cats or ecuai crotec :ion LroviUed for cacn person required to ride eawpment1 her, Jcc o :ca on tnc 'trrn\a, . ncad)Ignts . taillights. ors a lights. oaci;up lights. andTOIL-~/Fuet :a'KS peatea n0l :0 ~‚JI~ ~c :us or ,,\crtIO' S to run onto engine . -xnaubt. ur ctcCtncal equipment.16 .804)Exhaust or ,ascnarecs .:o not enuar.Fer ~%ommen or oostruct view of operator 116 3 .0:)'catbc)ts comoi% wttn 49CFR -;-I , Ib B .Us)Falling opted :rotcctr'c structures I FOPS) t 16 .8 . 11) la through c)Rollover protective st:.:aures i ROPS 1 i 16 B . i_ 1 ( a throuen e)Is glass Installed in operator s compartment satcty Class ' t I6 B .10)Points rcuulnne iuonruon Jur :ne_ operation shad have fittings so located or guarded to De accessiblewithout nazsrcous cvcosurc I h i3 I . 1Whenever ;onr cca cna-OUmO trailers arc used : t I b .B . I :) provide a roil-over wammg dev ice : tae de' ice16-11f/~-'vc r`'t/shall cave a continuous monnonne Utspia\ at the operator station to provide the operator with a quick andcast]-read indicator arc audible warring of an unsate condition .REMARKS . LSE REVERSE SIDE IF \ECESSARYIi;III\SPECTLD \ND LERT!FIED BY !)IEJ\A I LRE OF \ILCHANIC)I' .PA Furm t3 IRcvuca 1 \ta, I"V6).APPROVED B) i~iGKA F RE OF COMPANY OFFICIAL I' .AFETY INSPECTION CHECKLIST FOR CONSTRUCTION EQUIPMENTCONTRACT NUMBER :CONTRACTOR .0/1TYPEtyre - ?,2 c?' 005/, c- C G A/S u e r SOFEQUIPMENTEQUIPMENTNUMBER .DATE OF NSPE TION :1 CORPS OF ENGINEERS SAFET' :' .AND HEALTH REQUIREMENTS MANUAL . ENI ;85-1-1 . REVISION 92 .REFERENCES ARE IN PARENTHESESINDICATE ANSWERS BY PLACING "N" IN PROPER COLL1N .YESNO I N/A IMOTOR VEHICLES .\t0?oR \EMCLE stall 8E PL ACED IC SER \ ICE III. IT M 4S BEEN r'SPt TED BY a'iECH+~N iC \\ 0 rol.N) To BE M SAFE OPERMNG Covomo'I \ chide nas been checked to insure that the equipment aria accessories are in sate operating conaiuons andtree of atioarent damage that could cause ,atiure \\ hilc in use . i I8 .A .A'_ltcl_ . Lients : I IS .A .U11 All \enieles or comoim.ation of \erneles operates ter\ een Inc sunset and sunrise shallha%c the folio\%inv iiChts :1a . T \\o ncaaliglts- one on each side of t he front :\t :east one reu ta :i112r ; and one red or ameer stoeng nt on cacn side of the rear:t1~ . Dirccaonai si na ; : :tints - both front aria back : a :.dI~ . Ti:mce cmergenc\ ;fares . rcaecti .e markers- or euui\aient coracle \\amine device .:irv.e ~: \ stem : 1 1 s .A .U5I Ser\ Ice :-rakes and manuatl\-\\oeratea :cit.ins :rakes- c,cn \cnie :e snail na\e . n \\on.inc order :f IS A .ubi1.~'I1v:\ speedometera . Fuel gapec . An auable \\ am ;ng ue•. Ice : horn and or oaekuo -farm iJ . .A windshield eauiopeu \%ith an adeQuate \\ ineshie :d \\ ioerc . Defrosting and Qetoee ng deviceAdequate rear \ ic\\ mirror or mirrorsvg__-ve_yCye Cabs . cao sniclds . and other protection to protect :he-driver from the elements and fallingTor sniffing materialsn . Nonsitp surfaces on steps11 A oo\\er-operated starting deviceiXitaeGlass : I IS .A .U i l is \\inQsnicld . \\inoo\\s . and doors saictr- glass' .An\ cracked or broken glass shall bereplaced .e Fraiicrs : 1 18 A .U81a.Structur\xvCa i ly adeQuale for the \vcight dra%%n'_Orb . Locking device or oouole safety s\ stem pro\-taed ana \\orkine': . Safety chains and or cables'-_-I~~J . Trailers \\tth po\\cr nraices equipped with break -d\\a\ device \\hieh \\III effectively lockt uo crakes in event at sccaration'- Dumo true KS . 118 .A .1 U ia. Equipped \\ith a holdine device to prevent to crc\ent accidental lowenne of body duringmaintenance or inspection'b . Hoist levers can rte secured to prevent accidental starting or tnopIne'S trncrgcncv equipment: ( 18 .A . I I) \linimum tar venicles of I 12 ton or o\er operated on public high w a}'s .,hall be \\ hat is rcQuircQ by state la\\ but not less than ;a . One reC Ilae not less that I_ square with stanoaro aria three rerlecu\e markersIrb T\\o \% heel chocks or each unit ola combination of 'chielesc At least one 2 .A : 108 C fire extinguisher (t\%o orocert\ rated for flammable cargoes)RE\t .AR .~,S ,LSE REVERSE SIDE IF \ECESS .ARYIiIi' : SPEC T ED AND CERTIFIED UN t SIG` A I L : RE OF \IECH .A .IC,\PA Form 3 (Re\isei I \ti ivti91APPRO\ ED BY j SIG\A f 'RE OF COMPANY OFFICt .ALi\IACHINERY AND MECHANICAL EQLIP\IENT :,o uACHNERr Olt \IECI1 X\IC LL EOi ?\CEVT SH Ut. BE PL .%CEO IT SER'SICE LNTIt IT HAS BEEN NSPEC 1D k'O TESTED IN % CONPETE`T PERSON 4,N0C`ERT%F.' SAFE OPEMTl .G CONDIT10%i\DIC .aTE .a\SIVERS BY PLACING "- X" IN PROPER COLL\ININLqulpment reuwrcmcnLs . I : o _k U-1.i . ScaLS or ecual oroicctlun crovlded for each person required to rce eouipmento \\ hen ucc ;-atca on rte nlem~av . ncaullents . tailllehts , brake ilenLS . aact: up lights . ano2.NO IYES-0 LE: ;.rn sienals'Isloic from front ana r ear must be provided1i ;ih ,% In,:snlclds . snail oc equippca with power w iper and dcioeg!n „• detrostln „ ae\ icesJ . Scn Ice craze s' stem . oaring oraxc sv stem- and emergency (manually operatea rromJnycr s : osnlonle . Al a minimum . one an chemical or carbon -dioxide tire extineuisne '%Ith a rating of =3 :C Itaeecd . cnareca . and read s for userReverse signal I BACK- i: P` alarms I I It) B J1 1_L>'-Guaralne (16 B .03 ) is recuirca for the totlowing :> ;i beats . _ :ars . snatts . cutlcss . sprockets . spindles. drums t1''- to s. cnatnS. or"tncr r, . .croca :Ine . ru :aung . or moving parts of couipmentHuts aC :Suotne a\nauSt o .,^us or other lines:KID ; .1111 CC : rOvIUCU '. %Itn guaras on ooth sides arlu corn ,nas ell skip areahlatiorms1X.1~nanuhotusFuel tanks Ioca :ca not :o a :,u' ~ct1U or o erllo\ss to run onto engine , e .xnau L or : : rcnCa1 eoulcment1163011Exhaust or Ulscnarees :o rot cncanecr \%orKmcn or uostruet View of operator 1 It) 3 U :1h . Scatbclts comply satin 49CFR 5 71 I Ib B .U81Falling object orolectnc structures I FOPS) 1 16 .13 . I I ) (a throueh ci8. Rollover protective structures IROPSI I Ib . B .12) ( a through e)Is class tnstailea in operator s comoanment safety etass' 1 16-B . 101910 . Points requiring Iubnrrton dur ing operation shall have linings so located or euaraea to oe accessiblewithout hazardous e\eosure 1 16 3 I : I11 . Wheneser lone-OCa eno-oumD trailers are used : t 16 -B- 15 t provide a roll-over s .amine aesice: the de . iceshall have a continuous monitoring utspia% at the operator station to provide the ocerator with a quick andeasily-reaa Inaicator ana audible ""amine of an unsafe condition .'~;~~eREMARKS : (USE REVERSE SIDE IF \ECESSARY)INSPECTED .AD CERTIFIED B's ISIGNAILRE OF MECHANIC)\PA form 83 1Revtscu I \fa% 1Y1 61APPRO%EJBl iiGNATLRE OF COMPANY OFFICIALiSAFETY i\SPECTION CHECKLIST FOR CONSTRU CTION EQUIPMENTCONTRACT NUMBER--CON TR-, C TORC 5,C/V 5- LTl• PE Or E'1L I PMENIZ- /I V FSEQUIPMENTi` UMBERDATE OF I_/ 9CORPS OF ENGINEERS S .AI-ET':* ADD HEALTH REQLIREEIENTS MANUAL . EM 385-I-I . RE VISION 92 .REFERENCES .ARE 1N P .ARENT-iESES .INDIC .A T E .AN'S\ti ERS BY PL .ACiNG "X" IN PROPER COLLMti YES;NO I \ A IMOTOR VEHICLES .I ttOT00. YEHICL E SH LLL 3E PL kCED IN SERVICE t-'TIL IT HAS BEE". r'SPSC :ED Br A ttECit 'ic A'D FOUND TO SE IN SAFE OPEIL~AI NG CONDETtO'1Cmc :c nas oe r. cnC :1:eu to insure :nat :ne equipment ana accesones are in safe operating conditions andtree Of aDDarent Jamacc :nal cOUla Cause failure ttniie in use . i IS .A .Q2I(c)A Ul t ~ . tc- e es r .emeiflation of veniclcs opcratr :et"een : ne sunset and sunnse shall-ate :rc :oilo•tiri : ,,tsone or: : : n Side dl the fron t :.A : :east o c r : .. :atiiien : ara one red or ameer $:ODtient on eicn s ize 01 the rear :noin front.r_ano back . a: '.Xd . Tnrce c :^c :ce ct : :arc~_ ;Caeeti c markers- or coonatom Dortaolc %%arnine device .I _ -44 .~t stem : i f d .A 'J : I Scrt ;C . -rai .es ano manuaut -oreratco -~ . :ne : far cs~'I s =_-n t :Dic :e snail nave . :n t%orK : it: ordcri I3 . .A .u i1..k iCCeccmc :cr'OrD FUCi fa2cAn a uci bie 't arrt,ne act i c_ :horn and or Daexuo a :arrn tA •t inusnieid cculppcu •.t nn an adeuuate %%. inas ietu tt tocri . Oe :r. .IjI-e?C--~--_os :inc ir, ., . :Ul' IOC de% Ice.AOCOu'ate rear \ : ., mirror or mirrorsg . Cabs. cao sh ;c :us . and other protection to protect :he-onver from the elements and falling.)r sniriine ma :cr :aish . `onsiip surfaces on SICDSi._IKA cover-operated star.ine_ device_v(d . l ;iass : i 13 A .u'1 is t%indsmcId . itlruo s . ano doors Safe . „ISS$' ant cracked or broken glass shall bereDiaced .6 T .arrsi i td A .US)io~.i ocJraliv adCCJale : it the ttcient dra%%nh . Lone uct,cc or cnuc .c sate :\ system oro'iaeo ana ttorlang .'..-- I4'Z .iS 1 lea - C i a .n$ ar) .: Jr Cables'd . I-ratiers t% in,uucr nrakes equipped tt ith break-a%% a% uevicc tt nicn vvIII effectiv ely lockup orakcs in evcnt of ceparauon'-II\jDumo trucks i l S .A . I U )a. Equipped with a noldine device to prevent to orc'ent accidental lovvenne of body during-maintenance or nspcct :on"'b . Hoist levers can De secured to prevent acciecntat starting or tnootne8 . tmtree^ct equipment : t I S .A . I I i Minimum for vcnicies of I I : :on or of er occratcu on public highways .An a i be anal is rcuuirca by state ;a•.t nut not less than :a . One .'cc ilag not loss that 12 square with stanciara ano three retlecttve markersib . T ,%o tt necl chocks or each unit of a computation of t chicles,:.At least one _2 .A IOB C : .re extinguisher ( ttto oroocrn rated for tlarnmable cargoes)RENT. ;R:-,S LSE REVERSE SIDE :F \ECESS ..RY)!II\SPEL'ED AND LLR 1 ;FlED [r LITRE UI \IECH_X\IC, a?PRO \ ED B1 /SIGH RE OF COMPANY OFFICL i i\PA Form a) tRevisei I \Iav 1 Y106 i\I .ACHINERY AND MECHANICAL EQLIP'.',1ENT .• 0 ./ACHI\ERY O0. .TECH k'IC . . :UL :7` F .T 91 /L, bE P' %CEU I' SERVICE L`TIL IT HAS SEEN IM1SPECTED . .D TESTED 0 . . CO•tTETENT PERSON .n0 CEATIF:• SAFE OFEMTn.G CO .DITION`DICA 71E .1NS'•VERS BY PLACING `X" IN PROPER COLLMIV .I.YESTO BENO I N ALquipmect recuiremeaa : , ; o .A .U7I1. Seas or c :uai p rotection provided for eacn person required to ride ecuipment~\ hcn Jt:c :-zitea on : nc ; ;ten .. ; . - headlienis. taillights . brake Itghts . oacKup tights . ana.m sl2ras side ; :om ;rort and rear must be provided.rah oc equipoco .% ith power wiper and detoegtn2,detrosting aes ices_~cr !ce or 2.kc s . stem . parking DraKc s% stem . and erncr-eeric .' I manuail operate ; rrOm:osittonl3orecr. Crcm :Cai or ca:non-dioxide fire extinguisher %% ith a rating or' ; ._2L3'C :a22eO . Chareru . a:.u read% for userRe%erse s :ena ) IB .ALK-i. Pt alarms ~ io 8 UI )3Guaruire I lo B .U3 ) i5 r,C'.: ;rco for the tOiiowine :a. .a ;l belts . Snar.s . ewle .s . sprockets . spindles . drums. t1%%%hcc :s . C hains orother rcc : :rocatine . rotating . or mo v ing parts of equipmentc Hut sur.aees including exnaust p .pes or other linesl_, . C`a :2 :rt SXio snail be pro'. toed .% tin guarOs on both sides ana 0Dcr. :r. as Of skiD area_Zae :s- nanuhoiu!' 1F ue : t :rKsia"..z : :0 : : .J . . ~_ . .~ or o• c : :io .% s :o : :. :-, onto engine . c .'nausL Or e :C.tr1CaI equipment16804E6.-.hausit or oisc arses oo r:ei cruan_c : I .ort,mcn or oostruct vie .% of operator 116 B .U :)Scatbcits eomoly .\ tin 49CFR 5 1 I b .B .U8)Falling ooicct crotccti %c structures FOPS) 1 Ib .B I I) is through c)YYS.9.10 .Rollover protective stractu: es t RUT'S) 1 16 B . I .) 1 a through it)11 .Whenever tone-ocd ono -u uma trailers are uscu : i I b .B . 15) provide a roll-o . cr . .arnine desice: Utc desiceshall have a continuous monuerino displa- at tnc operator station to provide the operator with a quic k andIs glass installeu in ooclator s comoa -tment safety e)ass ' 1 16 B . IU)Points re q uiring lubncauon ;urine operation shall have titunes so located or guaraeo to be accessiblewithout ha ardous cs cosurc 1 16 B . 13, 17`-seasily-read : r,alcator ,rtu auo :ble . .aging of an unsafe condition .REMARKS iLSE REVERSE SiDF iF \ECESS RY)INSPECTED .\ 'D LERT : ; IE :.` B't t i L RL OF MECHANIC)NQ\PA Furm s IRe .iseu 1 \1a . .'.APPROVED BY t~,iG\ .A rLRE OF COMPANY OFFICIAL ISAFETY INSPECTION FOR MISCELLANEOUS EQUIPMENTU .S . Army Engineer District, AlaskaDate of Inspection :Contractor or Unit 0~ L - ' `Contract No . or ActivityInspected by (Signature)Witness ( Signature)RUBBER TIRED FARM TRACTORS, BACKHOES, FRONT END LOADERSYesNoNOTE : Safety and Health Requirements Manual (EM385-1-1 ) references inccrentheses .1 Is protection (grills . canopies, screens) provided to shield operator from falling orflying objects? (163 . 10 and 16 .8 .1 1)2 Is adequate roil-over protection provided? (16 .8 .12)./3 Are seat belts provided? (i63 .08)~/4 Are only designated qualifies operators Deing assigned to operate mechanizedequipment? (16 .A .04)~/5 Does the unit have a suitable fire extinguisher? 5 BC (16 .A .26)6 is there an effective , working, reverse alarm? ( 16 .8 .01)7 Are moving parts, snafts . sprockets, belts . etc . . guarded? (16 .13 .03 (a) andv~16 .B.07 and 16 .5 .13)8 Is protection(1 6 .B .03 (6) )against contact with hot surfaces . exhaust . etc ., provided?9 Are all screens , guards, shields in place and effective?v(16 .8 .03)10 Is a safe means of access to the cab provided ( steps , grab bars, non-slipsurfaces )? (16 .8 .03 (d) )`~11 Are pressurized cylinders . outriggers, etc ., equipped with a pilot check valve?(20 .A .17)12 Are sufficient lights erovicea for night operators? (1 6 .A .1 1)~/13 Are there initial inspections ana scneduled inspections of the equipment atregular intervals? (16 .A .02 (a) and (b) )14 Are fuel tanks located in a manner to prevent spills or overflows from runningonto engine exhaust or electrical equipment? (16 .8 .04)15 Are exhaust discharges from equipment so directed that they do not endangerpersons or obstruct the view of the operator? (16 .6 .05)16 Has the equipment been inspected and tested by a competentperson?(16 .A .01)17 Are inspection records kept available as a part of the official(16 .A .01 (b) )Remarks: ~GY c•~ .1 l'` tW-1l; cclC (G' e L ~--project file?`~N/ASAFETY INSPECTION FOR MISCELLANEOUS EQUIPMENTU .S . Army Engineer District, AlaskaDate, of Inspection :71i-l)?ContractororUnit~'i_Inspected by (Signature)Contract No . or Activityr- ~ r rWitness ( Signature)SCRAPERS, MOTOR GRADERS, HEAVY HAULING UNITSNOTE : Safety and Health Requirements Manual (EM385-1-1) references in parentheses .YesNoN/A1 Is the unit equipped with a ;uitabie fire extingusher (5 BC)? (16 .A .26)2 Is a safe means of access to the cco previaed (steps . grab bars, non-slip surfaces)?(16 .B .03 (d) )3 Is the operator protected against weather, failing or flying objects?'~(16 .8 .10 and 16 .8 .11)4 Are seat belts and adequate rollover protection provided where applicable? ( 16 .8 .08 &16 .8 .12)‚5 Are adequate head and tail lignts provided? (16 .A .07 (b))6 Have brakes been tested and found satisfactory? (16 .A .07 (d))Y7 Does the unit have an emergency brake system? (16 .A .07 (d))8 Can the emergency system oe activated from cab? (16 .A .07 (d))9 Does the emergency brake work automatically when regular brakes fail? (16 .A .07 (d))~-10 Have air tanks been tested and certified? (20 .A .01 (b)),~11 Is an air pressure gage in working condition installed on the unit? (20 .A .12)v12 Does the air tank have an accessible drain valve? (20 .8 .17)v13 Are the units equippej •v :in v--Andshieid wipers . defrosting and defogging equipment thatare in good operating condition? (16 .A .07)`/1/14 Is there an effective reverse signal where applicable? (I 6 .B .01)15 Has the unit been inspected ana certified mechanically safe bybefore being placed in use? (16 .A .01)a qualified personI/16 Is the record of the test available? (I 6 .A .01 (b) )17 Is the unit shut down for servicing, tueiing . etc .? (16 .A .14)18 Are only designates quaiifiea operators being assignedequipment? (16 .A .04)to operate mechanizedr/19 Are fuel tanks located in a manner to prevent spills or overflowsengine , exhause, or electrical equipment? (16 .6 .04)from running ontoy/20 Are exhaust discharges from equipment so directed that they do not endanger personsor obstruct the view of the operator? (16 .8 .05)21 Are seats provided for each person required to ride on equipment? (16 .A .07 (a))REMARKS :]-c c h r~'u-c)/r :rA.r' C)CA)C /JC, 1, leLLMNC: P1 ? C- riFoIn385-32-Rd v7-/A-,•,,-s__i Proponent CELN N -S CIEnvironmental Quality ControUQuality Assurance Report(ER 415. 1 . 10:1Contract Number I Delivery Order NumberUPC/Project TitleDACASS _ 97-D-OOIOID .O . 0004Debris Removal and Containerized Hazardous and Toxic Waste Removal'QC Report Number012Oat, or Time Period7117199ether Condlt onsemp Low 43_ Tamp HI10-33 Knots ConditionsWind SpeedLocation and TeamGambell , AlaskaContractor48CloudyOil Spill Consultants, Inc.Quality Control Inspections Performed This Oat . (Include inspections . results . deficiencies observed . and corrective action )Preparatory 0 s." aeach.d checklistIVubal0 a .e attached ch.ckltstFollow-Up0NO INSPECTIONS TODAYWasthedeficiencytrackinglistField Sampling and TestingHas field testing been performed this date ?Type of test MethodMtatnxupdatedthisdateYesQNoYes Q NoQuantity of samples ResultsNoneHave Data Quality objectives been achieved ?N /AYesoHave Samples Been Collected for Laboratory Analysts?Type of Test EPA Test Method/Matrix Quantity of Samples1400Yest] NooNoneHave required amount of OC trip blanks and nnsates been achieved ?N/AYesONoDHave appropriate QC laborabry tests been ordered 7 (matrix spikes . method blanks , surrogates , reference standards , etc .)YesONoDHave QA and QC samples been collected in the specified quantity?N/AYesONoDHave samples been property labeled and packaged ?N/AYesO MooHealth and SafetyWorker protection levels this date :Level A Q Level B Q Level C Q Level D 0 WAOYes 0 MooWas any work activity conducted within a confined space ?Yes0NoƒWas any work activity conducted within an area determined to be immediately dangerous to life and health ?Were approved decontamination procedures used on workers and equipment as required 'Yes 0 No 0Safety Commerft : (Include any infractions of approved safety plan, and include instructions from Government personnel . Specify corrective action taken .)ety meeting covered :Hazards to and from area trafficI he potential for eye injury from blowing grit was stressed at the safety meeting . It was also determined that the ATVtrailers could be used for crew transportation if they had sufficient seating and hand holds . The passengers must alsowear the same PPE as the AN operator. The AN must not travel faster than 20 mph on improved roads and 10 mphoff road while carrying passengers in the trailer .Repairs were completed on the Nodwell . A safety inspection was accomplished and the machine put back into service .A live power cable supporting FAA navaids was discovered , on the surface of the soil , on east side of runway in Area 8 .Personnel from the project had been collecting and stockpiling matting on foot and with heavy machinery in the area .The area was also a runway shoulder improvement project for Alaska DOT under construction by another contractor .The area was immediately marked and work suspend at that location . The contractor's Project Engineer reviewed theDOT project drawings indicating the presence of the of buried utilities . The route of the cable was marked , and allpersonnel were briefed to keep clear of the area .GAR SAFETY COMMENTS:j j uo w var'~-< ~~1°h v ~ S t9 ~ .'G-st t O # t; CC ,1'Y)EC r~ IV rv lam.1 t - C /t.. . 5 r i> .a'KaG'?~ ..4 o Tfib,-nvc r- C n~ ~t ~ioP/~ ci~ t=I A c .t~ + .vooP~rz'+-: I b f 5 T -~ . •v G . lei (e r e-/4fQ" TX(-1_1 kTi t4. Q '' A ' ,. f ~c 7t .a: 8Z CA---, LC/Q.4 c X c)'~ G/1 .~,'Sc~2'J7P~t c K .rt > c r crv 2 e' Q . . ,~~ .C " ~~J1-5I0'-~cr36~3>c•/t~ flIt-vi-i> O e'jnGtL C.r •v ~7 .7-&Ywo'= treeEnvironmental Quality Control/Quality Assurance Report(ER 41S-t -302)Continuation Sheet"'-At Activities Performed This Daterence (NAS ID //Tech Spec 0)Activity&LocationQuantityContractor_,.*m Removal (NAS ID 0020 . 02050) Stockpiled metal debris from Area 8 50% of metal stockpiled(the runway and west beach area)none yet weighedSpecific areas worked include thesouth overrun for the runway andthe area between the runway andTroutman LakeManpower and EquipmentLaborpesa1flcatlonProtect ManagerCOC System ManagersuperintendentArcheologistoperatorLaborersNumber111ManHours131313110EquipmentType4 wheelerCat 426 loaderArgoNodwellPickupCat 966 Loader16Total Hours .Number3121273134kssiruetlons Given by the Government to the Contractor ( Include names . reactions . and remarks .)none.Hours Used12018181103Total Hours :41Verbal Q Written 0work Progress rte there any Contractor caused delays or potential finding of fact?Are there any Government caused delays or potential finding of fact';Am there any unforeseeable or weather related delays ?Yes 0Yes 0Yes QNoNoNoRemarks (Mdude any visitors to project and miscellaneous remarks pertinent to work)Scheduled fuel barge did not arrive . Village store out of fuel . Now using limited drummed fuel brought out duringmobilization .Site reconnaissance of Area 12 conducted by Project Manager, COC Systems manager, QAR and Archeologist .tial inspection on HTW removal requested for 7/19/99 .Initial inspection requested on weighing procedures requested for 7/19/99 .Archeologist researching past studies and preparing field reports-I certify that the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this period were in strictcompliance with the contract plans and specifications a as noted above/ll/_'_i Z1_.C/ ___ ,Quality Control Manager SignatureDateGovemment Quality Assurance CommentsConcurs with the OC report?Additional comment or ehreptions :Pcsti02_ CA - r•s a'T rf-Wl A'f7t rV C.L.L'SISYes, No Q~h r tiv~1-~ -1,t_r- Cv , a :el cxir=t<7 Z) b° EZ re ( S~~I~ 20 L P OR )'VA CCAd-" .,rro Or, t S tft JtL2 . Fit 6*4V- L.T~1 ~ .r. 17 ~<1 1 ' -r- Kt~aw wthc")QAR Signature1.7"%j -J-P.4C-3~c?5 r~tt .~Date27f /7, 1 9Supervisors Inttal DateTˆcOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate : /' ~~1999 Time :Briefing Location :,,Activities Planned :Briefer :~J'~~ tTopic :2-"A'Topic :Topic :Briefer:Topic:,N( : c( fn v . r_5Topic :Topic :AttendeesSite Healthand Safety Officer :Date :1999HOT WORK PERMITContract: DACA95-97-D-0010, D .O . 0004Project : Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation: Gambell, Saint Lawrence Island, AlaskaType of Work :Heat Producing DeviceLocation-1p -Operator: (~_' Id" ~~Fire Guard :_L!ol % /,;may J ~L~s O~Scheduled Work Date :TimeStart: Time Finished :The Checklist Below Was ReviewedSu eri de 1~~ / C CC/Date : ISHSO :, i 0C MPLETE IMMEDIATELY PRIOR TO WORKHot Work ChecklistN/AItem1 . Are all flammables and at lest 50 ftaway?Yes No[]2 . Is the operator fully qualified to operate the equipment? fa []3 . Has the Fire Guard bean identified and briefed to observe the area for 1 hour atter work is f, Dcomplete?4 . Has emergency commjnication procedures been checked?5 . Is and ABC extinguisher present and is it in working order?6.Have the tools and equipment been inspected for safety?7. Is the correct PPE being wom?8 . Has the area been checked for flammable or explosive vapors?9 . Have containers been checked for explosive/ flammable residue or vapors?(drums and tanks)10 . Are torch hoses purged before lighting (torches only)?11 . Are nozzles and hose:s in good repair? (torches only)COMPLETE AFTER WORKTime StartC ?"'^Time Finished :Superintendent :; r ~.;Fire Guard Released :/Date//_BHSO:: 4V lDate :i ~LSAFETY INSPECTION FOR MISCELLANEOUS EQUIPMENTU .S . Army Engineer District , AlaskaDate of Insp ction :-711Contractor or UnitContract No . or ActivityInspected by (Signature)Witness ( Signature)SCRAPERS, MOTOR GRADERS, HEAVY HAULING UNITSNOTE : Safety and Health Requirements Manual (tM385- 1-1) references in parentheses .YesNo1 Is the unit equipped with a suitable fire extinguisher (5 BC)? (16 .A .26)2 is a safe means of access to the cab provided (steps, grab bars . non-slip surfaces)?(16 .B .03(d))3 Is the operator protected against weather, falling or flying objects? ( 16 .8 .10 and 16 .8 .11)4 Are seat belts and adequate rollover protection provided where applicable? (16 .8 .08 &16 .8 .12)5 Are adequate head and tail nights provided? (16 .A .07 (b) J6 Have brakes been tested and found satisfactory? (16 .A .07 (d))7Does the unit have an emergency brake system? (16 .A .07 (d))8 Can the emergency system be activated from cab? (16 .A .07 (d) )9 Does the emergency brake work automatically when regular brakes fail? (16 .A .07 (d) )10 Have air tanks been tested and certified? (20x4 .01 (b) )11 Is an air pressure gage in working condition installed on the unit? (20 .A .12)12 Does the air tank have an accessible drain valve? (20 .8 .17)13 Are the units equipped with windshield wipers, defrosting and defogging equipment thatare in good operating condition? (16 .A .07)kIL14 Is there an effective reverse signal where applicable? (16 .8 .01)15 Has the unit been inspected and certified mechanically safe by a qualified personbefore being placed in use? (16 .A .01)16 Is the record of the test available? (16 .A .01 (b))r17 Is the unit shut down for servicing, fueling , etc .? (16 .A .14)18 Are only designated qualified operators being assignedequipment? (16 .A .04)to operatemechanized19 Are fuel tanks located in a manner to prevent spills or overflows from running ontoengine , exhause . or electrical equipment? ( 16 .8 .04)20 Are exhaust discharges from equipment so directed that they do not endanger personsor obstruct the view of the operator? (16 .8 .05)Y21 Are seats provided for each person required to ride on equipment? (16 .A .07 (a) )REMARKS: vcL. S >S ~ ~ %" LNGr42EL1~Form 385-32-RLr2vzc`t1~FLProponent : CELM ttEnvironmental Quality Control/Quality Assurance ReportI ER 415-1 .30-)Corgract Number / Delivery Order Number UPCIPro/ect TitleDACASS- 97-0d0101D. O. 0004 Debris Removal and Containertzed Hazardous and To xic Waste Removal"4C Report Number Date or Time Period Location and Team0137f18l99Gambell, Alaskaiath.rConditionsContractor47Temp Low Q_ Temp HiConditionsVend Speed17 .28 KnotsCloudyOil Spill Consultants, Inc.Quality Control Inspections Performed This Date (Include inspections, results . deficiencies observed . and corrective action )Preparatory0 s.. aaache d checklistInitial 0 a.. aaach.d checklist 1Folk w-up 0NO INSPECTIONS TODAYWas the de6cien y tracking list updated this dateYesField Sampling and TestingHas field testing been performed this date ?Type of test0NoYes 0 NoMethod/Matrix Quantity of samples ResultsNoneHave Data Qualify Otifectives been ach ieved?WAYesDHave Samples Been Collected for Laboratory Analysis ?Type of Test EPA Test Method/MatrixMOOYesO N00Quantity of SamplesNoneHave required amount of QC trip blanks and rinsates been achieved ?NIAYes( :] NOC3Have appropriate QC laboratory tests been ordered) ( matnx spikes, method blanks . surrogates , reference standards . etc .)YesONo0Have QA and QC samples been collected in the specified quantity?WAYs0MoOHave samples been property labeled and packaged'N/AYssO MooHealth and SafetyWorker protection levels this date:Level A 0 Level B 0 Level C O Level D 0 wAOWas any work activity conducted within a confined space ?Yes 0 MooWas airy work activity conducted within an area determined to be immediately dangerous to life and health ?Yes 0 NoƒWere approved decontamination procedures used on workers and equipment as required? Yes 0 MooSafety Cortumerlts : (Include any infractions of approved safety plan . and include instructions from Government personnel . Specify corrective action taken .)he correct procedures for chop saw use were discussed at the safety meeting . Specifics includes rotation of personnelto avoid fatigue, correct PPE , and safe work distances . Crews were also briefed on the hazards caused by high winds.Handling sheet metal, flying debris, and potential grit in eyes were discussed .A crew break shelter with hot drinks and a rest area was set up in a connex . The was implemented to prevent crewfatigue or hypothermia as winds increase and temperatures drop .Heavy truck traffic was noticed along the road that parallels the runway . This transects our current work area . Thesuperintended briefed all personnel to use extra caution .Extra overburden was place in area of the buried electrical line discovered 7/17/99 to provide protection from equipmenttraffic along major haul routes .GAR SAFETY COMMENTS :1,1 JlOo C IC .. 't`'t soE) wtf 4Ze,thr 13,,JPor. t,/e--, ., -r lie,- -T~ . ti t. ~.,-syS4A2.,/L. erGS st l~/ > ticyest vwr r+t o‚`~ 5~'~ .n &) .IEnvironmental Quality Control/Quality Assurance ReportIER 415 .1302)Continuation Sheetft ActivitIes Performed This Datemice ( NAS 10 &Tech Spec8)AcUNty&LocationQuantity.,reins Removal (NAS ID 0020. 02050) Stockpiled Metal . Area 8 area between eastside of runway and parallel road Trimmedexposed end of partially timed metal matContractornot yet weighed .Scale hung on gantry Tare weightstaken in preparation for debris weighingHTRW Removal (NAS ID 0022 . 02050) Staked proposed area of Area 12Drum Dump south of Troutman LakeManpower and EquipmentEquipmentLaborCtasalicatlon Number ManHoursTypeNumber Hours UsedProjectmanager1124wheeler33017Cat426loaderttCDC System ManagerSAt :f a in gistoperatorLaborers'dent113Argo213110Nodwell10110Pwkup10550Cat966Loader13Total Hours .102TotalHoursYts*iuctfons Given by the Government to the Contractor (Include names . reactions . and remarks)noneVerbal 047Written 0Wort Progress Are there any Contractor caused delays or potential finding of tact )Yes Q NoAre there any Government caused delays or potential finding of tact' Yes Q NoAre there any unforeseeable or weather related delays?Yes Q NoRemarks (include any w3dors b project and miscellaneous remarks pertinent to work .)Fuel barge still not in due to high winds . Less than two days of fuel on hand .n attempt was made to deal with the exposed end of partially buried metal matting . Dirt was removed exposingIroximately one to two addition feet of buried mat . A cut was made with a chop saw along the dirt line . 1/10 of a miler ut. The new cut edge was inspected by the QAR . He stated that the approach tried would not be acceptable .Cat 426 had major hydraulic leak . Was removed from service .Archeologist researching past studies and preparing field reportsArcheologist Consulted with Mayor Winnie James and Sivuqaq Inc . President Job Koonooka about artifact/burialprocedures. They agreed that relics were to be turned over to Sivuqaq Inc, and indicated preference for human bones tobe reburied at the place of discovery , with the Project Liaison Burt Ooozevasouk witnessing . Consulted with OAR SteveLeClerc about follow-through , and decided Corps will draft letter based on Mobley draft reviewed by James andKoonooka . The USAFCE will submit the letter to City of Gambell, Sivugaq, Inc ., and Gambell IRA council .I certify tat the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this period were in strictcompliance with the contract plans and specifications except as noted above .Quality Control Manager Signature-z.42 4')-/2Date 7 ! `iGovernment quality Assurance CommentsConcurs with We OCreport'YesAddbonalla No 0commentsorexceptions-`.r RS-e- .Q-2 -t%;-~ 3= ''3 - too'" w.C .>`,ed - A>1Ew=A 3, `f, S IaVT-e- - •4s Y ,eCTh h ) r.,>=>C 7L%rk v.j Or- ~~Utvv4Tt~v r ll . tawˆS rL X t,Mend i) rl , Cs.71. V ev I '1>~"•c,4 , t5 F,?~.m.r'A-sLL l fix. r' ort_M a .~a .. c -)T A'% A-r- C-VPJtC SA-+t,v -'rt ,El17Datey2 -2V 'Y9SupervisoesInitialDataf2 .a e"D .OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate :1999Activities Planned :Briefer :Time :Briefing Location :'/?~Topic :Topic :6,1.fYhhfTopic :Briefer :Topic :Topic :Topic :Attendees i-Site Healthand Safety Officer : ' 2 , i5A- -4Date: i!J _ 1999HOT WORK PERMITContract: DACA95 - 97-D-0010 , 0 .0. 0004eject: Debris Removal and Containerized and Hazardous and Toxic Waste Removalration : Gambell , Saint Lawrence Island , AlaskaType of Work: _C-V \ )~-\ CHeat Producing DeviceOperator :Location :Fire Guard :Scheduled Work Date :i I ~ ITime Start:The Checklist Below Was Reviewed'Date :Superintendent :Jl C,^Time Finished :/_'~ 1 ' SHSO :Date: _CMPLETE IMMEDIATELY PRIOR TO WORKHot Work ChecklistN/AItemYes1 . Are all flammables and at lest 50 ft away ?2.Is the operator fully qualified to operate the equipment?Has the Fire Guard been identified and briefed to observe the area for 1 hour after work is LVjcomplete?4 . Has emergency communication procedures been checked?†Is and ABC extinguisher present and is it in working order?Q5.6. Have the tools and equipment been inspected for safety?Q7.Is the correct PPE being worn?~.J8.Has the area been checked for flammable or explosive vapors? a~QHave containers been checked for explosive/ flammable residue or vapors?Q9.(drums and tanks)10 . Are torch hoses purged before lighting (torches only )?11 . Are nozzles and hoses in good repair ?Time Start : Time Finished :Superintendent:iN,a(torches? •Ponly)QQQFire Guard Released : 3 . 3C>Date : j'' 0 /' SHSO:-Date : ~/qEnvironmental Quality Control/Quality Assurance Report(ER 4111•)( _)Contact Number / Delivery Order Number UPC/Project TitleDACAOS- 97-O-d010/D.O. 0004 Debris Removal and Contalne ized Hazardous and Toxic Wast e RemovalCQC Report Number Data or Time Period Location and Team1147/ 19/99Gambell , AlaskaherConditionsContractorp Low 43 Temp HI47Wind Speed17-2t KnotsConditions Light Rain.Oil Spill Consultants, Inc .Quality Control Inspections Performed This Date (include inspections, results . deficiencies observed . and corrective action.)Preparatory ƒ .. e attached chacklbt Waghing, HTW Removal, SanrVlinqInitial 0 We attached checkup SanpltnqFollow-Up 0Was the deficiency tracking list updated this dateYes 0 NoField Sampling and TestingHas field testing been performedthisdate?Yes0Type of testMetod/Matns Quantity of samples ResultsNoHave DataN/AQualityObjectivesbeenachieved?Have Samples Been Collected for Laboratory Analysis?Type of Test EPA Test Method/Matrix Quantity of Samples0YesOMoDYesDMooSee Chain of Custody Form and Field notes AttachedHave required amount of QC trap blanks and rinsates been achieved? WASYesDNoDHave appropriate QC laboratory tests been ordered ? (mat x spikes , method blanks , surrogates. reference standards . etc.)WADYesƒNODHave QA and OC samples been collected in the specified quantity? Not required by Delivery Order N/AƒYesDHO(]Have samples been properly labeled and packaged ?N/ADYesƒNoDHealth and SafetyWorker protection levels this date :Level A 0 Level B 0 Level C 0 Level D 0 WADWas any work activity conducted within a confined space ?Yes0NoƒWas any work activity conducted within an area determined to be immediately dangerous to life and health? Yes 0MooWere approved decontamination procedures used on workers and equipment as required?Yes 0 MOOSafety Comments: (Include any infractions of approved safety plan, and include instructions from Government personnel . Specify corrective action taken .)the safety meeting the presence of truck traffic from another contractor in the area was discussed and crews Weresited to yield to these vehicles and use extra caution . The presence of the underground electrical cable east of therunway and protective measures taken was briefed to the crew . All personnel were alerted to new excavations made bylocal residents in the road used to travel from the lodge to the lay down area . An alternate route was identified .Later in day the a suspension of work for cutting, heavy debris removal, and equipment movement was given in the areaof the buried electrical cable east of the runway .(see "directions" block)QAR SAFETY COMMENTS :Ltvb_ 34tC4F Vote .- too,_,,, ZIC, CA PS 4_GJw. c4..-, yZ~ I, A_, 2Z_@,4 +~ .:M Lt1r~: ~4 rAlvST4~~ of s~ryr+si r•va .VS r. ~j .Lh -tLaw 3 J,e tS SEAC4-, Fo rC~* 1%- p vT ~ c/~r‡S • 1.i1 ~ L V A-' r v .y,t ~. '~ 2~C .v .?L c t~ - -~. ~ . 4ttr.lrzd~7~ZJt ~ZL79~. ht ~2ow -t-v fF Ao A-fl .,,I c; Imo; M~ .,-y,C4L Z2>.-'tit.v. ..+Jrr• .ycJ C5C Z4I (.4ChE-=:- ~YC .~ - rr t~~, ~4PP 7,rN r°be c ctao Pi G. ,~. . ~c~ A-t>1u w, t,, t r t - - -,- W'V~r .J . .v cCc~ c4 c S i r .~ +yy . ,v f ` :'c'Y/l-+t: G S • 6J '~, t ou.. / t + t S A,0 ana, u , M t S zD ,f't' TN-~i~ DtGc~ NGS .td-et 6p M ET q - rT1r t - GP). uC1' E7L C,Rw,,"OOL6UA3vPIPat,A .Ytltlr cvt, .C- ATt t'1-Nlr1!oT" GA,ky\-f Yt'S k= 1 Vt~ C)ar - 1 C~ l3 Y 1°~u., ~.GL.LtTbd 1roX IC -leifvu H As`72 BtcA .~s~t~ wt~A c.D Ey , q , tT• a.) Q R E X C 4.,.Kt avV . My F> -' 4ol~ p l~,R-3 ,~e D av D'D%: c ^- st S t'rA'LL .4-vW/tS ttor Nt-r- fit! B v.T COULD% VC }/ISa4.h S t-4cT loo/'j E 4 4lv1'1 G d .KY C.hJM'R tTIVI14, Noj A)-7-44 D 1C1?Z b t t-Cow-, r-.4--Environmental Quality Control Quality Assurance Report(ER 415 .1-302)Continuation Sheet%ctlvltles Pedomsed This Oat*nce (NAS 10 lFTech spec s) Activity &LocationQuantityDebits Removal (NAS 10 9003, 02050 Weighed previously stockpiled Metal . Area 8,west beads. Continued to collect and stockpilefor area between runway and Troutman lake .Manpower and EquipmentLaborClassttlcatJonProtect ManagerCOC System ManagerSuperintendentArcheologistOperatorLaborersNumber11ManHours131311131016Total Hoes :1272102Contractor10,768 lb weighed to date50% d area 6 completedEquipmentType4 wheelerCat 426 loaderArgoNodwellPickupCat 966 LoaderHour Used364Number3121120110056Total Hours :instructions Given by the Govemrnent to the Contractor (Irldude names , reactions . and remarks .)Verbal0Mhfttan 0QAR Directed suspension heavy debris removal, cutting, and equipment operations in the area of the undergroundelectrical buried electrical cable between the runway and Troutman Lake . The area was marked with stakes andflagging, and all work in the area was suspended except for removal of light surface debris by personnel on foot . Allproject personnel were briefed of the hazard .QAR directed suspension of work on the partially buried metal matting along the east side of the runway where ashoulder improvement contract was underway by another contractor . Personnel had been trimming the exposed edge ofthe mat to reduce the visible area (see remarks, below) .QAR directed that if human remains were encountered, they should not be disturbed in any way . The Archeologistshould be alerted . The contractor would be responsible for interring the remains . This would be done only after theA^rheologist had approved the action . The interment must be done in the presence of the Archeologist and the Projectson from the Village of Gambell .The OAR informed the Project Manager and the CQC that it may be permissible to use non -HazWOPR-trained local-hirepersonnel for debris removal with special stipulations . This issue is being coordinated between the contractor and theFairbanks Resident Office of the USACE .Work Progress Are ewe any Contractor caused delays or potential finding of fact?Are there any Government caused delays or polenbal finding of fact?Are there any unforeseeable or weather related delays?Yes 0Yes 0Yes 0NoNoNoRemarks (Indkde any visitor's to protect and miscellaneous remarks pertinent to work)Fuel barge finally arrived . The pickup trick will be able to be used for crew transport once gasoline is available for saleby the village store .An attempt was made to deal with the exposed end of buried metal matting . Dirt was removed exposing approximatelyone to two addition feet of buried mat . A cut was made with a chop saw along the dirt line . 1/10 of a mile cut . The newcut edge was inspected by the QAR . He stated that the approach tried would not be acceptable . A direction to suspendthis work was subsequently given (see directions above) .The starter on the Nodwell failed and the unit was rev eweo°~ from service .Cat 426 which had been removed from service for major hydraulic leak was repaired and returned to service .Archeologist, the developer of the project archaeology/burial SOP for eventual USACE letter reviewed his latest draftwith QAR, USACE Steve LeClerc .sfy tut the above report is complete and coned and that all matenals and equipment used . work performed and lists conduced during this period were in strictplience with tha contract plans and speofications ela e ( asDate2; ;~Za J'OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title: Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, Alaska1999 Time: I')-7Date : -7/ "Briefing Location : L ~_,GUActivities Planned :Briefer:Ch ()Topic: ~I,rtl~~rcu11 I CTopic : L)Xk L. L lc t1 ii lncdBriefer :Topic :L-it'k'-Z-e'1(fATopic :161 1~ /_ ~c dTopic :Topic :AttendeesN1112 /X~I~1yLSite Healthand Safety Officer.i-~Date : / a1999Chain of CusProject' 1 ofDebris Removal & Containerized Hazardous & Toxic Waste RemovalGambell, AlaskaCo ntr act No: DACA8S-97-D-001 0, Delivery Order #4Authorization Number.Clientamplers :4.1OSCI Purchase Order No . 913yEf~~~/Oil Spill Consultants, Inc .The Environmental Cleanup Company(SignatureWitness:209 E . 51st . Avenue, Anchorage, Alaska 99503Tel : (907) 562-7169 Fax : (907) 562-7225r19SInature/Analysis Required by :~"Anal sis RequiredOraN,wmM 00) ti^NO-eldSampleOM,ScreenSample Number Date Time PID Reading-fRM-OD -•fr- - S1Relinquished by: (Printed)(SignaturesRelinquished by: (Printed)(Signature)Dispatched by : (Printed)7-/c/-Type# ofCont .aOOOd~$~adE °vapcoU ° ^vSorrv~/7/9-9'Soiv v rr7-/9t ; DDso,/v vADateTime••tlo00C ga° aN,OQ O(000NE --d=° °0) c U)wcmQedm01CoC13N. a° < <~/~/w'C:^Ow ooReceived by: ( Printed)(S nature)Received by : (Printed)(Signature)Received at Laboratory by :(Signature)Method of ShlpmenCondition of ContainersComments:Good Fair PoorReceived Temp/ acRequiredlNo . Icle•7 /1;1 04 7~io.~S afe,Js /e%. .qea o19em ripf ion2,ys,*M/ 99-GAM-00/-SL ‡7-/9-99 4.0, / :l oi ..t W S. . / from fief// j-, or3 99 - GAN/ -Oe .? - S! /27-/9-9.9/ .o "V ed7-/?-f7D./ S'/' .ned .r0 °/Q99- GAM-OOf -S1 2T,./ d.. ,ff*1/!!~p/'JNIfo / O ~!/0f l, .a/IIf/)X J Jy/,r too-'Or/ IoJ /v4 ,, ‰~ 'Itil~f'i 4,/ d-' Ii rrf p,%4 f av..//,O k f JJ/f/ /It,/'fs.l••tt#.~/% . f .' h e 1~ to Or .111/ • wfg,r /+ .Vr ., r, o-v ,y/ .~ r y/ •/I f f~!l.rl f Al yr,'~ ,,D 4 Jcw,,1d2i -w5 -P° ZV Pj/ y' ~~ ~/.. ..~ rw/16.V./p // .• •f ...nipf4/s/t L'Q; Jf If fir / j7 f off//9~' 'I (' ti IfJ/Jdrs/Q/ !..ivod . rJ ; / i'V/0,wI, ii547 - .9- 9 79pl,, /, /y o/ t~. . .irc/ SOi /,,,cf7%r,•7/e0Si ~C 2 /S /sled Ne /4e'•r f 0/ 6• .•., ell41#"/ /SO y~r~ frer+ //T d f~ oirli~e.xs, .4 tf • rs1 /oC~'.9r : 7r', = 1./9C/O/r)2 7kso HZ• 4/ 1i 71y o` ,f~c ~ .r ~IleJ So . lINSPECTION CHECKLISTContract: DACA95-97-D-0010, O.O. 0004act: Debris Removal and Containerized and Hazardous and Toxic Waste Removalation : Gambell , Saint Lawrence Island , AlaskaFeature of Work : Drum Removal/HTW CLIN : 3 Inspection : PreparatoryRelevant Specifications : SOW 1 .3 .1, SOW Table 2, 02050, 01130Submittals : Work Plan, Health and Safety Plan, Environmental Protection PlanInspection ChecklistItemYes NoNotObsrvd001 . Have all required submittals been approved?2 . Have the applicable section of the statement of work and specifications been 0 0reviewed?3 . Has a safety meeting beenheld?024. Have equipment and tools received a safety inspection?"5. Has the hazard analysis been reviewed?00000Have PPE requirements for the activity been established? ~~ 0 07 Has the area of work been defined?8 . Have the drums been located ?Z'Z]i'0009 . Are required materials for spill containment available?00010. Have staging areas , access routes , and collection points been established? 0 011 . Have procedures for handling drum liquids been reviewed? El 012 . Have procedures for cleaning and crushing drums been reviewed?Comments:--00&2zr-. e> c6(/ZVv/CQC System ManagerDateIeLe^ 1A,e4/SAFETY INSPECTION FOR MISCELLANEOUS EQUIPMENTDate of Inspection :U .S . Army Engineer District , AlaskaContractor or Unit'-/2Inspected by ( Signature )Contract No . or Activity160C KX o(17 /5~r4Witness (Signature) ~~RUBBER TIRED FARM TRACTORS, BACKHOES, FRONT END LOADERSNOTE : Safety and Health Requirements Manual (EM385- 1-1) references inparentheses .1 Is protection (grills, canopies, screens ) provided to shield operator from falling orflying objects? (16 .8 .10 and 16 . B .1 1)YesNoN/A`'2 Is adequate roll-over protection provided? (16 .8.12)3Are seat belts provided? (16 .B.08).i4 Are only designated qualified operators being assigned to operate mechanizedequipment? (16 .A .04)5 Does the unit have a suitable fire extinguisher? 5 BC (16 .A .26)~/6 is there an effective . working, reverse alarm ? ( 16.8 .01)~'7 Are moving parts . shafts, sprockets . belts, etc .. guarded? ( 16 .8.03 (a) and16.B.07 and 16 .13.13)`~8 Is protectionagainst contact with hot surfaces . exhaust, etc ., provided?(16 .8.03(6))9 Are all screens , guards . shields in place and effective? (1 6 .B .03)10 Is a safe means of access to the cab provided ( steps , grab bars . non-slipsurfaces)? (16 .8 .03 (d) )`~11 Are pressurized cylinders, outriggers . etc ., equipped with a pilot check valve?(20 .A .17)v12 Are sufficient lights provided for night operators? (16 .A .11)13 Are there initial inspections and scheduled inspections of the equipment atregular intervals? (16 .A .02 (a) and (b) )14 Are fuel tanks located in a manner to prevent spills or overflows from runningonto engine exhaust or electrical equipment? (16 .8 .04)`~15 Are exhaust discharges from equipment so directed that they do not endangerpersons or obstruct the view of the operator? (16 .11 .05)16 Has the equipment been inspected and`~tested by a competent person?(16 .A .01)17 Are inspection records kept available as a part of the official project file?(16 .A .01 (b) )Remarks:ifv~fac~/ /l~ 6E P.~~a '0/M-vContract: DACA95-97-D-0010, D .O. 0004Project: Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island, Alaskat ire of Work : Sampling CLIN : 4, and 5Inspection : PreparatoryRelevant Specifications : 1450Submittals : Sampling and Analysis PlanInspection ChecklistItemYes No1 . Have all required submittals been approved?M0NotObsrvd02 . Have the applicable section of the statement of work and specifications beenQ' 0 0reviewed?3 . Has a safety meeting been held?4 . Have equipment and tools received a safety inspection?5 . Has the hazard analysis been reviewed?6 . Have PPE requirements for the activity been established?-las the area of work been defined?8 . Has stained soil been located?9 . Are required materials for spill containment available?10 . Have sampling locations been established?11 . Have procedures for handling IDW been defined?12 . Have procedures for cleaning and decontamination been established?Comments :_C ys m MafiageDateContract: DACA95-97-D-0010, D .O . 0004Project: Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island, Alaskaure of Work : Debris Removal CLIN : 2Inspection : PreparatoryRelevant Specifications : SOW 1 .3.1, SOW Table 2, 02050, 01130, 01450Submittals : Work Plan, Health and Safety Plan, Environmental Protection PlanInspection ChecklistNotObsrvdItemYes No1 . Have all required submittals been approved?0002. Have the applicable section of the statement of work and specifications beenreviewed?0003 . Has a safety meeting been held?4 . Have equipment and tools received a safety inspection?5 . Has the hazard analysis been reviewed?6 . Have PPE requirements for the activity been established?las the area of work been delineated?Has the scrap to be removed been identified?9 . Are personnel operating cutting equipment fully trained?10. Have staging areas , haul routes, and collection points been established?11 . Have hot work procedures and areas been identified?12 . Have weighing procedures been established?13 . Has site control been established?14. Have procedures for cutting , loading , transporting , and off-loading metal debrisbeen reviewed?Comments:CQCste4,ManagerDatec Jk (/Weigh TicketDebris Removal and Containerized HTW Removal , Gambell AlaskaTicket #SiteDateCollectedDateLoadedDateWeighedCount:Description_BDRSSOtherHTWCSGrossWeightTare WeightNet WeightNetWeightTare toConnexGross toTicket #DateCollectedDateWeighedSiteConnexInitialsConnex#DateLoadedBDRSSCount :DescriptionHTWCSOtherGrossWeightTare WeightNet WeightNetWeightTare toConnexGross toConnexDateCollectedDateWeighedTicket #SiteInitialsConnex#DateLoadedCount :DescriptionBDRSsOtherGrosslWeightTare WeightNet WeightNetWeightTare toConnexGross toConnexInitialsConnex#HTWCSCONTRACT LINE ITEM , TRACKING SHEETAREA 8DebrisContract Line item 2total WtinconnexDateNet Wt loadedTare inConnex # connexDateNet Wt loadedtotal WtTare in inconnexConnex# connexDateCount Net Wt loadedtotal WtTare In InConnex # connex connexDate DateWt Ticket # Collected Weighed D escription CountCurrent TotalHTWContract Line item 3Date DateWt Ticket # Collected WeighedCountDescriptionurrent TotalStained Soil Contract Line item 4Date DateWt Ticket # Collected WeighedDescriptionCurrent TotalPage 1Weight maryDebris removal and Co, arized HTW Removal~~ Debris-TaWaI Weight toSites Weight DateHTWTable 2 Weight toWeight DateSite 2160020Site 3770600Site 4/Area 4A5410i2140 jSite 4/Area 4B9052230Site4/Area 4D10000Site 53150site 5 and 355100Site 63500Site 71500Site 81150006200Site 1013002300 1Site 1210012550Site 13300,~, __-0 .Stained soil Contaminated SoilWeight to Weight toDateDateArea betweenTotals 127255Percent of Weight00%1614000%194990'0140000v4L't i01', 0%Page1As00%of :7/18/99,10:19 PMContract DACA95-97-D-0010, D .O . 0004Project Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island, Alaska.ure of Work : Sampling CLIN : 4, and 5Inspection : InitialRelevant Specifications : 1450Submittals : Sampling and Analysis PlanInspection ChecklistItemesootObsrvd1 . Are sample points correctly located and marked?(ElEl2 . Do collection methods meet requirements of analysis ordered?•0El3 . Has a safety meeting been held?Q'El04 . Are proper precautions to prevent cross contamination being followed?i005 . Are field notes documenting sampling locations being made?Q'006 . Is the proper PPE being worn?Q007 Are clean sampling tools being used?Q'0Elb . is only Stained soil being sampled?15009 . Are measurements of sample locations being made?QEl010. Is the proper sample i .d. used?L10El11 . Area procedures for handling IDW being followed?L 'El0El012 . Is the COC form being filled out with all the proper data fields?Comments :iAgolfftemManagertoEnvironmental Quality Control/Quality Assurance Report(EA AISI)2)Contract Number I Delivery Order Number UPC / Pro1ect TitleOACASS- 97-D-00101 0.0. 0004 Debris Removal and Contalnertzed Hazardous and Toxic Waste RemovalCQC Report Number Date or Time Period Location and Team99-0157120199Gambell,AlaskaWeatherConditionsContractorTemp Low 47 Temp HI $2Oil Spill Consultants, Inc.Conditions Cloudy a m Sunny . o.m10-21 KnotsWind SpeedQuality Control Inspections Performed This Date (Include inspections . results. deficiencies observed, and corrective action)Preparatory 0 se" attached checktlstInitial a se* attached checklist HTW RemovalFollow-UpaSamplingYes OWas the deficiency tracking list updated this dateNoField Sampling and TestingHas field testing been performed this date ?Type of test Method/MatnxHave Data Quality Objectives been achieved'Have Samples BeenType of TestN/AYes a No 0Quantity of samples ResultsYesONo0Collected for Laboratory Analysis?EPA Test Method/Matrix Quantity of SamplesYesOMooSee Chain of Custody Form and Field notes AttachedN/A°YesONo0Have required amount of ac trip blanks and nnsates been achieved ?Have appropnate QC laboratory tests been ordered ? ( matrix spikes . method blanks. surrogates , reference standards . etc .) NIAOYesaNoON/A°YesDNoOHave QA and QC samples been collected in the specified quantity? Not required by Delivery OrderIAO YesONoONHave samples been property labeled and packaged ?Health and SafetyLevel A 0 Level B 0 Level C a Level O a NIAOWorker protection levels this date:Yes 0 NoeWas any work activity conducted within a confined space 'Yes O NoeWas any work activity conducted within an area determined to be immediately dangerous to life and health 'Were approved decontamination procedures used on workers and equipment as required' Yes 0 MooSafety Comments : ( Include any infractions of approved safety plan , and include instructions from Government personnel . Specify corrective action taken )The safety meeting addressed the hazards of handling landing mat . Workers loading landing mat into connexes whilestanding in dose proximity to each other must exercise caution to avoid striking each other with the jagged metal . Thecorrect PPE and material collection procedures for drums and batteries was also discussed . This was in preparation forthe removal of HTW from Area 12 that would start that day .QAR SAFETY COMMENTS:P 2tC r+,~0rv P +`t_C0-fe,e r3GT - !},~`^^'s TS( - 4 .iS . I`to , 1e--BL .cy . < 0r35c-`rt ..C T2)L "e-rr rv -r7t X . - EYLIEnvironmental Quality Control/Quality Assurance Report(ER 4 tS .1 . 3021Continuation Sheet3 k Activities Performed This Date,eference (HAS 10 INrech Spec s)QuantityActivity & LocationHTRW Removal (HAS t0 0022 . 02050) initial HTW removal on Area 12 . drum dumpsouth of Troutman Lake . Drums and batteriesremoved .ofdrums at this site collected35 % of drums at this site weighed . 4 .448 lb b dateStained soil associated with drums and batteries 75% of stained soil at this site collectedat Area 12 excavated . containerized and weighed 50 % of stained soil at this site weighed . 2.594 lb to dateStained Sod Removal ( NAS ID 0019 . 02050)Debris Removal (HAS ID 0020 . 02050)75%ContractorArea . 12 . small amounts of non-HTW metal not yet weigheddebris segregated from drumsManpower and EquipmentLaborCtassmcadonPry ManagerCOC System ManagerSuperintendentArcheologistNumber11ManHours1313EquipmentType4 wheelerCat 426 loader111310ArgoNodwell21160Laborers18Total Hours1272133PickupCat 966 Loader100056OpalNumber31Hours Used364Total Hours .hstrucUons Given by the Government to the Contractor ( Include names, reactions , and remarks .)Verbal° Written QQAR approved the substitute of an Argo for the Archeologists sole use in lieu of the four -wheeler identified by themodification extending the archeologists time on site .QAR directed that the cans of solidified paint found during the cleanup of Area 12 (the drum dump south of TroutmanLake) were to be left on site .Yes 0Yes 0Yes 0Work Progress Are there any Contractor caused delays or potential finding of fact?Are there any Government caused delays or potential finding of fact?Are there any unforeseeable or weather related delays?NoNoNoRemarks ( Include any wsitors to project and miscellaneous remarks pertinent to work)With only approximately 50% of the drums in Area 12 weighed, the recorded weight to date of 4,484 lb already exceedsthe Delivery Order estimate of 2,550 lb for that site . Visual estimates of non-hazardous metal debris exceed the 100 lbestimate in the delivery order .The Archeologist coordinated with Suzanne Beauchamp, Project Manager for the Corps of Engineers, concerning detailsof artifact/burial Standard Operating Procedure to be agreed upon between the Corps and the to City of Gambell .Sivuqaq Inc, and Gambell IRA . Later that day he briefed the contractor's Project Manager, Randy Easley .During a Reconnaissance of Area 4, (the mountain top) conducted later that evening by the Archeologist , the OAR andthe Contractor ' s Project manager, several graves, one rockshelter with a hearth , were discovered along with militaryfeatures . The contractor's Argo mechanic also noticed one burial at which the bones had scattered .I certify Chat the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this period were in strictwnpliarlce with ft contract plans and specifications ezcept,as noted above .JtLality Control Manager SynatureGovernment Quality Assurance Commentstheconcurs withAdditional comments or exceptionst)( 3hfi Lr/NY!~L7Date/~4QCfitc"to`fDreport?YesRJ1 0 .J C ct - f- c '\ jwX ‚ r>W LL_l_1 .n+~`EbIL./N+'T1-QNo 0Pk ‚ N C4 4cC Nyc-h,W, H+o35 L '-'C'. 4& ct4,azttC~S :$ + TZ ao01CoC<QwmM'= ~~Uin .. aamMQƒa Nw.o/ QCi7RequiredAll~~‚C - -S!7-19JSoiSd- M-ooc- SzRelinquished by : (Printed)(S nature)Relinquished by : (Printed)(Signature)Dispatched by : (Printed)(Signature)Method of ShipmentComments:7110 y9it' 3oDateTimeReceived b : (Printed)(Signature)Received by: (Printed)S nature )Received at laboratory by:Condition of ContainersGood Fair Pooreceived Temp :OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate :1999Activities Planned :Briefer:Time :C~ZG L`'Briefing Location :L- - ~- ?~Topic :r ,-Ir, ; ; 2~plc,Topic: Tr (n ) P G~ Ov 4Topic:Briefer :Topic :Topic :Topic :AttendeesJhfSite4 Ithand Safety Officer :,Date: / / 1999,e /C/ /Ylc nn 470-0,,off, .r/we Jefo,07 :~s ,y/--//o 70~- /~yG/ir~H'7PContract: DACA95-97-D-0010, D .O . 0004Project: Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island , AlaskaFeature of Work : Drum Removal/HTW CLIN : 3Inspection : InitialRelevant Specifications : SOW 1 .3.1, SOW Table 2, 02050, 01130Submittals : Work Plan, Health and Safety Plan, Environmental Protection PlanInspection ChecklistYes NoItemNotObsrvd1 . Is the proper PPE being wom?2 . Is the work being conducted a safe manner?3 . Is spill containment being place correctly?4 . Are drum inspected for liquids before the drums are disturbed?5 . Are haul routes being maintained in a manner safe for vehicles?6 . Are appropriate lifting and tie-down methods being used?1PMR7 . Are staging areas fully-lined and liquid tight?8 . Are generators grounded?D9. Is all fuel -powered equipment within lined areas?10 . Are GFI' s in use?DD11 . Are drum liquids and solids removed before rinsing?E'DD12 . Are drum solids and liquids properly contained?0'DD13. Are drums being triple rinsed?D0014 . Is hot water being used for drum washing?DEl.4015. Is drum washing area fully contained and liquid tight?DDEr16. Are washed drums free of any residue?Ga'DD17. Are rinsates being properly collected for treatment .DDEn18 . Are drums fully crushed?El19. Are drum weights being entered on the correct ledger?_: ~ /7OW CQC System ManagerDea' DDEnvironmental Quality Control/Quality Assurance ReportIER 41 .I‚kT_1SUPC/Prolect TitleContract Number / Delivery Order NumberDebris Removal and Containerized Hazardous and Toxic Waste Removal^ACA8S.97 -O-00101 D.0 . 0004Data or Time Period7121199C Report Number.016Weather ConditionsTemp Low 43 Temp HI 49wind Speed3- 10 KnotsLocation and TeamGambell , AlaskaContractorOil Spill Consultants, Inc .Conditions SunnyQuality Control Inspections Performed This Date (Include inspections results deficiencies observed . and corrective action )Preparatory 0 s . attach.d checklisttinitial 0 s .. attach ed checklistFollow-Up0Yes 0 NoWas the deficiency tracking list updated this daleField Sampling and TestingHas field testing been performed this date?TypeoftestMethod/Matrix Quantity of samplesYes 0 NoResultsHave Data Quality Objectives been achieved ? N/AHave Samples Been Collected for Laboratory Analysis?Type of TestesOo0YesONoOQuantity of SamplesEPA Test Method/MatnxWAOYesONoDHave required amount of QC trip blanks and nnsates been achieved )N/AOYesONoDHave appropriate OC laboratory tests been ordered 7 (matrix spikes . method blanks. surrogates . reference standards . etc.)N/ADYesDNoDHave QA and QC samples been collected in the specified quantity? Not required by Delivery OrderN/ADYesONoDHave samples been property labeled and packaged ?Health and SafetyLevel A 0 Level B 0 Level C 0 Level D ° WADWorker protection levels this date :Yes0NoOWas any work activity conducted within a confined space ?Yes0No°Was any work activity conducted within an area determined to be immediately dangerous to life and health ?Yes0MooWere approved decontamination procedures used on workers and equipment as required?,fety Comments : ( Include any infractions of approved safety plan , and include instructions from Government personnel Specify corrective action taken .)ne safety meeting addressed the continuing hazards of the large earth moving trucks on the roads throughout theproject area . All personnel were instructed to yield right of way to these vehicles at all times . Drivers were cautioned tomaintain a safe travel speed while transporting debris . Debris falling from the vehicles while hauling must be avoided .The superintendent directed that chocks be made for ATV-drawn trailers . These trailers must be chocked while parkedon sloped terrain .A water heater was identified in west beach area (Area 8) . The item was listed in the Delivery Order table as a "metaldebris" item . Workers observed crumbling refractory material spilling from the unit . The CQC contacted the QAR todetermine if the item had been previously been examined for asbestos . The OAR directed that the water heater be left inplace pending a determination of asbestos content .QAR SAFETY COMMENTS :T&~ArV isATDG-v'cC- tAleiE lp Awf .v G C4 ._M v _ s L ;J_0 T 4*_~C1P~Uitor`'1/oT130r NLock(_' A-D-A~~c .NG,c71e A55 v Jc1 r. il-N-c v e r D Th C-1} 5 6 rp-4t+ t C-i4 5 eC-ZV I . Tu t2 JOt_; S H A t/C Br~V,,L,ESr , cAD5 .'5v- 1-14AT 5o4 .7t' lt?1r.JO . 1 'C4 5 AeC- Nt L _7C-ID 110Ft~ T`~CPcf~`TJC t iw ',N‚4gtS wA5'INur) F-t 5 wCR/Q-Rcr04')4DWc1ST LNO-7-Acve-.J ntg CA - -,A-t. 4Iofk-"hEnvironmental Quality Control/Quality Assurance Report(ER 413 .1 .302)Continuation SheetWork Activities Performed This DateReference (NAS ID s/Tech Spec !) Activity & locationQuantityHTRW Removal (HAS ID 0022 . 02050) HTW removal on Area 12 . drum dumpsouth of Troutman Lake . was completed today100% of drums and other HTW at this site coltcted100 % of drums and KTE . 6 .873 lb lo dateStained Soil Removal (NAS ID 0019 . 02050)Debris Removal ( HAS 10 0020 , 02050)Exavation of Stained soil associated with drumsat Area 12 was completed todayArea , 12 . small amounts of non-HTW metal100% of stained soil at this site collected100 % of stained Sol at this site weighed . 5 .754 tb to date100 % of metal debris at this site collecteddebris segregated from drums was completed todayManpower and EquipmentLaborClassificationProtect ManagerCOC System ManagerSuperintendentArcheologistOperatorLaborersContractor100% of metal debris at this site weighed . 798 lb to dateNumber111ManHours31213EquipmentType4 wheelerCat 426 loaderArgo112Nodwell101272124PickupCat 966 Loader101266816Total HoursNumber312Hours Used36212Total HoursVerbal ° Written 0Instructions Given by the Government to the Contractor (Include names, reactions, and remarks .)The QAR directed that the water heater found on Area 8 be left in place pending a determination of Asbestoscontent .(see safety remarks)Yes 0Yes 0Work Progress Are there any Contractor caused delays or potential finding of fact'Are there any Government caused delays or potential finding of fact'Are there any unforeseeable or weather related delays 'Yes 0NoNONoRemarks (Include any visitor to project and miscellaneous remarks pertinent to work .)HTW removed from Area 12 totaled 6,873 lbs . Most of this was drums and batteries . This exceeds the Delivery Orderestimate for that site of 2,550 lb . 798 lbs of non-hazardous metal debris was also removed, exceeding the 100 lbestimate in the delivery order .Mr . Easley, the Contractors Project Manager left the site today .The Archeologist spent most of the day in Area 4 (the mountain top) with the, USACE village liaison Bert Oozevasouk .The Archeologist recorded : 1) human skull fragment within military dump at burned radar dish site on edge of cliff aboveold village well, along with military debris, and reburied it, 2) closed grave box with associated wood sled (first reported itDaily Report of 7/20/99) and nearby human phalange, reburied phalange ; 3) open grave box with associated wood sledand ice probe (first reported in Daily Report of 7/20/99) ; 4) open grave box with associated wood sled and widelyscattered human bones ; 5) two isolated human phalanges .I certify that the above report is complete and correct and that all materials and equipment used . work performed and Mists conducted during this period were in strictcompliance with the contract plans and specifications er*ept as noted aboveDateQuality Control Manager Signature2T ,QzEnvironmental Quality Control/Quality Assurance ReporttER 415 - 1 .302)Continuation SheetGovernment Quality Assurance Comm.ntsConcswltftAdditional comments or exeptions .the. Co+~T.+-.vt1t- C-tom r r ,ALU t--'t-C'5 SS EA- (- A-report?' Y A- : c t ~.t R Z" , t'V!3;>t')7 I t_ )754- oytc r. ..cv2 tG.r 5 $c't2~ biz ' c ;`-~~; t ctiv S ‚t/h ct/ECT tS(,U LJ h/lh CM-v,h~ :7cY2 ƒir4v~6 wN ., --r- rv r> -> -Tl S w .Pts.LI GA- r vzC,5 1hn ,K- ~,'M v (,,g t-7,->bs L. '<w r,-70-,.'k g4t ~_ t1 f. LLz t -rr- A=z3.2 SI-T A,2-,F Yt S t'.TE{t~cy` .,--_LI rU s /~ ~ .~'T c: C Z .A rC l.. ..-'7 ` >~A-,A---> TH r SpvL .tT trt'T4fiec,/ s A ) vz/t Y / r-~Wf .aDatei/ -a,;I. C. K .Supervisor's Initial Date;3 1,Weight SummaryDebris removal and Containerized HTW RemovalHTWDebrisMContaminated SoilStained soilUUAActualWeight toDateMSitesActualWeight toDateActualWeight toDateVActualWeight toDateSite 2160020Site 3770600Site 4/Area 4A54102140Site 4/Area 4B9052230Site4/Area 4D10000Site 53150esite 5 and 355100Site 63500Site 71500Site 811500025419620040251259Site 101300023007170Site 12100798255078296302Site 13300343000104000Totals 127255 26560 1614021%Percent of Contract Wt12571 40000 7561 104000 078%19%0%Page 1As of 7/ 22/99 .9*35 PMOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage, Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title :Debris RemovalRemovalProject Site Location :Gambell , AlaskaDate:1999Time :,.' /-1and Containerized Hazardous Waste and ToxicBriefing Location :Activities Planned :Briefer:Topic :Topic :Topic :-Briefer:Topic :Topic :"t~I. .Topic :AttendeestI &AA/I,Site Health/and Safety Officer : /1 J/ E ~~ /11Date :1999HOT WORK PERMITContract : DACA95-97-D-0010 . D . 0 . 0004Project: Debris Removal and Containerized and Hazardous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island , AlaskaAType of Work :HeatProducingLocation :A / tDevice(-Operator :IFire Guard :Scheduled Work Date :ZTime Start: / ' '- ` 1 %Time Finished :The Checklist Below Was Reviewedr .' _z Y- -'Date : //‚_ / S HSO :SuperintendentDate :'COMPLETE IMMEDIATELY PRIOR TO WORKHot Work ChecklistItemN /A Yes No1 . Are all flammables and at lest 50 ft away?2 . Is the operator fully qualified to operate the equipment?3 . Has the Fire Guard been identified and briefed to observe the area for 1 hour after work is Zcomplete?04 . Has emergency communication procedures been0checked?95 . Is and ABC extinguisher present and is it in working order?6 . Have the tools and equipment been inspected for safety?7. Is the correct PPE being worn?8 . Has the area been checked for flammable or explosive vapors?Have containers been checked for explosive/ flammable residue or vapors?(drums and tanks)10 . Are torch hoses purged before lighting (torches only)?n11 . Are nozzles and hoses in good repair? (torches only)lf-' 0 00 uCOMPLETE AFTER WORKTime Start :t-Superintendent :[Time Finished :~~Ll C' Pl'"Date :Ar L Z /___ -Z,15HSO :Fire Guard Released :/ ~C ;' .! '~ 1~'10,Date : 'Environmental Quality ControUQuality Assurance ReportII C i t- i 4,' tContract Number / DeliveryOrderNumberUPC /Protect TineDACABS- 97.O-00101D . O. 0004 Debris Removal and Containerized Hazardous and Toxic Waste RemovalCOC Report Number Date or Time Period Location and Team99-0187/23199WeatherConditionsTemp Low 45 Temp Ht 47Wind Speed27 .36 KnotsGambell , AlaskaContractorConditions Cloudy . Blowing RainOil Spill Consultants, Inc .Quality Control Inspections Performed This Date !Include inspections results deficiencies observed and corrective action 1Preparatory0 we attached checklistInitial0seeattach .d checklistFollow-up 0NO INSPECTIONS TODAYYes 0 No 0Was the deficiency tracking list updated this dateField Sampling and TestingHas fieldType of testtestingbeen performed this date? Yes 0Mettiod/Matnx Quantity of samples ResultsNoISNO FIELD TESTING TODAYH a ve Data Qua lity Objectives been achieved'N/AYesOHave Samples Been Collected forLaboratoryType of Test EPA Test Method/ MatrixNo0Analysis?YesOQuantity of SamplesNooNO SAMPLING TODAYHave required amount of QC trip blanks and rtnsates beenachieved)N/AOYeSONoDHave appropriate QC laboratory tests been ordered 7 (matrix spikes . method blanks . surrogates . reference standards . etc i N/AOYesONOOHave QA and QC samples been collected in the specified quantity? Not required byDeliveryOrderWAOYeSONOOH ave samples been properly labeled andpackaged?N/AOYes0No0Health and SafetyWorker protection leveis this date Level A 0 Level B 0 Level C 0 Level 0 ° WAOWas any work activity conducted within a confinedspace')Yes0No°Was any work activity conducted within an area determined to be immediately dangerous to life and health Yes 0 NoOWere approved decontamination procedures used on workers and equipment as reguired7 Yes 0 NosSafety Comments (Include any infractions of approved safety plan . and include instructions from Government personnel Specify corrective action taken ,At the safety meeting, the Argo operators video was shown to the crew . The superintendent address the importance ofoperating these machines within their designed performance limits . The difference between Argos and four wheelersincluding the wider stance and lower ground clearance was emphasized .A high wind warning was issued later in the day as peak gusts approached 40 knots . Personnel were advised to useextra caution and be prepared to seek shelter if necessary .GAR SAFETY COMMENTS :14, 0 q-A-IEnvironmental Q uality C'untroUQuality Assurance ReporttER 4'5 r Jc:Continuation ShcctWork Activities Performed This DateReference (NAS ID #/Tech Spec a)Activity & LocationQuantityContractorLocate S ites(NAS 10 0011)The archeological site added to Site 8 was surveyed stakedand reviewed by the OAR100.6 of sites surveyed and one new site addedHTRW Removal (NAS ID 0022 02050)6 Tar barrels were removed from Sited the west beach6 235 ;b removed to dale from this sireDrums and 2 Tanks removec from Site 3 at the mountain base653Ibs of HTW removed This site r96%Drum removal was completed on Sree 6 North of the High School100% complete 2 418 lb of debris removedStained Soil Removal ( NAS ID 0019. 02050)Debris Removal (NAS ID 0020 . 02050 )Stained Soil removal continued on Site 8 the west beach6.235 lbs of stained soil at this site collectediweighedDebris removal was completed except for final pickupon Site 3 at the base of the mountain95% of metal debris . 159 lbs at this site collectedDebris removal was completed except for final pickup95% complete Debris was weighed with Site 3 Debrison Site 2 east of the mountain on the gravel MatsDebris removal was completed except for final pickupon Site 6 North of the High School95'4 complete 7897 lb of debris removedDebris removal was completed except for final pickupon Site 7 west of the High School95% complete No measurable debris recoveredManpower and EquipmentLaborClassificationProtect ManagerCOC System ManagerNumber11ManHours312EquipmentType4 wheelerCat 426 loaderSuperintendentArcheologistOperator111131212ArgoNodwel lPickup4113604Laborers784Cat 966 Loader110Total Hours124Number31Hours Used363Total Hours89Instructions Given by the Govemment to the Contractor (Include names . reactions, and remarks) Verbal 0 Written 0After a tour of the historic site between the north end of the runway and the village , and west of the village road, by theQAR, Superintendent , and Project Archeologist , the Archeologist determined that the surface debris could be recoveredwithout significant archeological impact . The QAR directed that the boundaries of Site 8 ( the West Beach ) be expandedto incorporate the historic site . The QAR furhter directed that work must be performed by local labor and theArcheologist would supervise . Mechanical excavation would not be permitted , with all debris collection being performedby hand .Work Progress Are there any Contractor caused delays or potential lending of fact?Are there any Government caused delays or potential finding of tact?Are there any unforeseeable or weather related delays?Yes 0NoYes 0Yes 0NoNoRemarks ( Include any visitors to project and miscellaneous remarks pertinent to work)High cross winds kept planes from landing . This prevented a USACE staff visit .The CQC requested a preparatory inspection for debris , soil, and HTW removal. in Sites 10 (the trail system and tundra)and Site 4 (the mountain top) for the morning of 7/26 .The archeologist coordinated grave protection and archeology procedures with USAGE Project Manager SuzanneBeauchamp via telephone . Later in the day he monitored debris clean-up in Area 3 and reburied six human bones withProject Liaison Bert Oozevaseuk as villager witness .I certify that the above report is complete and correct and that all materials and equipment used work performed and tests conducted during this period were in strictcompliance with the contract plans and specifications except as noted aboveQuality Control Manager SI nature7fI,oat*'iEnvironmental Quality Control/Quality Assurance ReporttER 415 t 30: ;Continuation SheetGovernment Quality Aeaurance CommentsConcurs with the OC report/Yes61No0Additional comments or exceptionsME7 4-La` -C.>CfOAR SignatureQ-% SSCt ‡~:"~~N;,, A-M r-~- l trz . . -dry' T.. A Q U L t iAP irr-z-~~1' sG~ti~~c`'c :~_ , PS4 - t` CiwVde J~rtc 1 la :&T1t- Ai t ri.r~~~r~a)-Date /`' J7Supervisor' s Initial DateWeight SummaryDebris removal and Containerized HTW RemovalHTWDebrisuAVctualWeight toNSitesUAUA0 3DateUctualWeight toL0 3CContaminated SoilStained soilVA03DateU ..Site 21600Site 3770Site 4/Area 4A54102140Site 4/Area 489052230Site4/Area 4D10000Site 53150Area betweensite 5 and 355100Site 6350Site 7150Site 811500025419Site 101300Site 12Site 130-UActual(aWeight toDateUo 3ctualWeight toDate20159241860006530104000789706200623524700230071701007982550782963023003430000Totals 127255 29137 16140 23331 40000 8772 104000 0Percent of Contract Wt23%145%22%0%n‚,, . .,In- r if7/7/O 454 PMOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage . Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location :Gambell , AlaskaDate : 3 1999 Time : OC/ Briefing Location :lActivities Planned :Briefer :Topic:alioAN All'Topic :Topic :Briefer :Topic :Topic:Topic :0Site Healthand Safety Officer :Date :t1999HOT WORK PERMITContract: DACA95-97-D-0010, D .O . 0004Project : Debris Removal and Containerized and Hazarc!ous and Toxic Waste RemovalLocation : Gambell, Saint Lawrence Island, AlaskaType of Work :HeatProducingLocation :49&kDeviceiOperator : --~Fire Guard :1~I~~/,21 -7?" P/I Time Finished :Tire Start :S-.}!Scheduled Work Date :The Checklist Below Was ReviewedDate :7 / Z HSO :Superintendent:Date: 4YCOMPLETE IMMEDIATELY PRIOR TO WORKHot Work ChecklistNIAItem1.Are all flammables and at lest 50 ft away?2.Is the operator fully qualified to operate the equipment?3.Has the Fire Guard been identified and briefed tocomplete?4.Has emergency communication procedures been checked?5.Is and ABC extinguisher present and is it in working order?6.Have the tools and equipment been inspected for safety?7.Is the correct PPE being worn?8.Has the area been checked for flammable or explosive vapors? ,09.Have containers been checked for explosive/ flan mable residue or vapors? [~(drums and tanks)~J=-:a for t hoi it aft‡ r work is I~011 . Are nozzles and hoses in good repair? (torches oily)COMPLETE AFTER WORKTime Finished:_Superintendent :VIZ,Date :Du10 . Are torch hoses purged before lighting (torches only)?Time Start:Yes No\ Fire Guard Released :__SgO:O1Environmental Quality Control/ Quality Assurance ReportI rit J1tt -w‚,Contrail Number / Delivery Order NumberUPC/Project TitleDebris Removal and Containerized Hazardous and Toxic Waste RemovalOACA85- 97 .O`O010/O .O . 0004CQC Report Number99-019Date or Time Period7124/99Weather ConditionsTemp Low 42 Temp HI 47Wind Speed10-21KnotsLocation and TeamGambell , AlaskaContractorConditions Ctoudv . intermittent rainOil Spill Consultants, Inc .Quality Control Inspections Performed This Date (Include inspections results deficiencies observed and corrective action IPreparatory C) S" attached chocALWIInitial 0 s.. .sacred ch.ckllstFollow-Up 0NO INSPECTIONS TODAYWas the defic iency becking list updated this dateYes 0Field Sampling and TestingHas field testing been performed this date ?TypeoftestNoYes 0 NoMethod ,tl4atrix Quantity of samplesResultsNO FIELD TESTING TODAYH a ve Data Qua lity Obj ectives been achieved'N/AHave Samples Been Collected for Laboratory Analysis ?Type of Test EPA Test Method/MatrixYesONODYesDNo°Quantity of SamplesNO SAMPLING TODAYHave required amount of OC trip blanks and rinsates beenachieved?N/AOY .sDNoOHave appropriate OC laboratory tests been ordered' (matrix spikes , method blanks surrogates . reference standards etc i WAQYSDNODHave OA and OC samples been collected in the specified quantity ? Not required by Delivery Order WAQYesDNoOH a v e samples been properly label ed and packaged ?N/ADYesONoDHealth and SafetyWorker protection levels this date .Level A D Level B D Level C D Level D ° WADWas any work activity conducted within a confined space ?Yes 0 NowWas any work activity conducted within an area determined to be immediately dangerous to life and health? Yes D NoeWere approved decontamination procedures used on workers and equipment as required) Yes 0 NomSafety Comments (Include any infractions of approved safety plan , and include instructions from Government Personnel Specify corrective action taken )The dangers of high winds were discussed at the safety meeting . The potential for serious injury from wind-blown objectswas emphasized . The Superintendent also stress precautionary steps to take in the event of high winds These includedlimiting activities that involved sheet metal and other material that could create hazardous conditions during high winds .The Need to stay dry while working and the dangers of hypothermia was also discussed .OAR SAFETY COMMENTS :tit m S l+tititZ-~C ~~ . l'L A -Cnr' ^t )' ? (St;c-TV C7 L d'Q 16 tLZ~y& It-Pl'~ .i7 rA A-rS dt-4C-X..IRiuu7SOI .N^gr1 e~Environmental Quality Control/Quality Assurance Report(ER 415-1 -302)Continuation Sheet'Nor* Activities Performird This DabReference (NAS 10 a(Tech Spec a)HTRW Removal (HAS ID 0022 . 02050)Stained Soil Removal (NAS ID 0019 .02050)QuantityActivity 6 LocationDrums and 2 Tanks removed from Site 3 at the mountain baseStained Soil removal started at oil spill site in Site 2Contractor1 150 ib of HTW removed This site 100%24 .985 lb of stained soil at this site OolleCledtw"he(lWork halted when extensive Contamination was discoveredDebris Removal (HAS ID 0020. 02050)Contaminated Soil (HAS ID 0016 , 02220)Manpower and EquipmentLaborClassMcationDebris removal was completedon Site 3 at the base of the mountain100% of metal debris removedDebris removal was completedon Site 2 east of the mountain on the gravel flats100% completeDebris was weighed with Site 3 DebrisDebris removal was completed except for final pickupon Site 6 North of the High School100% complete7897 lb of debris removedDebris removal was completed except for final pickupon Site 7 west of the High School100 % completeNo measurable debris recoveredDebris removal started on Site 5 the cable areaup the slope east of the High School2,418 lbs removed to date 20 % completeA trail was blazed through the tundra to the MountainTop and through the boulder field to Site 48 Trailimprovements made and field survey made for possiblestaging areasManHoursEquipmentType111117014131212844 wheelerCat 426 loaderArgoNodwellPickupCat 966 LoaderTotal Hours135NumberProject ManagerCOC System ManagerSuperintendentArcheologistOperatorLaborersinstructions Given by the Government to the Contractor (Include names . reactions . and remarks)NumberHours Used314ttt365360010Total HoursVerbal7° Written 0Excavation of stained soil was initiated at the oil spill site near the base of the mountain in Site 3 . It soon was discoveredthat significant amounts of product had penetrated deeper then 3 ft . and laterally greater than 30 ft . An inspection of theexcavation of the site was made by CQC Dave Rein . He suspend the work as it appeared to be beyond the contractintent to removed stained soil associated with drums and other debris . The CQC contacted the OAR Steve LeClerc andwho concurred with the interpretation of the contract and decision to suspend work in that area .Work Progress Are there any Contractor caused delays or potential landing of fact'Are there any Government caused delays or potential finding of fact'Are there any unforeseeable or weather related delays?Yes 0Yes 0Yes 0NoNoNoRemarks (Include any visitors to protect and miscellaneous remarks pertinent to work )Richard Jackson, of the Environmental Engineering section of the USACE Alaska District arrived on site today . He andOAR Steve LeClerc coordinated on technical issues and toured the cleanup sites .The Project Archeologists received a copy of USACE letter to three Gambell government . entities regarding artifact andburial protection protocols . Later in the day he interviewed Cheryl Koonooka about her 1997 4-wheeler accident onmilitary debris . This type of information will be used for project context in the final report .I certify that the above report is Complete and correct and that all materials and equipment used work performed and tests conducted during this period were in strictcompliance with the contract plans and specifications except as noted aboveQuality Control Manager SignatureDate a~ 1Environmental Quality Control/Quality Assurance Report(EP 41 5 .1 302)Continuation SheetGov .mm.nt Quality Assurance CommentsConcurs wrth the DC report?&ddit ;onat comments or exceptions4V tG.c~YesX No 09r _ j/- Si /4.‚4T1 wU (~ c .k t_ h *~ ' / i~cw-~~~7] ' i ttt SLLt`Ir-rt 7OAR Signature~ytit4w''fix: t_ L L.A, A ~'r `> EIL. kS1l.:i.~ 1L rtr, C- rt ~.10Dateb- J A S /1o-) o t.L S r~53c'-*-) -'2h.j CitJ ~ 4q-,l A,iC--"Supervisors InitialDateWeight SummaryDebris removal and Containerized HTW RemovalSitesStained soilHTWDebrisuuco0c -0 3UActualWeight toDateContaminated SoilUMuAActualbc ~-Weight toUDate4-o 3UActualWeight toDateUSite 21600020024985Site 377015960011500Site 4/Area 4A54102140Site 4/Area 4B9052230Site4/Area 4D10000Site 5Area betweensite 5 and 3315Site 6350Site 7150Site 811500025419Site 101300Site 12Site 131040007897574006200623524700230071701007982550782963023003430002418550ActualWeight toDate4c0100000Totals 127255 29137 16140 23828 40000 34331 104000 0Percent of Contract Wt23%148%86%0%Page 1Asof7/25/991254AMOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title :Debris Removal and Containerized Hazardous WasteRemovalProject Site Location :Gambell , Alaska199 9Date :and ToxicTime : Briefing Location :Activities Planned :Topic :Briefer:'N/Topic :Topic :Topic :Briefer :Topic:Topic :rAttendees~IIZ~ l "~~Lti .`~-1 1Site Healthand Safety Officer :Date :1999Environmental Quality Control/Quality Assurance ReportIER 41S.1-10:1Contract Number I Delivery Order Number UPC/Pro1ect TideDACASS -97-O-001 WO . O. 0004 Debris Removal and Containerized Hazardous and To xic Waste Removal'QC Report Number Date or Time Period Location and TeamGambell , Alaska9-0207/25199WeatherConditionsContractorTemp Low 45 Temp Hi 47Oil Spill Consultants, Inc .Wind Speedcalm-3 KnotsConditions Cloudy.Quality Control Inspections Performed This Date (Incude inspections results deficiencies observed, and corrective action )PreparatoryInitialD she attached checklist0seeattached checklistFollow-Up a Follow up inspection of drum processing and loading identified incompletely washed drtms(See deficiency tracking form 001)Was the deficiency tracking listupdatedField Sampling and TestingHas field testing been performed this date ?Type of testthisdateYesaNo0Yes0NoMethod/AAatnxQuantity of samples ResultsNO FIELD TESTING TODAYHave Data Quality Objectives been achieved ?HaveYesOWASamples Been Collected for Laboratory Analysis?Type of Test EPA Test Method /Matnx Quantity of SamplesYesOMooNoONO SAMPLING TODAYHave required amount of OC trip blanks and nnsates been achieved 'N/AOYesONOOHave appropriate OC laboratory tests been ordered ? ( matrix spikes . method blanks , surrogates . reference standards. etc I WAOYesDNoOHave OA and OC samples been collected in the specified quantity? Not required by Delivery Order WAQYesONoOHave samples been property labeled and packaged )WAOYesONoDHealth and SafetyLevel A 0 Level B 0 Level C O Level D a WADWorker protection levels this date .Was any wortt activity conducted within a confined space? Yes 0 NoaYes 0 NoaWas any work activity, conducted within an area determined to be immediately dangerous to life and health ?Were approved decontamination procedures used on workers and equipment as required ?Yes 0 No°Safety Comments ( Include any infractions of approved safety plan . and include instructions from Government personnel Specify corrective action taken )The superintendent addressed the need for extreme caution while operating ATVs near the cliff edge at the top of thenountain . This was in connection with the preparations that were being made for the work in Site 4 at the top of themountain . Safe speeds and loading of ATV trailers while transporting debris was also discussed .QAR SAFETY COMMENTS :c)A ;L_l~w t t L "l tC/~ ct~ CJ r\ .5..1 7W"OV;, r L tS1r716.;I rt.} tv(S~y t: (._r)t, it ~y~5* ti4.(e r-STEL}3v' :,-'~ h-4'_t St~ , F'~Zl vyv i d4Y1h. t r. . .t i7 tlLL_t:~I-z Cƒ ~-l~L i1~Ry)tS i‚ 4 D ~~ t3AT Y ateL3~~~ r F~ ;v< .~P t.= jIEnvironmental Quality Control/Quality Assurance Report(ER 415- 1 .3021Continuation ShirtWork Activities Performed This DateReference (NAS 0 s/Tech Spec 6) ActivityHTRW Removal ( NAS 0 0022 . 02050 )&LocationQuantityDrums removed from Site 10 . off the roads near the 5 .990 lb of HTW removed to date This site 20%south end of Troutman LakeDebris Removal ( NAS 10 0020-02050) Previously-stockpiled debris from Site 8 ( the west beach )was weighed and loadedContaminated Sod (NAS ID 0016. 02220)Contractor39 .621 lb of HTW removed to date This site 60%A trail work continued onn trail improvements to the MountainTop and through the boulder field to Site 48Manpower and EquipmentLaborClassificationProtect ManagerCQC System ManagerSuperintendentArcheologistOperatorLaborersNumber11ManHours012EquipmentType4 wheelerCat 426 loader111312ArgoNodwell4136011284Pickup1127Cat 966 Loader110Total Hours .133Number31Hours Used360Total HoursInstructions Given by the Government to the Contractor (Include names , reactions . and remarks )Verbal94° Written 0The government officially removed the soil dumping area site near the base of the mountain in Site 3 from the project .The QAR confirmed that it was beyond the contract intent of removing stained soil associated with drums and otherdebris . The QAR further confirmed that this was a major spill area that had only been included in the contract because ofgovernment error.Yes 0Yes 0Yes 0Work Progress Are there any Contractor caused delays or potential finding of fact)Are there any Government caused delays or potential finding of fact)Are (here any unforeseeable or weather related delays?NoNoNoRemarks ( Induce any visitors, to project and miscellaneous remarks pertinent to work .)Richard Jackson, of the Environmental Engineering section of the USACE Alaska District departed site today .The Project Archeologist gather taped interviews for background material associated with the final report .I certify that the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this penod were in strictcompliance with the contract plans and specifications except as noted aboveQ uality Control Manager SignatureDateGovernment Quality Assurance Commentsconcurs with Ox OC report?Yes ~( No 0Additional comments or exceptions'rub `'tP~gk12‚(-- ) 4 J4 ctt fl r- l e =--,? 7~,- v r-i TZL,/VOW, G c> Tt-i,< e-;~,t,`)vrc,4,N~+4 > t,tSGt-5UT=Nprcw~("-Ay--)Gtr,‚ M ?h-t-s 1h,4 C.7) t~,J-s na/G,^ Fr~~/cIFkL Lt-t->4 t > .'ra 6, .,c ‚r i3 F-~top,>.l ~-c>~ 11~ . pi d,'Y7' c . ~c~CK CYO)+-7-kit : 1 be 'jruQs'iC .TP tf, C-J-::> !qstPQ~Srit .PtJGSfX'\.L . N r i-9-0 P.c;K t ,A u P kC *t f,,JQAR SignatureZZe U,-4_2ct $~.,vrjDate~‚95supervisors IntUalDateJ.Weight SummaryDebris removal and Containerized HTW RemovalHTWDebrisUAUActualWeight toDateCSitesStained soil3U ,,,Contaminated SoilutoUeoao 3ctualWeight to0 ..Date0MS0Uctuali`ƒMo0 3U ..Weight toDateSite 21600020024985Site 377015960011500Site 4/Area 4A54102140Site 4/Area 4B9052230S i te4/Area 4D10000Site 5Area betweensite 5 and 3315Site 6350Site 7150Site 811500039621Site 101300Site 12Site 130006200749412110230059900100798255078296302300343000550Date10400078972992ctualWeight to100000Totals 127255 43913L 16140 30360PercentofContractWt40000 3249835%188%104000 081%0%7 1')r/00 11) 7'1 DAADeficiency Tracking ReportContract Number I Delivery Order NumberDACA8S97-a-0o1010.O. 0004OTL001UPCIPro eat TideDebris Removal and Containerized Hazardous and Toxic Waste RemovalDate or Time PeriodLocation and TeamGambell , Alaska7/25199Description of deficiency :Inspection of processed drums in connexes 201291 and 205563 noted the following deficiencies1 . A petroleum odor indicated that at least one drum in each connex had been insufficiently cleaned .2 . A bent and perforated but otherwise intact drum indicated that drums had not been deheaded .3 . Excessive dirt on the surfaces of some drum remnants indicated that soil was not being removed before processing .Corrective Action :1 . Connexes to be unpacked .2 . Processed drums to be inspected .3 . Drums requiring deheading and washing to be processed accordingly .4 . Connexes to be decontaminated .5 . Contaminated soil from floor of connex to be containerized for disposal .6 . Connexes to be reinspected .COC SignatureDate L' ;'Government Quality Assurance CommentsConcurs with the corrective action ?Additional comments or exceptions-Ys0No0CQAR Signatu re/_e -?- ') .5-4iRelnspectlon of Corrected DeficiencyCQCSignatureDateGovernment Quality Assurance CommentsDeficiency corrected?Yes 0 No 0Additional comments or exceptionsGARSignatureDateIOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and Toxic RemovalProject Site Location : Gambell, AlaskaDate :1999Time : 1 i22iBriefing Location :7 /VActivities Planned :1111ilkr rTopic-Briefer :L/TopicTopic :Briefer:Topic-.Topic :Topic :Attendees,C-!tQSite Healthand Safety Officer :Date1999Environmental Quality Control/Quality Assurance ReportiLR 41%4- 30]1Contract Number / Oehvsry Order NumberUPC/ Protect TitleDACA5S97-Q00101D . O. 0004Debris Removal and Containerized Hazardous and Toxic Waste RemovalCOC Report NumberDate or Time PeriodLocation and Team99-0217/26/99Gambell, AlaskaWeth. r ConditionsTemp HI 1~Temp Low 45Wind Speedcalm-S KnotsContractorConditions Cloudy, intermittent Ight rain011 Spill Consultants, Inc.Quality Control Inspections Performed This Oat . (Include inspections . results . deficiencies observedd and corrective action)Preparatory ° ii. .each.d ch .ckaatPreparatory inspection for debris, HTW, and contaminated soil removal from Site 4 . the mountain toptuba)O a.e amch.d ctwctJiaFollow-Up ° Fellow up inspectron of drum processing and loading identified open seam in staging area liner(See deficiency DTL 001)Follow up inspection of drum processing showed corrected deficiencies(See deficiencies OIL 001, and DTL 002)Was the deficiency tracking list updated this dateYes ° No 0Field Sampling and TestingHas field testing been performed this date ?Type of testYes 0 NoMethod/Matnx Quantity of samplesResultsNO FIELD TESTING TODAYHave Data Quality Objectives been achieved ? NIAesDHave Samples Been Collected for Laboratory Mafysls?Type of TestYes0EPA Test MethodmilnxooNOQuantity of SamplesNO SAMPLING TODAYWAOYesONoDHave required amount of OC trip blanks and nnsates been achieved)Have appropriate QC laboratory tests been ordered ? ( matrix spikes . method blanks. surrogates . reference standards . etc I N/AOYesONOOHave QA and QC samples been collected in the specified quantity? Not required by Delivery OrderN/AOYasONoOHave samples been property labeled and packaged ?NIAOYes0NoDHealth and SafetyWorker protection levels this date Level A O Level B 0 Level C O Level 0 0 WA0Was any work activity conducted within a confined space ?Yes O NooWas any work activity conducted within an area determined to be immediately dangerous to life and health Yes 0 No°Were approved decontamination procedures used on workers and equipment as required'Yes 0 No°Safety Comments : ( Include any infractions of approved safety plan . and include instructions from Government personnel Specify corrective action taken )The superintendent addressed the need to work with the new local-hire personnel that were added to the project today .These people needed to be integrated into the buddy system , and assisted to insure that they were fully aware of therequired safety practices . The need to use caution while operating around equipment was addressed . The requirementfor only one spotter as well as the need for personnel on the ground to be cognizant of the equipment movement areawas emphasized . Other potential hazards addressed at the meeting included the safe use of portable generators andloading metal into connexesQAR SAFETY COMMENTS:i'c(> RA, .~ pg~Pi rc ,Ct--T"Aye_~) ~-rD\ N ` tom' 1,j-'e-pr--Pr Y .I~;;~r-c c: L; ,-t-t-~- .SeNzLH i SEnvironmental Quality Control/Quality Assurance Report1Ee 415 r 302Continuation SheetWork Activities Performed This DateReference (NAS 10 SJTechSpeca)Activity&LocationQuantityContractorHTRW Removal (NAS 10 0022, 02050) Prewously removed drums from Site 10 . were sorted and processed 5.990 lb of HTW removed b date This site 20%.621 lb of Debris removed to date Thus site 60%Debris Removal (NAS 10 0020, 02050) Sweeps by personnel on foot were conducted in 8 . (the west beach) 39along the west shore of Troutman LakeContaminated Soil (NAS 10 0016. 02220) Trail work continued on trail improvements to the MountainTop and through the boulder field to Site 48 Argos were modified tocarry loads over the Tundra. and emergency equipment was prepared fortransport to the mountain topManpower and EquipmentLaborclasslfkation1111113ManHours212131212127Total Hours .178NumberProtect ManagerCOC System ManagerSuipenntendentArcheologistOperatorLaborersEquipmentType4 wheelerCat 426 loaderArgoNodwellPickupCat 966 LoaderNumber314111Hours Used364360124Total Hours92Verbal a Written 0Instructions Given by the Government to the Contractor ( k elude names reactions . and remarks )The OAR informed the CQC and Superintendent that he wish to be present for the operating load test of the Argoscrossing the tundra .Yes 0Yes 0Work Progress Are there any Contractor caused delays or potential finding of fad ?Are there any Government caused delays or potential finding of fact?Are there any unforeseeable or weather related delays?NoNoNoYes 0Remarks (Include any visitors to protect and miscellaneous remarks pertinent to work)Four new local-hire personnel were added to the project today .The Contractor ' s Project manager arrived on site today .The Project Archeologist delivered an archaeology and human bone protection briefing to the field crew at morningsafety meeting . He coordinated with the QAR on the potential use of additional Native liaisons . He also collected moreverbal histories to use as contextual material in the final report .The QAR informed the CQC that the water heater with suspect asbestos had been previously sampled . It had beendetermined to contain no asbestos .I certify that the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this period were in strictcompliance with the contract plans and specifications s noted abovey'r ` r~ t-f rduality Control Manager SignatureGovernmentConcurs with the oC report ?Additional Comments or exceptionsQualityAssuranceCommentsYes(,No4t,rX}nlG w l-jC TJ2o .'~Date4 J -) t.:u rf %&`~ ,c7 pC~ 2 cac L J l~ L_U M t T`j'% . t>!Eb-D 4,~'J4OAR Signature~ ~,,0~o ftjt, ~'pktmt')vt A t t! 1 .* ~~ .Date7-97Supervisoes Initial Oats~3Weight SummaryDebris removal and Containerized HTW RemovalDebrisActualWeight to0ActualUAR0DateU ..Weight toDate0 ..UAbSites0 3U0Contaminated SoilStained soilHTWUA00UAAActualWeight toDate0 30Site 21600020024985Site 377015960011500Site 4/Area 4A54102140Site 4/Area 4B9052230Site4/Area 4D10000Site 5Area betweensite 5 and 3315Site 6350Site 7150Site 811500039621Site 101300Site 12Site 1307897062007494121102300599054010079825507829783030034300055010400000ActualWeight toDate100299200Totals 127255 43913Percent of Contract Wt 35%16140 30360 40000 34566 104000 0188%86%0%Page 1As of 7/26/99 .9 01 PMDeficiency Tracking ReportContract Number / Delivery Order NumberUPCIProlect TitleOACA8S97-O-0OIOID.O . 0004Debris Removal and Containerized Hazardous and Toxic Waste RemovalOTLOate or Tim. PeriodLocation and Team0017123199Gambell , AlaskaDescription of deficiency :Inspection of processed drums in connexes 201291 and 205563 noted the following deficiencies :1 . A petroleum odor indicated that at least one drum in each connex had been insufficiently cleaned .2 . A bent and perforated but otherwise intact drum indicated that drums had not been deheaded .3 . Excessive dirt on the surfaces of some drum remnants indicated that soil was not being removed before processing .Corrective Action :1 . Connexes to be unpacked .2 . Processed drums to be inspected .3 . Drums requiring deheading and washing to be processed accordingly .4 . Connexes to be decontaminated .5 . Contaminated soil from floor of connex to be containerized for disposal .6 . Connexes to be rein ed .CCCSignatur-DateGovernment Quality Assurance CommentsConcurs with the corrective action?Yes gNoDAdditional comments or ex ceptons'(zRZ e2k &'F't, ,er'~Ar-CIQ0 ce . ~, .C,4,r‚CAR SignatureReinspection of Corrected DeficiencyPartial reinspection of connex 201291, 0900 hrs, 7/26/99 :Results : Connex fully decontamitated ( clean of dint, no diesel smell suspect drums segreated . Clean drumsrepacked into new connex . No diesel smell , minimal dirt residue.Final reinspection of connex 205563 , 1800 hrs, 7/26/99 :Results: Connex fully decontaminated (clean of dirt , no diesel smell) suspect drums segreated . Clean drumsrepacked into new connex . No diesel smell , minimal dirt residue .A suspect ms taped in ermed and lined area , heads c open for inspection and cleaning .CCC S1ynawrsOateGDericency corrected-) Ys 0 No [7Government Quality Assurance CommentsDeficiency corrected' Yes gNo t]Additional comments or exceptionsCAR Signature "i,"~U-'Date -2 , -2I/ YDeficiency Tracking ReportContract Number I Delivery Order NumberUPC/Protect TitleDACAtS-97-OM100.0 . 0004OTL002Debris Removal and Containerized Hazardous and Toxic Waste RemovalData or Time P.rlod7/26/99Location and TeamGambell , AlaskaDescription of deficiency :Inspection of the lined area where incoming drums are opened and inspected reveal an unsealed seam across the centerof the containment area . The created the potential for leaks .Corrective Action :1 . Improved the integrity of the lined area to prevent the potential for leaksW99CQC Signature_Government Quality Assurance CommentsConcurs with the corrective action?YjNo QAdditional comments or eweptions .OAR Slgnatu`DateLReinspectlon of Corrected DeficiencyReinspection of the lined area at 1800 hrs . on 7/26/99 revealed that an additional layer of liner had been placed over thecenter section restoring the integrity of the seamed area . Plywood had been added on top of the liner to protect the linerfrom puncture from the staged drums .COC Sl9natureDateDetiuencY corrected? Yes °No 0Government Quality Assurance CommentsDeficiency corrected? Yes0Additional comments or exceptionsOAR SignatureOat .I7'OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate : 7 /6 1999 Time :. G Briefing Location :L 0 d G CActivities Planned :Topic : /l/Z-_7 4 S a ~-'--'Location:Scheduled Work Date :7 - 2' - ' /Operator:< CAR Signature.ra?Lt'sDate~~ dCRelnspection of Corrected DeficiencyReinspection at 1630 hrs on 7/29 /99 revealed that the ground Wire had been satisfactorily installedCQCSignatureDateGovernment Quality Assurance CommentsDeficiency corrected ' Yes 0 No 0Additional comments or exceptionsOARSignatureDateIDeficiency corrected? Yes 0 No 00Deficiency Tracking ReportContract Number , Delivery Order NumberUPGProlect TitleDACA8S-97-0-0010/0.0 . 0004Debris Removal and Containerized Hazardous and Toxic Waste RemovaloTL006Date or Time PeriodLocation and Team7129/99Gambell , AlaskaDescription of deficiency :SAFETY DEFFICIENCYInspection of the generator at the site 4 top camp revealed that the ground wire was loosely connected to the generator .The wing nut intended to insure a positive connection was backed off greater than 1/Z inch . Consequently a positiveconnection was not made .Note : The CQC finger -tightened the connection before leaving the site .Corrective Action :1 . Tighten the grounding wired connection at the generator .2. Check for similar unsafe conditions throughout the project .COC Signature _ d[~J l=T!-1 Lfr'Date r%Government Quality Assurance CommentsConcurs with the corrective action?Additional comments or exceptionsCAR Signatu_DateYesXNO0'T 3& -' ' GReinspection of Corrected DeficiencyCOCSignatureDateGovernment Quality Assurance CommentsDeficiency corrected? Yes 0 No 0Additional Comments or eieptonsOARSignatureDateIDeficiency corrected' Yes ° No 0Deficiency Tracking ReportContract Number / Delivery Order Number UPC/Proiect TitleOACASS-97-D001010 .0. 0004Debris Removal and Containerized Hazardous and Toxic Waste RemovalttLDateorTim. PeriodLocation and Team005712 9/99Gambell,AlaskaDescription of deficiency :Inspection of drum staging and processing at the main staging area revealed that staged drums were being placeddirectly on the ground . Temporary liner was available, but not being used . This practice risks staining additional soilNote : This issue had been brought to the attention of the superintendent on not less than two previous occasions .Corrective Action :1 . Use Temporary liner while staging HTW items.2 . Check for similar conditions at HTW staging points throughout the project .JcoC Signature-,1-•1DateGovernment Quality Assurance CommentsConcurs with theAdditional comments or exceptions :11tNt72w X >t , F A ;GAR Signaturew`'~'Date+"Reinspect)on of Corrected DeficiencyReinspection at 1630 on 729/99 revealed that liner was being used to stage drums during processing to avoid thepotential for staini soil .,cOC signaturelLDateDeficiency corrected? Yes a No 0IGovernment Quality Assurance CommentsDeficiency corrected? Yes 0 No 0Additional comments or exceptionsQM Signature1Deficiency Tracking ReportContract Number / Delivery Order NumberUPC/Pro ect TitleDACA85-97-O-0010 / D .O. 0004Debris Removal and Contain e rized Hazardous and Toxic Waste RemovalDate or Time Period7/2 9199)TL.J7Location and TeamGam bell , AlaskaDescription of deficiency :Inspection of the generator at the Site 4 staging area revealed that there was no spill containment under the generator asrequired by the work plan . This condition creates the potential for soil contamination should an inadvertent spill occurduring refueling .Note : This condition had been brought to the attention of the Superintendent on not less than three separate occasionsat a different location in the project .Corrective Action :1 . Place spill containment under the generator2 . Check for similar conditions elsewhere throughout the project .COCSignaturepaleGovernment Quality Assurance CommentsConcurs with the corrective action?Additional comments or exceptionsLUAUOARS nature~~Yes 0 No 0J-Ltt L~1DateRelnspectlon of Corrected DeficiencyCQCSignatureDateDeficiencyGovernment Quality Assurance CommentsDeficiency corrected? Yes 0 No 0Additional comments or exceptionsOARSignatureDate1corrected ? Yes 0 No 0OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate :~'1999Time : Briefing Location :Activities Planned :Briefer.Topic :Topic :Topic :Briefer:Topic:Topic :Topic :AttendeesSite Healthand Safety Officer :LHOT WORK PERMITContract: DACA95-97-D-0010, D .O . 0004roject: Debris Removal and Containerized and Hazardous and Toxic Waste Removalecation : Gambell, Saint Lawrence Island . AlaskaType of Work :Heat Producing DeviceOperator :Location :Fire Guard :Scheduled Work Date :TimeThe Checklist Below WasSuperintendent :StartTimeReviewed~`Date :,_Finished:4fiDate :SHSO :LICOMPLETE IMMEDIATELY PRIOR TO WORKHot Work ChecklistItemNIA YesNo1 . Are all flammables and at lest 50 ft away?2.Is the operator fully qualified to operate the equipment?3.Has the Fire Guard been identified and briefed to observe the area for 1hour after work is0complete?4.Has emergency communication procedures been checked?Q5.Is and ABC extinguisher present and is it in working order?Q6. Have the tools and equipment been inspected for safety?Q7.IsthecorrectPPEbeingwom?°Qr8.Has the area been checked for flammable or explosive vapors?..QQ9.Have containers been checked for explosive/ flammable residue or vapors? Q(drums and tanks)Q10 . Are torch hoses purged before lighting (torches only)? Q011 . Are nozzles and hoses in good repair? (torches only) QQCOMPLETE AFTER WORKTime Start Time Finished :Superintendent:J'SC3Date :Fire Guard Released :SHSO:t/-,,Date :Environmental Quality Control/Quality Assurance ReportILK .Iii . WaContract Number / Delivery Order NumberUPCiProl .U TitleDACAIILS-97-) OM`1 0 D .O . 0004Debris Removal and Contaln . riz .d Hazardous and Toxic Waste RemovalCOC Report Numberpate or Time Period99-0257130199Weather ConditionsTemp Low 42Temp HI MWind Speed3-17KnobLocation and TeamGambeil . AlaskaContractorConditions Cloudy . windy . toe , intermittent boy" rainOil Spill Consultants, Inc .Ouatlty Control Inspections Performed This Date (houde inspections results deficiencies observed . and corrective action)Preparatory O s.. atbcMd ctwilli tin".cUht Cannminat.d Soil Excav .don° s. . aaacMd chFollwwUp 0W as the deficiency tracing fist updated Rks dateField Sampling and TestingHas field testu+p been performed the dale-)Type of lest Metttod/MatnxYes 0 NoYes 0 No aQuantityofsamplesResultsNO FIELD TESTING TODAYHave Data Q uality Objectives been adtieved ?N/AYesD NODHave Samples Beers Coll ected for Laboratory Matysis?Type of Test EPA Test MethodMlabuY.sDNO°Quantity of SamplesNO SAMPLING TODAYHave required amount of OC trip banks and rinsates been achievedHave appropriate QC Laboratory tests been ordered 7 (matrix spikes . method blanks . surrogates . reference standards .Have QA and OC samples been collected n the specified quantity? Not required by Delivery OrderHave samples been property labeled and packaged ?etcIwAOrsONoON/AOYuDNoOIYAOYsONoON/AOYssONoDHealth and SafetyWorker protection levels this dateLevel A O Level B O Level C O Level D °Was any work activity conducted within a confined space ?Ys OWas any work activity conducted within an area determined to be immediately dangerous to life and health ?Yes 0Were approved decontamination procedures used on workers and equipment as required'Yes 0Safety Comments (hdude any infractions of approved safety plan, and include instructions from Government Personnel Specify corrective action taker l)WA( :)No°Nom160 CaThe Crew Foreman, a local resident , highlighted the hazards posed by wildlife . Of special concern were foxes . Thenormally-shy animals could carry rabies . Any fox that approached closer than 50 yards was not behaving in a normalmanner should be assumed to be diseased . Steps should be taken to avoid coming in contact with the animal . TheSuperintendent repeated his cautions of the previous day for personnel to use extreme care while travelling on foot overthe boulder field . The rain-slick boulders present the potential for slips and falls . The need for care while travelling thefoot trail to the mountain top was also discussed .After the safety meeting the CQC and the Superintendent reviewed the results of the previous day's safety inspection .Possible improvements in generator grounding , spill containment , and fuel storage were discussed .In the evening the Site Safety and Health Officer reviewed with work crew the results of the samples of the Area 4Bcontaminated soil taken during previous study . The origins of the contaminants found, their effects, and appropriate PPEwas discussed .OAR SAFETY COMMENTS :L'1(CL,eii,~j~. t -, P ' eR'GZ~`~i isA--.t L Pp C 1 NIP tJf cEnvironmental Quality Control/Quality Assurance ReportIER4ty 1 3021Continuation Sheet•rk Activities Performed This Deberence (NAS IO WTed+ Spec 9) Activity & LocationOetxks Removal ( NAS ID 0020 02050)ContiadorOuantrtyStained Soil Removal (NAS b 0019 . 02050) Stained sod was collected from Area 4A at MW top of Mmountain but not yet weighed35.614 lb of Stained soil removed to date protect-wideAt Site 4• Areas 40 . 48 . and 4A . the mountain top personnel 54 .477 Ib of peons removed to date protect-wdecollected and stockpled. None yet weighedways weighedContaminated Sod (NAS ID 0016 . 02220)Site control was established and eacavaeon started AN digging byby hand Appro xmately 1 c y dug and containerizedManpower and EquipmentLaborCta*sNk4 tlonProtect ManagerCOC System ManagerSuperintendentArrlleoiogkstOpeabrLabormsNumberEquipmentTypeManHoursNumber Hours Used124wheeler312112Cat426loader10113Argo624112Nodwd/10112Pickup11210116Cat966Loader10TotalHours167Total Hours 48lnstn cUons Given by the Government to the Contractor (Include names . reacbdns . and remarks)Verbal 0 Wrttten 0NONEWork Progress Are mere any Contractor caused delays or potential findutg offact'YesAre there any Government caused delays or potential finding offact'YesAre there any unforeseeable or we~ related delays'00YesNoNo0 160Remarks ( Include any wsrtors to protect and miscellaneous remarks pert rent to work )o new Argos were delivered to the project today .The Contractor's Project Manager left the site today .I certify that the above report is complete and correct and that all materials and equipment used work performed and tests conducted during this period were in strictmpsance with the contract plans and specifications except as noted aboveQuality Control Manager Signature~' / 'rte JDateGovernment Quality Assurance CommentsComers with the OC reports/Yes NZNo 0Addibonai comments or Seepbons..-S ;i-ic K'kCtLMk,j .n,!CTC--'Iv?- l ' ~oF fit: pri4 Or t--7C CA v .tTr~I .roes:O' - 6'Yi~ C ~ e~rz . ra F=rLrut .Fot_f la - I )r z •., AT . d . ~t ;', Su~~ t,1~rkl~ warms .A> F~~- 1 f3'~ ~rtrf .Environmental Quality Control/Quality Assurance Report(ER 415-1 .302)Continuation Sheet4cttvltles Performed This Dateonce (NAS ID & Tech Spec 8)Activity & LocationQuantityStained Soil Removal (NAS ID 0019 . 02050) No Activities Involving stained sod todayContracior35 .619 tb of Stained soil removed to date props-wdeHTW Removal (NAS ID 0022 . 02050)Sites . 2. 3 . 5. 8, 7. 12, and 13 completeAll HTW at site 4 stockpiled awaiting transportation32.631 lb of HTW removed to date prated-wideDebris Removal (NAS ID 0020 . 02050)Sites, 2. 3 . 5. 6 . 7 . 12, and 13 complete8 .803 Ibs of debris at Site 8 weighed and loaded63.380 lb of Debris removed to date project-wdeAll debris at Site 4 collectedContaminated Sod (NAS ID 0018 . 02220)E*avated soil was transported the staging area and10 .117 lb of contaminated Soil removed to dateWeighed . 10 .117 Ibs weighed today . more stockadedManpower and EquipmentLaborCfasslflcat/onProtect ManagerCOC System managerSupenntendentAro-wologistoperatorLaborersNumber011ManHours0121311211012116Total Hours.165EquipmentType4 wtieeterCat 428 loaderArgoNodwellPicJupCat 966 LoaderHours Used24380Number31810111210Total HoursItstructlons Given by the Government to the Contractor (include names , reactions , and remarks)109Versaf 0 Written QNONEWork Progress Are there any Contractor caused delays or potential finding of ract7Are there any Government caused delays or potential finding of fact?Ve there any unforeseeable or weather related delays?Yes QYes 0Yes 0NoNoNone.narks ( Include any visitors to project and miscellaneous remarks pertinent to work)Two new Argos with bad clutches were repaired today and returned to service . The Cat 973 track -loader was repairedtoday .I certify that the above report is complete and correct and that all materials and equipment used . work performed and tests conducted during this period were rn stnctcompliance with the contract plans and speurica~s except as doted aboveOualtty Control Manager Slg natumGovernment OuaIIty Assurance Comm.ntaCancans with the OC report?Yes(3No0Additional comments or exceptionsk-L>L'Ci r' Tj .F?ut'.,NGcrjQ k t ' r :-'S O 2Dv~7bl' ~L*T r~- li3 5rt"LLt rr . , r* rt c7yt JS , 5~f~ Yrul.fi0-• iz i U >`' rfo~ 'T FF .S v--~r•'~K PLo -JGG1-FtIEnvironmental Quality Control /Quality Assurance Report(ER 415.1 .3022)Continuation Sheet`work Activates Psrfonme This bats*once ( HAS 10 s(Tech Spec 6)AdMty & LocationQuantity,,tamed Sod Removal (HAS b 0019 . 02050 ) NO stained soil collected todayContractor35.695 Ib of Stained sod removed to date protect-wide14TW Removal (HAS 10 0022.02050)Previously, collected HTW from Sim S . was we.phed todev470 lbs processed today35 .877 lb of HTW removed b date prged-wideDebris Removal (HAS ID 0020. 02050)Previously sl x*pded debris at Sits 8 was processedAnd Debris from Sots 4A was transported o6 the mountainand processed . 13.993 weighed and loaded today72 .626 1b of Dews removed b date protect-wideContaminated Soil (HAS b 0016 . 02220)E=avated sad was transported b the staging areaNo additional $od excavated or weighed16 .932 lb of contaminated Sod weighed 10 dateManpower and EquipmentLaborClasslfcattonProtect Managercot system ManagerSuperintendentOperatorLaborersEqulpenentNumber ManHours Type004wheeler112Cal426Numb"3loader113Argo112Nodws!112Pickup9 106 Cat 966 LoaderCat 973 Trade LoaderTotal Hours :157Hours Used24163861111012103ToW Hours 116Instructions Given by the Government to the Contractor (Include names , reactions . and remarts .)Verbal0 Written 0NONEYes 0Yes 0Yes 0Work Progress Are there any Conraclor caused delays or potential finding d tact?Are there any Goverrrnent caused decays or potential finding at tact ?Are there any un*xeseeable or weather related delays ?NoNoNosmarts ( include any wsibrs to project and miscellaneous remarks pertinent b work .)The COC and a facilities technician from the FAA used test equipment to locate and mark the live electric cable that hadbeen discovered between the east side of the runway and the road in Site 8 . The live cable was found to be buried lessthan one foot deep along the run from the power enclosure at the mid -point of the runway to the junction box at the southend of the runway . In all other areas it was buried 6 to 10 feet below grade .The Project Archeologist called SHPO representative Tim Smith and asked him (he agreed ) to call Suzanne Beauchampto confirm no problem with cleanup in archaeological site XSL-005, at end of airstrip adjacent to Area 8 . This area is acandidate for inclusion in the project .Later he met with Sivuqaq Inc . President Job Koonooka and Native Liaison Bert Oozevaseuk regarding disposition ofrockshelter with hearth in Area 4. Koonooka favors protection if site proves to be archaeologically significant .Koonooka' s decision was to : a) confer privately with elder Conrad Oozeva rather than whole Board ; b) depending on thatconversation , he would request that the Archeologist and Bert test site to determine age (not outside the usualcompliance parameters for a project such as this ) ; and c) depending on that conversation , the full Board would decide theCorporation 's protection strategy (protection from villagers , not from our cleanup work ) . Also delivered Artifact #1 andobtained signed receipt .I certify MM t e above reports compete and correct and that ON materials and equipment used. work performed and tests conducted during this period were in strictcompliance with the eoneract plans and specfir ltions;- reas noted above00-1-17Quality Control Manager Signature99-028lkDate2Environmental Quali ty Costrol/Quality Assurance Report(ER 41St Jp2lContinuation SheetGovernment Quality A .wranc. commentsConcurs wdh ft QCreport?Additional comments or acepbons:r'9 wGGf~OrI~c~ J~ Ci•f c, Jk-i t;-,-, L 0 (A-r'Tv1a,2a-ar:c~ `r ~C` t5 .*4Lsv vYsdNOCh"~G~YaL)~-~~~~7YV/~rti JCwt1~h~) TLSt ~rS~ ~Ni~GM 3lgnaturat --~-.e~49 .22~;~_ kr . .'E~t i ~~r T) ~•v A U a r A-y 540-%4-)- U"-"Ac~f t 6 L YtMk5 AZIP A'cFc~; cImo(-s$VA C-r- Sk-A, t-C 4s- c>0Lvc AINt?st.3`3yj.L rv 3N .r,,j L G c1,-- t Eti..1 l. :c $1.sup .rvlsof s Initial lateOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate :1999 Time :r.• ! CA ~ .•JBriefing Location :*-LActivities Planned :Briefer:~-C1:c,-0. hJ CA~Topic :..mod~h 0 &G5L/Topic: LTopic:Topic :Briefer:Topic :Topic :AttendeesL4OSite Healthand Safety Officer :Date :O1999Weight a .. . .imaryDebris removal and Containerized HTW RemovalDebrisf0Actual†umcWeight tocDate0uSitesHTW0†uActualWeight toDateContaminated SoilStained soilf†C0 -U†uL‡†C0ActualWeight toDateUSite 21600020024985Site 377015960011500Site 4/Area 4A541012348214022780Site 4/Area 48905022301688526Site4/Area 4D10002948021570Site 5315113104700site 5 and 355Site 635078970Site 7150Site 811500073936620074941814Site 101300023007071540Site 12100798255078297830Site 13300343000Totals 127255Percent of Contract Wt9465574%16140†104000ActualWeight toDate16932AreaWEEKWEEK10029920038034 40000236%Page35695 104000, 1693289%16%1Asof : 8/3/99, 6 :48 PMEnvironmental Quality Control/Qnslity Assurance Report(ER 415-1-302)Contract Number I Delivery Order Number :UPCIPrgec TileDACA8S-97-O-O0101D .O. 0004Debris Re noval and Contain rtz .d Hazardous and Toxic Waste Removal'OC Report NumberData or Time PeriodLocation and TeamM30114199Gaanb.ll, AlaskaWeather ConditionsTemp Low a4 Temp M 4,1Wind Speed15.35 KnQtaCo.tractorConditions windy and ravro.Oil Spill Consultants, Inc .Quality Control Inspections Pedorm.d This Oate ( Include inspections. results. defiaenaes Deserved . and corrective action .)Preparatory 0 on saw" clockftknbal 0 w a acMO ch.ckFmiFollow-up0Was the deficiency tracking list updated INS dataField Sampling and TestingHas field testing been performed this da e?Type of testYes 0 NoYes 0 NoMedhod/littnxQuantity of samplesResultsNO FIELD TESTING TODAYHave Oats Quality Ob} ectives teen acheved?N/AY .sOHave Samples 8..n Collected forLaboratoryType of Test EPA Test Medhod/ MatrucAnalysis?Quantity of SamplesYsOMooMOONO SAMPLING TODAYHave required amount of QC trip blanks and nnsates been achieved?WAOYesONOOHave appropriate OC laboratory tests been ordered 7 (matrix spikes, method blanks, surrogates, reference standards . etc.)WAOYesONOOHave QA and OC samples been collected in the specified quantity? Not required by Delivery OrderN/AOYasONoDHave samples been properly Labeled and packaged?WAOY.s0NOOHealth and SafetyWorker protection levels This date :Level A O Level B O Level C O Level O 0 NYACWas any work activity conducted within a confined space ?Yes0MooYes0MooWas any work activity conducted within an arom determined to be immediately dangerous b life and health ?Were approved decontamination procedures used on workers and equipment as required ?Yes0MooSafety Comments : (include any irtfrsctions of approved safety plan . and include instnrctiona from Government personnel . Specify corrective action taken)The Superintendent addressed importance of wearing the minimum level of PPE during all activities . This includes hardhats , steel-toed boots , and safety glasses . The PPE upgrades for ATV use were also stressed as was the general safetypractices for operating ATVs . These practices included safe travel speed , awareness of terrain , and proper cargoloading . The need for the buddy system , during periods of low visibility, was also stressed .OAR SAFETY COMMENTS:~t G•frv.7 ~ , rtR, .. ,.v ,?~, lC .x~XC r~c~ .C`jIo,. _' Sr~trvg.T' "-t u,v' 1Environmental Quality Control/Quality Assurance Report.(ER 4 15.1-3021Continuation SheetWort ActivltIes Performed This DataReference (HAS D I/T.cn Spec6)Acbwity&LocationQuantityContractorCREW ON STANDBY DUE TO WEATHER ALL DAYStained Soul Removal (HAS 0 0019 .02050)HTW Removal (HAS D 0022 . 02050)NoscrimtodayNO ac" todayDebris Removal ( HAS D 0020 . 02)50)Contaminated Soil (HAS D 0016 . 02220)NoNo35 .695 lb of Stained soil removed to date proiecl .wooe38 .034 lb of HTW removed to date protect-wideactiMtytoday94 .655 lb of Debris removed to dais protect-wideactivitytoday16 .932 Ib of contaminated Soil weighed to dateManpower and EquipmentLaborClassification NumberProject Manager 0coC system Manager15uperimene"I1ArChe06091l1Operator1Laborers13EquipmentTypeManHours0ee8ewheeler3Cal 426 loader1Argo6Nodwell1Pickup1104Total Hours:Number Hours Used4Cat 968LoaderCat 973 Track Loader136TotalInstructions Given by the Government to the Contractor (kldude names . reactions . and remarks .)Haas60600110012verbal l7 Written 0NONEWok Progress Are there any Contractor caused delays a potential finding of fad?Are there any Government caused delays or potential finding of fact?Are there any utoreseea )le or weather related delays?Yes 0 NoYes 0 HoYes 0 No I&Remarks (kuciude any visitors 10 project and miscellaneous remarks pertinent to work)Severe weather, (cold temperatures, strong winds, blowing rain) forced a cessation of all cleanup activities for the entireday . Crew on standby for 8 hours .One additional HazWopr laborer arrived on the project today .A four-man USCG helicopter Search and Rescue (SAR) team led by Lt . Orin Rush arrive on sight today . Their missionwas to search for skiffs and people missing at sea from the flotilla of Russian natives that had left Gambell for Russia onthe previous day . Contractor-provided support to the SAR team included evening meals, ground transportation, andphone and fax support .I Certify Vial the above report is complete and Correct and that all materials and equipment used . work performed and tats conducted during thus period were n strictcompliance with the contract plans and spedagpome e.cept as noted above .Government Quality Assurance CommentsConcurs with th QC report?Yes 10No0Additional comments or exceptions .( ,y-r,r1 c rE 4d 7` F e n :'+ }3t' v T 4 '5 v f7pui c i X ` X_K c.1.1>c fviK"4,- `5 --71SL t?t~ >pIS1~ ~ZZ~$`r4r~. Ge..., n:`0-AC17 L .Lic> k 1L7T 13r- je.' vi t tI(S C 4 , !+L_ Aal_y • ST --CEQAR Signature99-030Date2(,vim-ti~~c(oa r , L rv-CD-- fort V=T- Lo L LC) A rv 1 t.> > & 6 rv t PC nevi,-- N' -41 V ,1 Supervisor' s Initial Date.OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location :Gambell , AlaskaDate: -041- 1999Time :7.'ao 4/y1Briefing Location :L GG'~~Activities Planned :Briefer:Ck06K Y4-747-1-1Topic: A64 RIO R4 7STopic: -4 T VTopic:Briefer :Topic :S4 Fc r YPP!"xcavc f'f~•~ ~4rcSG -Fc 7 G 10 5 STopic : •-ra 'e, or ITopic :AttendeeseL ~4Z4ZSite Healthand Safety Officer.tI B 14 r5 CEnvironmental Quality Control/Quality Assurance Reportiu 415.1 -t0C9Contract Number / DeliveryOrderNumberUPC /Prgect Ties.OACASS97-O4010dD.O . 0004Debris Removal and Contalnertzed Hazardous and Toxic Waste Removal7C Report NumberDate or Time PeriodLocation and Team1-031list"Gamb.fl, AlaskaWeather ConditionsContractorTemp Lour 46 Tamp K RWind Speed1535 KnotaConditions windy and ram,ON Spill Consultants, Inc.Quality Control Inspections Performed This Data pndude mspecbons. results . oelt '- CvPz u.~+tf + let C. 14 ~ut~ slet ,. AArj, uG~v a~t-1- 41000' 9 k : t.44"V"z •G S ~I.k tom .. ft 4 aEnvironmental Quality Control/Quality Assurance ReportMR 415.1-)Continuation Sheetforte Act vItfes Performed This Oateeferet a (NAS 10 ?(Tech Spec 0)Acbrty & LocationQuantityContractorStained Soil Removal ( HAS t0 0019 . 02050) No stained soil collected today36 .158 rb of Staurd sod removed o date D( o -wideHTW Remove) ( HAS ID 0022. 02050)Prewously.odtecfed drums kom Site 10 (Rte lundrs )and SiM 4 (tn mountain top) were weighed 1 .294 Ib44 .943 lb of HTW removed to dale prgect-wideDebris Removal (NAS ID 0020 , 02050)No debris was processed today94 .655 lb of Debris removed lo date protect-wideContaminated Soil (NAS 10 0016 . 02220)21,294 lbs of soil was weighed and lorded today7.663 to of rail .46.069 lo of contaminated So l weighed to dateManpower and EquipmentLaborClassNtcationProtect ManagerCOC System ManagerSupennter dervArcheologistoperatorlaborersNumber0111111Total Hours :EquipmentManHours Type04 wheeler12Cat 425 loader14ArgoNumber Hours Used33014666Nodwell1012 Pickup132Cat 966 LoaderCat 973 Track Loader1111210012182instrvctlons Given by the Government to the Contractor (hdude names. reactions, and remarks .)Total Hours128Verbal 0 Written 0The OAR provided direction to the CQC to expand the cleanup effort in Site 8 (the west beach area ) to incorporate thearcheological site north of the runway and west of the road to the runway . Work must be done under the supervision ofthe Project Archeologist and focal personnel will perform the work .It was brought to the OAR's attention that earth work by another contractor was uncovering drums , previously buried, inthe southeast comer of Site 8 . This was increasing the amount of HTW material projected to be in the area . The OARdirected that no new drums be picked up in these areas .Yes 0Work Progress Are there any Contractor caused delays or polenbai 6n6ng of fact?No aAre there any Government caused delays or potential tUtding of fact?Yes 0No aM there any unforeseeable or weather related delays?Yes 0NoRemarks (Include any visitor$ to project and miscellaneous remarks pertinent to work)Native Liaison Bert Oozevaseuk , identified a sled frame in Site 5 , east of the High School . that had not been previouslycatalogued for removal . The OAR was informed . The item will be considered for possible inclusion in the cleanupprogram .The CQC and the OAR conducted a survey of the Air Force and Army Trails in the Tundra portion of Site 10 . The OARtook GPS readings and plotted the location of the trails (Map attached). Approximately 600 If of 6 ft galvanized chainlink fence was found near the north end of the Air Force trail . The Native Liaison , Bert Oozevaseuk , identified this fenceas the remains of a reindeer coral , not from previous military activities .The USCG SAR Team stationed at Gambell left today .I certify M at the above report is complete and coned and that as maMv ˆls and equp .nent used . work performed and tests conducted during ttws period were in strictcompliance with the contract plans and specs icstions except as nosed aboveQuality Control Manager Signature99 .032f '4'o. .Environmental Quality Cwtrol/Quality Assurance Report(ER 41 .133Continuation SheetGov.mm.nt Quality Assurance Comm .ntsConcur "Oh to QC report?Additional commerw or eacsptiorn :- A) Gn r-, E. iYes&No Qv1 4V/4/9? (? 'rP Mi'd.-L 7~. 1t3fl-~A .r-, !~,Efh $Cc 'tomcc-b-t-U-Ls)lV."~JtiGc S Qom . kl.f 1 C S e=vc"-/t'~ ~tye~S'1 ~l JOo`JrS . m--r::- S• rL-t~.~r~ 1.e/ t~ .~K c P C ~J1 '7f--• /1.~ r W4. ~ L.& - /{gyp Fr .T--DQ^R SignatureQ9-032C .~ ,(,~t(X`StA-5 ~ l ` . r•/fYPArc~Tv +r)P 'y`o p %-; r~,& .S Lttd- SQkqeL w-,&-W P-r c0SSup .rvlsor s Initial Date37 - ~~-iOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907)!562-7169Safety Meeting MinutesProject Title: Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell . AlaskaDate :1999Briefing Location : __L1Time :Activities Planned :Topic :Topic :Topic :Topic :Briefer:Topic :Topic :Attendees'11)c l''I•(2~L is ' lJ l~JSite Health J~r~ :'~ L~?~ -~ rand Safety Officer :Date : ~' 1999Weight . _ . ,imaryDebris removal and Containerized HTW RemovalActualWeight toDateSitesStained soilHTWDebrisContaminated SoilActualWeight toDateActualWeight toDateActualWeight toDateSite 21600020024985Site 377015960011500Site 4/Area 4A5.41012348214022780Site 4/Area 4B905022301688526Site4/Area 4D100029480596946311310470078970Site 5315Area Derweensite 5 and 355Site 6350Site 7150Site 811500073936620074941814Site 1013000230010168540Site 12100798255078297830Site 1330034300010400046089100299200Totals 12725594655 16140Percent of Contract Wt74%44943 40000278%Page36158 104000 4608990%44%1Asof 8/6/99,8 :01 PMEnvironmental Quality ContrC4VQuality Assurance ReportContract thsnber I D.lwy Order Humber :UPC1Proj.ct TII sDebate R .movd and Contaln.rtzsd Hazardous and Toxk West. RemovalDACASS-I7-O-O01WO 0.0004Defft or nme PedoddRf91sport Number.3Location end TeamGarnbo ll, AhsaContractorYW.tisr CordklonsTemp Loa 44 Temp 14Wind Spiedcalm - i KnobOn spm Consultant.. Ire.Conditions da,Cr_Oualty Control inspections Pertomm .d This Des ( tiduds Inspections. refits. den denrles observed, and conrecta action .)Pneparatcxy a e† srdwd eh .eldtabredFoltow.Upass. ties ant owk"°Debts loading: 10 roars e- Iropected and reed, for movement to barge loading ares .(r pectlon lit attad+ed)Was t e defkfency b-addnq IM updated era dal.Yen o NoField Sampan aid TwangHas Nest tssang been paormed era.?dalYesaNoType d fast Method %Itrbc Ousnetp d sample, ResultsNO FIELD TESTING TODAYHave Dets Qt y Obfeceves been sd*wed7WAY090MOOMe" Samples Seen Collected for Laboratory Analysis? YeeD mooType d Test EPA Test Meetod / M.bbc Quantity d SamplesNO SAMPLING TODAYHave req *ed .mount d QC tip blanks and dmates beat actread7WAOYssONoeHave appnopAab QC laboratory tests been ordered ? (mat tt spiksa, method blanks, surogates, rererenc. standards , eti) WAOYasONoaHave QA and QC samples been od ecled ln tine spedlted quenetl? Not nqub .d by Dmvery Order IYAOY.(JNoaHave samples been txvperty labeled and packaged? NIAOYesONOOHealth and SafetyWonrsrr prasc a lava s this cle tr Level A D Level S a Level C 0 Level 0 0 WADWas any work ac" aonducled within a oonfned spec.?YesaNo°Was aq wok aeevfgr conducted wMi an are . determined lo be lmmedlalefy dangerous lo We and beam? Yes C3 1400Was approved dscanUmin.eon procedures used an workers and equlpmers n rsqAed7Yes C3 1400Safety Conxmergs ( 4nclude arty inA aetlorri d approved safety plan, end indude Instructions tram Oo%ernment persomet. Spedly corrective aeon taken .)--,9 Superintendent addressed the need to adhere to Hard hats, steel-toed boots, and safety glasses as the minimum' PPE for all activities and the wear of helmets while riding four-wheelers . The Site Safety and Health Officer.ianphasized the need to avoid 'going home syndrome .' This Is the condition where caution, attentiveness, and safetypractices tend to lapse as field work nears completion . With no accidents or injuries on the project to date . personnelneed to maintain the same level of safety awareness all the way through to the end of the projectQAR SAFETY COMMENrs :.%, A -CAe,L,.Jl e*7 t7tcr`f~aF 'a'>^,<tA~t/9s L/''Zb~l .) rOfm !JE'if•Lc L ,? (J r n, %r5I.~ ttEnvironmental Quality Control/Quality Assurance ReportIER 418-1-302)Continuation Sheetvoril Ac!lvRfe. Performed This Dabefereno. ( NAS D *fT.dh Sb.c 0)AdvRy & LOCaanOust"Sts ned So0 Remove (HAS D 0019 . 02050)216 D d prevft*-W~ a9Ued son proc.ased belay*6,M tb d Stained so t rsnwM d b dab proj. el-wW .MTW Remoal (HAS D 0022, 02030)Pre+busfroobxled Qtma Rum She 10 Mw tundra)and Sft 4 (1M matx+tin to were *Wifilned 2,761 lb47,704 lb d HTW removed b das p coed-w4d .Debris R.mo614 e d prtvbustf co6ected debris was proc e ssed bdey93,1691b d Debris removed b daW Pled-wide16.611 fare d can n kneel sad was wsI led ")r-11 todayAppro mateq 1 .375 lb d ad b.gped but not weighed64,900 d oontamknaled Sob we" b date.(t4AS D 0020, 02050)Canlanikrod Son (HAS D 0016 . 02220)Manpower and EquipmentLaborclassiflcadcePru)ed wMarCOC Stem flrYr"WNumber0EquipmentTypeManHours0121comradorNumber4 of*"Cat 426 beder313Argo6Hours Used304661ArcJheo/ogbt112Nodwel10operaw112Ptdaq112Labours12144Cat 966 loaderCat 973 Track Loader1110STOHoes:193Tow/ Hours:I %*thICnons div an by the Go..rnrn .nt 101} 1 . Con1Ml Dr (Rldude name, reacU. -, and rlnM127Vetted 0 Wrltten ONONEWork Progress Are there any Contractor = used deIs s or potmisai Mdrq d fact?Are tiara any Govemmere = used deterr or poisn4at &, ng d acnAm twe any lydbrese nwe or weather raf=ted detare?Yes OYle DNoNoYes ONoRemarks (Rrhrde arty vls1bxs b project and rtlta areas remarlrs pertinernt b wOIL)The Cat 973 was repaired and returned to service today . tt moved 4 connexes from the staging area to the north Beachbarge loading site .During and Inspection of Site 12 It was noted that persons unknown had been digging In the area and unearthed aditlonaldebits. The OAR was Informed.The Superintendent reported the following sites complete and ready for CQC Inspection : 2, 3, 6, 7 , 12, 13 .i oerey Qua Q1e above report is aompleis and Correct and 9ha at matatws arvd equlpm er* used, work peAommd and lssa Conducted dlrkq 91b perld wars ti =tactoompba a with the Contract plm and speefteftru New s$ rested above.DGovernment t]ua ty Assurance CommentsConcurs with t1. CC report?Addt5onai co-w-w Or ., ;N .YesANO. P-A- -1 S . 'flits, C G r-o c*-t- P/t G Avx)4-S4,r-r'St ‰ E %'-'- (,r .,, ' 'JP.-6 7tT -P*e .' Part rT- au ~oZLA, c, .01 " uvtl'tY'b-Lk ,i-.7- >1^- Z Gs' e 7-t e,-,S .iN 5 oa~7 cJrv S W I L LS F" bfj1WOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate :1999Time : Briefing Location : 04l1~f Or'/~/f1O1~~xL~ VQ,fivn A f 1v.Activities Planned :•flsiBriefer.Topic : L (Y$f 0PPLTopic:Topic :BrieferC//2Topic:/Id/Y.JI!7Topic :Topic:AttendeesDate:1999LOADED CONNEX INSPECTION SHEETConnexes CompleteConnex # Wt ticket Collected Whelghed20567661537/30/997 /31/9920567661547/30/997/31/ 9920567661557/30/997/31/9920567661567/ 30/997/ 31/9920567661577/30/997/31/9920567661587/30/997/31/9920567661597/301997/31/9920567661607/31/997/31/9920567661617/31/997/31/9920567661627/31/997/31/9920567661637/31/997/31/9920567661847/31/997/31/99DescripitionContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated Soilnet Wt.LoadedTare Gross Wt Total WL61849181379384186797110206269537385757/31/997/31/997/31/997/31/997/31/997131/997/31/997131/997/31/997/31/997/31/997/31/997777777777776254988208008488749781027633960745582205676620567661651697/31/997/31/997/31/99811/99Contaminated SoilContaminated Soil8118697/31/998/1/997781887620667661707/31/99811/99Contaminated Soil8838/1/997890,8/1/998/1/99778308658/1/998/1/998/1/998/1/998/1/998/1/9977777750006227524892922415025000,205676620567661711727131/997/31/998/1/998/1/99Contaminated SoilContaminated Soil8238582056766205676620567662056766205676620567661731741751761771787/31/997/31/997/31/997/31/997/31/997/31/998/1/998/1/998/1/998/1/998/1/998/1/99Contaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilConnexConnex Gross weight615745482285234495Inspection date , 8/7/9916567500021567LOADED CONNEX INSPECTION SHEETConnexes CompleteConnex #Wt ticketCollected WheighedDescripitionnet Wt . Loaded Tare Gross Wt Total Wt.1006851827/28/998/1/99Drum Pieces9048/1/9909041006851006851006851006851006851832102142172207/281998/2/998/3/998/5/998/3/998/1/998/3/998/5/998/5/998/5/99Drum PiecesDrum partsDrum PiecesDrum PiecesDrum parts791964888118411518/1/998/3/998/5/998/5/998/519900000791964888118411511006852218/31998/5/99Drum Pieces10018/5/9901001014350122695445000 , 50005000145441006852228/3/991006852238/5/998/5/991007161007161951967/25/997/26/99Drum partsDrum parts8/6/99ConnexConnex Gross weight8/2/99Landing Mat8/2/99 Landing Mat, Weasel Track, Misc14358/5/9912268/6/9979311318/2/998/2/990079311311007162008 / 2/998/2/99Misc Metal17328/2/99017321007162018/2/998/2/99MIsc Metal7888/2/9907688/3/9901430100716202811/99813/99Quonset Hut Debris14301007162038/1/998/3/99Quonset Hut Debris12768/3/99012761007161007161007162042062068/1/99812/99812/998/3/998/31998/3/99Quonset Hut DebrisMisc Metal debrisMisc Metal139210929908/3/998/3/998/3/99000139210929901007161007162072088/2/998/2/998/3/998/3/9910508068/3/998/3/990050001050,806500020112420112468697/17/997/17/997/22/997/22/99166214487/22/997/22/990016621448201124707/17/997/22/9916497/22/990164920112420112420112420112420112420112471721471481491507/17/997/17/997/20/997/20/997/20/997/20/997/22/997/22/997/31/997/31/997/31/997/31/99Misc MetalMisc MetalConnexConnex Gross weightLanding MatLanding MatLanding MatLanding MatLanding MatLanding MatLanding MatLanding MatLanding MatConnexConnex Gross weight1769135612091253106310567/22/997/221997/31/997/31/997/31/997/31/9900000050001769135612091253106310565000Inspection date , 817/9912460500017460,12465500017465LOADED CONNEX INSPECTION SHEETConnexes CompleteConn ex #201153201153201153201153201153201153201153201153201153201153201153Wt ticket Collected Whelghed1117/17/9971251991127/17/997/25/991137/17/997/25/991147/17/997/251991157/17/997/25/991167/17/997/251991177/17/997/25/991187/17/997/251991197/17/997/251991207/17/997/251991467/20/997/31/992012161247/25/992012161257/25/992012162012162012162012162012162012162012162012162012162012162012161261271281291391401411811972092387/25/997/25/997/25/997/25/997/29/997/28/997/28/997/221997/261998/2/998/6/992012782012782012782012782012781511521661671687/20/997/20/997/20/997/20/997/20/99/27/25/99DescripitionLanding MatLanding MatLanding MatLanding MatLanding MatLanding MatWeasel TrackLanding MatLanding MatLanding MatLanding MatLoaded Tare Gross Wt Total WLnet Wt.8347/22199083411487/22/9901148159115917/22/990166116617/22/990193319337/22/99017467/22/99017468587/22/99085811497/22/990114912517/22/990125120317/22/99020318097/31/99080915011Connex5000500020011Connex Gross weightrum Feces1081901081Drum Pieces75171251990751982999895565136128740110814701193247/25/997/25/997/25/997/25/997/29/997/29/997/29/99811/99812/998/3/998/6/99000000000005000982999895565136128740110814701193245000127811661881173016707/31/997/31/99811/998/1/998/1/990000050001278116618811730 ,167050007/25199Drum Pieces7/25/99Drum PiecesDrum Pieces7/25/997/25/99Drum Pieces7/29199Generator7/29/99 nerators 1 10 kw enerator , 17/29/99Engine Block8/1/99Drum Pieces812/99Drum Parts813199Drum partsDrum Pieces8/6199ConnexConnex Gross weight7/31/99Landing Mat7/31/99Landing Mat8/1/99Landing Mat811/99Landing Mat811/99Landing MatConnexConnex Gross weightInspection date, 8/7/995000A-198655000148657725500012725LOADED CONNEX INSPECTION SHEETConnexes CompleteConnex #201448201448201448201448201448201448201448201448Wt ticket Collected Whelghed1317/26/997129/991327/26/997/29/991337/26/997129/9913771261997/29/991427/26/997/29/991437/26/997/29/991447/20/997/29/991457/201997/31/99DescripitionMisc Metal debrisMisc Metal debrisMisc Metal debrisLanding MatLanding MatLanding MatLanding MatLanding MatConnexnet Wt. Loaded Tare G ross Wt Total Wt.18797/29/99716868988917/29/99712087/29/997121516897/29/9901689771, 7/29/99077111307/29/990113014017/29/99014019697/ 31/9909699759500050005000147592592322268/6/998/6199Connex Gross weightContaminated Soil14348/6/9972592322278/6/998/6/99Contaminated Soil16098/6/99716162592322288/6/998/6199Contaminated Soil14318/6/99714382592322298/8/998/6/99Contaminated Soil11898/6/9971196269232230816/998/6/99Contaminated Soil14348/6/99714412592322592322592322592322592322592322312322332342352368/6/998/6/99816/998/6/998/6/998/6/998/6/ 998/6/998/6/998/6/998/61998/6/991538142110181386148614968/6/998/6/998/6/998/6/998/6/998/6/997777775000,15451428102513931493150350002610682610682610682610682610682610682610682610681891901911921931941981997/ 25/997125/997/251997/25/997/25/997/25/997/28/998/1/998/2/998/2/998/2/998/2/998/2/998/2/99812/998/2/99Contaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilContaminated SoilConnexConnex Gross weightLanding MatLanding MatLanding MatLanding MatLanding MatLanding MatQuonset Hut DebrisQuonset Hut DebrisConnexConnex Gross weight122912441755745101412367617948/2/998/2/998/2/996/2/998/21998/2/998/2/998/2/99000000005000122912441755745101412367617945000Inspection date , 817/991441155195000205198778500013778Weight SummaryDebris removal and Containerized HTW RemovalHTWDebrisActualc Weight toDate()ActualWeight toDateSitesStained soilContaminated SoilActual T ActualWeight to c Weight toDateuDatesSite 21600020024985Site 377067360011500Site 4/Area 4A541012348214024240Site 4/Area 46905022301764225Site4/Area 4D1000294807418463Site 5315113104700resite 5 and 355Site 635078970Site 7150Site 811500073936620085842340Site 1013000230010168540Site 12100798255078297830Site 1330034300010400064900100299200Totals 12725595169 16140Percent of Contract Wt75%47704 40000296%Page36383 104000 6490091%62%1Asof :811/99,8 :00 PMEnvironmental Quality Control/Qu ality Assurance ReportEll 415. 1 . )02)Cantrw Number / Defnery Order Number,UPCJProfecl Ti0&DACAUS. IJ-0-OQIWD. O. 0004Debris R .rtwval and Con talnortz .d Hazardous and Toxic Wash RemovalCQC Report Numb ..Date or Time P.rioaLocation and Team99-034Nd91Oaenbell. AlaskaW.atfNr CondflonsTemp Low 46 Temp M 44Wind speedF AIM .11 KnotsContractorConditions poly dougy_041 spin Consuftanb, ktc.a .Uty Control inspections Performed This Del . (Yndude wnpectorns . resurb, defiuencies observed . and corrSCbve .ceon .)Prapa,lpryr 0 ee. ae.ched dieca .eMal0dncMNFolbwdlpa Debris and HTW remove)CCD performed final inspection on Sites 2, 3, 6, 7, 12, and 13 . One item of debris found and flagged in Site 2 . All sitesready for OAR inspection .was the deeaency backing list updated this daisField Sampling and TesdnpHas field Mating been performed this date ?Type of testYes 0 NoYes 0 NoL4e0wd/MWmQuantity of srnplesResultsNO FIELD TESTING TODAYHare Data Ouelity Objecli res been achieved? WAYsO NoQHer . S.mples Been Collected for Laboratory Analysis?Ya0Toe of Teat EPA Test McRwd .tatnxQuantity of SamplesMooNO SAMPLING TODAYHave r.gLwvd amount of OC trip blanks and rirtsates been adweved ?WACY.QN0OHem appropnab OC laboratory tests been ordered 7 (matrix spikes, method Banks, surragafes. reference standards. M)WAQYssGNoDHave QA and OC samples been collected in the specified qu nbtyrt Not required by Delivery OrderWADYesQMo0Have samples been properly labeled and packaged ?NAQYesONOQHeat and SafetyWorker prolecs an levels Tim data :LevelA0Level B 0 Level C 0 Level D ° WA(3Was any work acclivity conducted within a confined spew? Yes 0 NoWas "workwork activity conducted within an area detain ined b be immediately dangerous to life and heal h?Yes 0 MooWere approved decontamination procedures used on worturs and egiApment as required ?Yes 0 MooSafety conxnee: (rndude any infractions of approved safety plan . and include in actions b&n Government personnel. specify conectrw action tak n .)The Superintendent addressed the need to pay attention to your working environment . Awareness of the conditions andactivities in your work site was emphasized as the foundation of 'Safety Awareness .' Examples of specific hazards inthe working environment were discussed . These included heavy equipment operating nearby, slippery conditions whileclimbing over rocks, and sharp pieces of heavy metal debris .OAR SAFETY COMMENTS :. r n/ l'>1 rS -1-b ShJeI L< cti MdtAr .'f~N ChJ~7"~ .v..~'SE,4-, M- a,K-,ctVN i ti ,Atyr id 'L-5 .For- 5c`cY.,..-S 'rte C o---,C-?-T th 5p 0-R ~Wevl-r-N <p..Js d F- L4pj .}D> n'.l,. Ld ~I51 rW M c-+r'" %W6 7-1," &5.., C S,rt' mar .-~- s r. 2a-s cf O&-OL.~J w~ o af .,Td LSEnvironmental Quality Coutrol/Quality Assurance Report(ER 413.1-02)Continuation Sheett ActhIbes Perforn" This Oftonce (NAS D NTech Spec 5)Adtvity 4 LxcatianOuantrStrrvsd Sad Remove! ( W\S D 0019. 02030)1 .977 b of prsvbusly- ao4scfsd stau+s0 soil processed today,34 .260 b of StsmW sal rsnwvs0 b dab props-AwigHTW Removal (WAS D 0022 .02030)No HTW was p ssed way47 .704 b of HTW removed t0 dote prc ed-wideDews Remove/ (NAS D 0020 . 02030)9.531 b 01 doWs from snsa S. and /or was proWSed bela yT hts mcfudal ttw trst sectors ot the Navy sonar note95.169 Ib d Oebns removed b daft proled .wrdeContaminated Sod (HAS D 0016 . 02220)9.655 bed contaminated soil was weighed and badsd todayAgproamately 5 .390 lb of soil bagged but not weighed74555 of contaminated Soil weighed 10 daftManpower and EqutpmsrtLaborcusslticadaProject MV49WCQC System Manager54gennilenawtOPWOWLaborwaContractorEQUIP-Number01111Mant1 ouvs1213SType4w1wie ra12Cat 426 bans1312NodwesPickupCat 966 LoaderCat 973 Track Loader12Total Hours:Number Hours Used330136W101121103183Total Hours : 106kˆwcttons Given by the Govern wnt to the Contractor (kldude names , rtac0orts, and remain .)Verbal Q WAtten QNONEWork Progress Are there any Contractor caused delays or poterrbal ftndirlg of bet?M tier any Cvam wnt caused decays or potentia l Ending of tact?Are twrs any wftreseegbpe or wwtw related delays?Yes QYee QYes QNoNoNoRamaArs (Y+dude any visitors b p" W and rtwscallaneas remarks pertinent b work)NONE .I csrtity that 9w strove report is complete and c0l, and that 80 materials and eQu/pmen t used . wart performed and tests conducted during dlis period were n strictcompliance with the contract plans and axoept s, n oted bove,_r .A . .nN P~ .M..d Yin .n .r lL.n .h~ 'w/~~~ C/~. rGovernment OuaUty Assurance CommentsConcurs with tin OC rspoi?Addibonal conifers or exceptions :?'1MS .M, .4iCYes IS No Q(a- roc P . T I rir 5 a M . . .ateo~ TES s rv ]-~. .~ L O ~- ( A t e' `T O r= -St+ t Pub, rv ~s'_ I'~14 JA TT'1G .-rUC- A PPi - K t .ve G t+r'5 N tr- a r~la~ G u(- 5 .McEV 7 ~G`TTarY u~u' !Z~ o c.o -td .C. Lort/,7~ i4> - ~-u Š t c 4 fTsib b T‡:>A-T-&Ct~vt~.~.-zc 1E S.1 tc_i C- tf c~*A4-.DA,-t'-ySe f1a-)>Z 1s w oe-ic% .v G. lrvto)03-, M o r> QOOAR Sig99 .034Supsrvfton' s lnmal bet .+&,FOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage . Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate : ,'Activities Planned :1999Time : 7'. U yBriefing Location :04L] r : / k Gcc ~• C-11[411Briefer: (-0g(1 C X k,'~T H'Topic :Topic :Topic :BrieferTopic :Topic :Topic :Attendees_;&~711r~77Site Healthand Safety Officer :Date : 9--M1999Weight SummaryDebris removal and Containerized HTW RemovalUActualWeight toDatecSites0UoUContaminated SoilStained soilHTWDebrisActualWeight toDateActualWeight toDate00Site 21600020024985Site 377067360011500Site 4/Area 4A541012348214024241877Site 4/Area 4B90560122301764225Site4/Area 4D1000636107418463Site 5Area Derween315257204700site 5 and 355Site 635078970Site 7150Site 811500077791620085842340Site 101300221230010168540Site 12100798255078297830Site 13300343000ActualWeight toDate1040007455547704 40000 38260 104000Wt82%296%96%7455572%100299200Totals 127255 104700 16140PercentofContractPage 1Asof : 8/8/99 , 8 :05 PMEnvironmental Quality Control/Quality Assurance Report{ER 4I -I-)4 nUPCJPrq .d TdContract keumb.r f Delivery Order NumberOACA$Sg7-0-M O10.O. 0004Debris Removal and container z .d Hazardous and Toxic Waste RemovalCOC Report NumberDote or Time PeriodLocation and To"9"35S19r9!Oamb.ll, Alaskawe~ Co wodoruTemp Low M Tamp M 444Wind SpeedContractorCond*lons osrtiv dandy .16 - 31 KnotsOil Spill Consultants, Ire .Q+aOty Control Inspections PerormW This Date (include rrapectfons . resurb . degaenoes obserred, are correctve acaon )Prep aratory D w a$eclsd doctaalD a.a ae chi d cS5ck tVitalFollow-up•mate"' M'eipht trsckfn9The CQC completed an internal audit of weight tickets and the tracking data base . Several duplicate entries and oneomitted data entry were found . The data base was corrected, and the audit routine rerun . No errors were then found .Was 9ne deiloenc tacking sst updated th is daleY ea OFleid Sanp$ng and Too"Has Mid lesbng been performed this deb?Type of 00NoYes(:] NoMadnodAAMnxQuantity of samples ResultsNO FIELD TESTING TODAYWAY.. NoDHave Dets Qwkty Objecfhes been achieved ?YesD No•Have Sw Ies 9 .en Collected for Laboratory MalysIs?EPA Test MethodVm xOuanbty d SamplesType of TestNO SAA42LM TODAYHave reamed amount of OC IV Marts and finales been adWAd?,Have approprtste OC laboratory less been ordered ? ( matbc sprint, method blanks , surtogates reference standards . at)Have oil aid QC samples been coSecied h vie spe i6ed amntM Not required by D.Nvery OrderHave samples been properly labeled and packaged ?WACYesONoaWAOYs.ONoONiADYesONOONIACYesQNoOLevel A O Lev el 5 D Level C O Lave 0 • WADWorker protedfon levels leis dole:Was any sat activity concluded wi9m a confined specs? Yes l7 No•Was any .ak activity eandudsd wi iin an wee determined b be immerhatety dangerous to life and health? Yes O No•Yes 0 No•Were approved deoontamrsa0orn procedures used on workers and equipmera as required ?Sty Corrrnans: (include any infractions d approved eddy plan and include instructions from GovermneM personnel. Specify corrective action taken .)The Superintendent addressed reemphasized the need to adhere to level D PPE . He stressed the importance of notletting wear of hard hats, steel -toed shoes, and safety glasses get lax in the closing days of the project. TheSuperintendent also cautioned personnel to use care While working on foot on rocky terrain . It was emphasized that slips,trips and falls were one of the most common causes of site injuries industry-wide .CAR SAFETY COMMENTS :fN t-~-t.~ C ovv D t Y--o -.- r ~s~S~-C i~ a"C--n,- / A'c' Lade, S. Er4-N f-:-S A'F_ hJc~LT'S rtre ..~y1 es'4x J~tif r e~'S °'~-' E2 ove- rl)'An e r.AQ ", A' G 'Ti't wcY-5 F .LArx+ r,c ~Lc lG/?-o CK 'FLa e 5-1 r"‚hr-~Dw-t -YOLtiCc CZ5 .15,Wart Activities Performed This DateR.terenoe (14AS D $I Teth Spec 0)Activity & LocationQuantity ContactorStained So l Removel (NAS D 0019, 02050) No stained sod was processed today38.035 lb of stained soil removed b date posed-wipeHTW Removet (HAS D 0022, 02050)No I TW was processed today48.642 b of HTW removed b date protect-wideDebris RamoW (HAS ID 0020.02050)No debris processed today104,700 b of Debris removed to date protect-wideConfaninabd Soil (HAS D 0016 , 02220)9,655 ft of contaminated sod wee weighed and ceded today$1,247 b of contaminated Soil weighed b date .MOM sod bagged tut awaiting Pansportabon1Environmental Quality Control/Quality Assurance Report(ER °t s°h 4Rt)Continuation SheetManpow e r and EquipmentLaborCfue+Ncadonprgect MWM9WNumber0tCOC Systarn Managerswerve andenlArcth.akgVttMan*ours012131212121351OperabrLaborersTom Hours:EquipmentTypeNumber34 wthee/erCat 426 ioedartNodwMletHours Used303480aidanpCM 966 LoaderCat 973 Track LoeGr12103ttaiTom HoursInstructions GIv .n by the Government to the Contractor (Include names . reactions . and reworks )106Vwtai Q Written QNONEWork progress Are there any Con acbr caused delays or potential &v *V of tootAre thre arty Government csu"d delfts or po Ending of Awt?Are there any tAoreseeable or weaQher relaeed delays?Yes proe pnee pNoNoNo •Ramnerks (b duds arty asias lo pr*ct and macearleatq re-rim perbnartt io work)Preliminary results of samples taken earlier in the project were received to for the contractor's anchorage office andprovided to the OAR.A number of mechanical failures in the Argo fleet slowed production on stained soil excavation .I certify that the above report is comp/ft and caned and 1hW all materials and equipment wed . wor k perbmed and tests conducted during this penod were in stricxComplianCt with the ctxib hx plarhs and apedllca0orhs emmtxpl as nole0 aboh) ..control Manager SignatureL/L+r27V'/1Government Quality Assurance ComrnenfaConcurs with ft OC report?Additiond tommsr or e)capeou-Vc.l.1/%--"Y,/7-Ewe,YestNoC.0A . h. eve C.E T"Tt &JG luweg l .W-r5 of ~g c.,rn 3L r ~~ .-"S h nsD rvate t .v G'~.,-K>4-t . k t r4( o K-c~" t .cJ~- s< L _ , -rAr So T" Y~'1 A L-?-,F1rv5 ox .,S ,f-,2~ +n,cv .U n ti G .~ J~II c c~ s599-0332CEP-J071Continuation ShectMartposr and pulp~LaborC1eeeMkad"Protect MensgrCoc Sywm Mw"wBLvwvftvwg"U "*W01>aItaNlw.ra0010101312410908012LaborersNumber4161Type4 wNSMerC411426 badeArgoNodw.aPkla,pCat 906 Lo.drarCat 973 Track LoedaMoue Used30224061210111162Told Moors:Tow HM"Instructions ON .n by the Gov ernment to Ow Contraobr (hctude rwnes. reocwm . and rema1 .)96Q W. no Ovtrea/NONElftlbelr Program Art two any Convacwr caused delays a patsi t v*D d tact?Are them any GowwWWO caused dMaye or poMdlal Sr g or tect7yes O NoYea O NoNo 11yes OM Mrs any urdoreseesbla or weeew related dMeys9Rwri.ets (Viduds any risibrt 10 prgtd and mboMleMan ramerlez P W%rMV b work)A eve d the Alaska DOT called and requested that connexes be kept out of the north approach zone of therunway . All cortexes were moved within 4 hours.The OAR and the COC presented a briefing to the tonal native corporation board of elders . The progress of the project to.date and the projected schedule ware covered . M question and answer session followed1 asrOry flat to a m s repel is cmnp4a and coned WW that 61 malertala and puiprtant used, work perbmsd and tru corl0txyad dump 54 psrsod wen in w1aooenpiero.4th M contract plane and apedpCabre a+eept as rroled abOW. Conun.nts.Government auatRy AssurancCaroms we M QC rspnrt7AdddkxW aorrrrlenb or errCepOorr :Ce0„=Dl &I kr' aV%,Yu )lo O~FTrfCZ-T~SI~ F3 yc9 - wv~~,4#,p QC- t.to7" C h vN~ C Pr71 "RD e t~v>z-~-L .V` re k' -41- "rg r t_ 1 .4y > I a~ }oW%4-,,A401,1L,tJ O-W )CI &J GT I tZ3 c, T7 ^-,a -F4 c .7 e ,6- / ors 5 Ff t Pr T- .A,n4UJ r LL t!e vq er,/ + TN LesSL1 eL -e172- mil 5 et t P rSS tJ pT'r'4-hu'll'o owe-DcSeMo>° o, .f tc..;~g .4°CEM77-~2Stlva z t- g4,t3t.as-i-ts6GevoSupavbors trdtial-2. rt*-a esC a~ ° v'dYz C)KC i`"r g a 5 j?>or-~,,n,,,efl,, ..~-tttaw' tupeaMar AVil-t L_/}t3c- -99-036s r-Ac i cw wt rie- ; o.v s ., p G ec ri-1.1- r~*r- llS,.*r 15 1Orfr Lc,t'0 S Can Qt- -fw~TssFc,a,~ 1 rt o^ -)S .GAr, V at rJ51-AV--J f:->, ;;-raOIL SPILL CONSULTANTS . INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title:Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell . AlaskaDate:In 1999 Time : O7 C2)OBriefing Location :Activities Planned :Briefer :LPC ~ ~ try ~~ t ti ~Topic :Topic :Topic :BrieferTopic:Topic :Topic:l) AttendeesSite Healthand Safety Officer.Date:1999Environmental Quality ControUQuality Assurance Report(ER 4nyr- MCnContract Number I Oetiwy Order Number :OACAU .97-0-001010.0.0004UPGPro1.et Ties.O.Orb Removal and Contatn.rQ.d I4a srdous and Tonk Waata RemovalCCC Report NumberDate or Tim. Pe riodLocation and Team!l-03711111!Gambef, AlaskaVV*~ Condition .T.n.p Low N Temp H AContractorConditions aMy tdoudv .Calm -11 Knot!Wind SpeedON Spill Consultants, Inc .puapty Control inspections performed This Del. ( trnclude respecaons . moults. deicrencles ooeen d . and co' ective ac I )Prep .r,MOry 0 eve ae.cMd dncaaSIn" 0 we aladnd 0--titaMat .Aal handlingFollow-upA final inspection of multiple sites was conducted in the evening by the CAR . contractors Project Manager, and theCOC . The results area as follows :Sites 2 , 6, 7, 12 , and 13 - Completed SatisfactorilySite 3 - Complete debris removal at higher elevations but only where terrain will allow work to be done safely .Was tie delioency talking 10 updated this daleyes0Field Sarnpang and TestlnlHas Nrd ksbng been part mod this dab?NoYes 0 No ataednodAMatrtitTyped tatOuanaty or samplesRssuftNO FIELD TESTING TODAYbeen schwved? WAmHave Data.Collatedfor Laboratory AnahslsMove Sernptas B. .Type d TatYq= 0Yp0 mooOuaity or sample,EPA Test MetTodAvtavaNO SAA43LIVG TODAYHave, required .most d QC to blanks and rinsates been adwe ed?Have appropriaMe OC laboratory Mete been ordered 7 (matrtic spikes . rneenod blank. surrogates, reference standards, side)Have OA and OC samples been oJected n /x sped /bd quantity? Not required by Dalh.ry OrderHave sarnpies been properly labeled an-4 p g!0WADYeONoDWAOYspNo0N/ADYMONoOWADYs NODH.sRh and safetyWorker prusec i knela Vie date: Level A D Laval S 0 Level C 0 Laval D 0 WADwas any wont acltvty ccndnuofed ie1wi a oonrirnd space ?Ys0NoeWas any work .cift* card to within an area determined b be immedialely dangerous b life and heafln?Yes (3 No ardW6WproceduresusedonWorkersandequipmentasrequired?were approved decoM.Yes 0 NoaSafety Comments : (IrrAde any 1*at lion . d approved safety plan, and include insiYUCtions from Goverrwnent personnel Speafy corrective action taken .)At the safety meeting, the Superintendent focused on hazards associated with the ongoing operation to move connexesfrom the south staging area to the barge loading area in the north . Operations were planned to avoid routes heavilytraveled by the egtupment form another contractor in the area. The need to practice caution with respect to the ATVtraffic from the village was heavily stressed. Work was scheduled to have operators move connexes in evening hourswhen local traffic is light Special attention was given to total operating hours and crew rest for the operators working theevening shiftLater in the day the Site Health and Safety Officer observed the connex moving operation . Operators were using careand interference with local traffic appeared minimal .OAR SAFETY COSw1af tL,a a eL . U-n r v o~ n -S Ar 5 t G E To V P'0+T fig ti '~ . ~ 8 c vt txv St r.,~y P~ c . rL . 01nJS+V-t:-ry A r-F'(yu , ./ s5r2<,wtS.E L_ tLt/Ai' L a, Dsc ' 4 5 5~~j N e, .-'-… t +rnr o …g,e t5 .[h> S7 k3t . .E . 1UE W%-L- 14Cl- Sw bc, Or 514 t? 4vi>o2xroye 14ov+ 7 .icrU' `~-tom"', ~ Kr7 -v-e~~,,,rr. G~rtw ReST l,5 Ajj e-~1> "rd do-/t y,*- s 4'f "'LSr- w aI1 15 i5.t(51,N)c , , K o u~A'T , N+--Environmental Quality Coatrol/Quality Assurance Report(ER 41}1 30MContinuation SheetWont ActtvIMs P.Awnwd This DabR.Lrance (HAS D WTedt Spec AAc9Mty & LocationQUW"cƒw .aorStared Sod Removal (NAS ID 0019 . 02050) No Stowed $d was processed today38 .03$ b d Staw4d tbi remote b dale protect wideHTW Removal (WS D 0022 . 02030)605 b d HTW was processed today49 .245 b d KTW removed to daft prgecl-wpeThe last debris *am She 48 was moved todayNo debris was masd .104,700 b d Debris removed to dale proteCl-w,pe8 .634 b d ca vton*lad 909 was WOWted and loaded todayAddbonal sand bpi are waryng to be ..eelE„avap0n estimated to be CornpieW .90 .829 b 01 carRarnired Soil wegned to dateNumberHours Used482400Debris RImo(NAS D 0020 . 02050)Contanwtated sad (NAS D 0016 . 02220)Wnpower and EqulpmertLaborclass" catdonProtect MsnparNumber0ManHours6COC 9y-Mm Mrtpar114Cat 426 loaderSupertlsndent11112131213136ArgoArchoofopstOperatorLaborersTotal Hours:EquipmentType4 wheeler4161NodwellPickupCat 966 LoaderCat 973 Trade Loader112110101193Trial Horn :122Vorbal 0 Wman OIrtatnurions Given by the Government to OW Contractor (Include names . reacdons_ and rents.)NOWWart Progress Are there any Contractor caused delays or polsntial finolntg a fact?M 8mre any Government causal delays or pollor" 6ndng d fact?Are 8,are any ta*r seembit or weafw related delays?YesYeaYesOOONoNoNoRomarfrs ( bsdude any vi7ADr$ to prged and rtes arreola remarks perbnerri to work .)The contractor 's Project Manager , Mr. Randy E . Easley arrived on site todayI cer4/y 91st ttr . above report is 0ompkls and cartact and 91st all materials and eq iprrrrt used . work performed and left eondrctsd during 914 period were in smaompiartca with 914 00ntrad pans and sped6a6Cns sxept as noted above.Government Ouafity Assurance CommentsComaswilhAddeorrl nitertts or aocepbolw:S.-ra 't.L9T.ferr ,-19eOCreport?Yes k NoNo 0~j ~t1ittit7 isic~Lt ~C- `s'j°.ts6~r~et~4*-t__A'WPe~Os~l n .i G Cv~ _ UZ v n. ` 1R1 ,~ .~tL 1 ` --'2,~f7~ let 113gemC rr &Q ' ' .PLJDOAR SigSupervbors Initial2DateOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage . Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambeil, AlaskaDate : -61A q4 1999 Time : C776&Briefing Location :Activities Planned :J&l f xculru-1rG/)Qr, ( 5Briefer:Topic :Topic :Topic :BrieferTopic :Topic :Topic :a'4'0Je"!'Rt,l i V -dWeight SummaryDebris removal and Containerized HTW RemovaluSites89SWeight toc85ActualActualActualActualWeight toDate9Contaminated SoilStained soilHTWDebrisaDateWeight toDatec8Site 21600020024985Site 377067380011500Site 4/Area 4A541012348214033621877Site 4/Area 4B905601223017640SIte4IArea 4D1000638108308463Site 5315257204700site 5 and 355Site 835078970Site 7150Site 811500077791620088842340Site 10130022123009280540Site 12100798255081547830Site 13300343000104000Weight toDate90892Area MAWR100299200Totals 127255 104700Percent of Con tract Wt 82 %16140 49247 40000 38035 104000 90892305%95%87%Environmental Quality Control/Quality Assurance ReporttER_41 i $-31M)UPC o Ct Ttd.Cons.d NuT+W( / Deavey Order Numb(O.brts Removal and Contalrvetzed Hazardous and To xic Waste RemovalOACAa.17 -0-o010ID . O. 0004COC Report Number",4MDate or Tkn. PeriodLocation and Tees$/12MGamb. ll, AlaskaContractor. Cavdlt/orvsvv.Tamp Low 41 Temp Pf !MWend Speed6-16KnotsConditions ft .Oil Split Consultants, Inc.Quality Control Inspection s Performed This Deft ( Inck a inspections . results . deliuenaes observed . and corrective action )Prspwalory O w seach .d dv.caarMleerOse" ranched ch .daatFoNow-Up • Debris Removal Stockpling o/ debss removed Sites S . 3 . and 5 Work gang welI . no defosnoesWas Iho de loervcy racking list upda ted fhis daftField SampNng and TestingHas field lasting been performed tws dais?Type of artYes O NoYea O NoMef XY MMU Quantity, of samplesResrrlttNO FIELD TESTING TODAYHave Data Quality Objectives bee n achieved? WAHave Samples Ben Collected for Laboratory MalysW?Type of TeatYesOYes(:)EPA Test Mefhoc Ma&uNCONomQuantity d SamplesNO SA W>LING TODAYHave regi%ud amount of OC tip blarWs and riroatas been adreved9. surrogates . reference standards . sit)Have approprtale OC laboratory tab been ordered 7 (matrix spikes. me0wd blanksHave QA Mid OC senlptss been collected in the specified quantity? Not required b Dellvey OrderHave samples bee n prmpsly labeled and packaged ?N/AOYSSONoONIAOYssDNoONAOYssI]NOOw Yes0NOpWorker and sanerWorker projection levels In data:Level A O Level 9 (3 Level C O Level D • NUOYesONoWas any work activity canduc ed einrn a cn * eel specs?Was any watt ectiwty conducted within en area determined b be immedately, dangerous b life and heft?Yes O NoeWes approved dscorrryrnination proesduns used on waters and egupment as "Pried?Yes 0 NoeSafety Comments : (1r'cti a any infractions d approved safety plan . and include nstrardions from Government personnel . Specify corrective action Islam .)At the safety, the Superintendent again addressed the hazards associated with the ongoing operation to move connexesfrom the south staging area to the barge loading area in the north. Routes were planned to avoid interference with localtraffic and avoid the construction area for an ongoing airfield paving project . Special attention was given to operatorworking hours and crew rest to insure that personnel were rested and alert while operating equipment .Later in the day the Site Health and Safety Officer observed the connex moving operation . Work was being conductedsafety and without interference with local traffic .QAR SAFETY COMMENTS :4PgVCl &,5,1-LL.-r'R S A c.-Vi-,-0L."X., S *- Ft ES f 7uHvo W tTLfI3 Y2p,,'l -.CT'2. W r'.Y1tc /i U 4j; .D .rEnvironmental Quality ConttroUQuality Assurance Report(ER 41 5- 1 .3a21Continuation Sheetyllbrh fr vIlea performed This DebReference ( HAS D WTedh Spec 8)Ac why & LocationQuantityStained Sod Remo.d (MASK) 0019. 02050)2 .450 Ib d stained 50A was processed soday Mom Onsn cleaningand processing t rougl'oi4 Oe protect.40 .085 ib d Stained Um rammed b date prorea .waleHTW Remd.M (NAS D 0022 .02050)HTW rsmcwi from arc h oo/ogical site r.0r4h of the n%hwsyIn site 6 . The mountain sift. She 3, and Site 5, the caDteburial artm up the mountain side was c wn%eted WayThis HTW has yet b be weighed .49 .247 lb of (1TW ramowed b dale protect . .,deebris Ramrod ( NAS D 0020. 02050)Debris remwol from ardneoiogrral sit sow th d the runwayin site 6, The mountain side. Site 3. and Site 5. the cableburial area up the mou*am $ite was Completed WayThe Navy cable in site 10 was picked up w d ay05 .237 Ib of Doors removed b dft project-wideConractor537 Ib d debris processed. More yet ba be wegeedCordaminaled Sod (NAS D 0016 . 02220)Manpower and EqulprrentlaborPnbl.ct merwerCOC Systrm t ,AanagerSupwkiiendardArdwftgWOperatorLaborers103 .969 Ib of Conbmnaled 5d wtbgne 10 dateThis darn Complete2.450 Ib previously excavated contamirsased $0A .was weighed and loaded way complebnp this her .NumberManHours11211111212131212138EquipmentType4 wheelerCat 426 loaferArgoNOdwelPickupCat 966 LoaderNumber416111Cat 973 Track LoaderTotal Hours:Hours Used48044S12e01199Total MOWS .tlstrutdtl0ns Given by five Government to the Connector (tidude names . reacbore. w remarks.)verbal0M1101,11713The OAR approved an alternate seed mix for tundra planting . Memo is attachedWoAt Progress Am tiere any Confsctor caused delays or potential finding of tact?Am flare any Government caused delays or potential finding of !ad?M fare any umtoreseeabl or weather related delays?R,amarb (Widude airy welters b project and micttanearsYo OYes 0Ya.ONoNoNoremarks pertinent b worth-)Weather cancelled the scheduled arrival of the Resident Engineer from the Fairbanks Resident Office, USAGE .The project Archeologist monitored debris removal from archaeological site XSL-005, annexed to Area 8 ., MonitoredNavy sub-detection wire removal from archaeological site XSL-002, in Area 5, Navy sub-detection wire removal fromhillside adjacent to archaeological site XSL-001, in Area 5 . and Monitored debris removal from among grave boxes inArea 3.I certify fit go above report is complete and correct and hat at materials and egt4proerd used . work performed and tests oonduct .d during in period as, in strich -1 1above .compliance with t e cweract plans and specifications 6311"trant anutunDebGovernment Oualhy Assurance CommentsCongas with five OC report?Addbonal comments or wcepiona :Vtorcheir' 4r 17 (--)~-`ryG-r'2't` r.am.11010/slgmtum-~99MVI-P,aYUXNDr%Yk0-, L AAs, &e, r53AO-rat P ti>gu,`,-,~&V,6710" h44- Nor YET ,2 ,0+0t is(j,t)sr.e g ! ? 3upervl. or's Initial217--- --1- --Weight SummaryDebris removal and Containerized HTW RemovalHTWDebrisActualWeight toDatecSitesContaminated SoilStained soilc‚ActualWeight toDateSite 21600020024985Site 3770121060011500Site 4/Area 4A541012348214033821877Site 4/Area 4B905801223017840SIte4/Area 4D1000638108306483Site 531525720470078970Area DeTweensite 5 and 355Site 6350Site 7150Site 811500077791620088844790Site 10130022123009280540Site 12100798255081547830Site 13300343000104000103969100299200Totals 12 105237Percent of Con tract Wt 83%1644949247 40000305%Page 140485 104000 103969101%100%Asof 8/12/99,8 25 PMOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title :Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location :Gambell , AlaskaDate :1999Time :Briefing Location :o-'k 0~(rActivities Planned :fBriefer :`Ite 7oTopic :Xc" ~nn,GYt,~to l-Topic :Topic :Briefer.Topic :Topic :Topic :AttendeesW, ZDate: 1 01999rte ~`Environmcntal Quality Control/Quality Assurance ReportnEft 1I%1,to.')Contract Number I OWKWy Order Number .DACAUS91Z-W0/0 . O . 0004UPCJProlect TitleDebris Removal and Contalnertzed Hazardous and Toxic West. RemovalCQC Report NumberDate or Time PeriodLocation and Team9!-0318/13/99Gamb.l, AlaskaWeetWr ConditionTemp Low 44 Tap N 111Wind SpendI . /S KnotsContractorOil Split Consultants, Inc.Conditions leo a m - sumo p mQuality Control Inspections Perform ed This Oat. (Include inspections . results . deftaenues observed . and corrective action)O s . . .e died cMckIMPreperasoryttAal0 s .o aesdee U.ctl.rFosovwUpa Debris Removal Demolition of Navy Shack . Sle 10 Work going wen . no deflcencxsFinal inspections : A final inspection of multiple sites was conducted by the CQC and the QAR . The following were theresults :Site 3 - The deficiencies identified by the previous final inspection were corrected satisfactorily by Daniel. The site was accepted by the QAR .Apassingok . Robert Tungiyan , and Gordon OozovasekSite 4a - The site was accepted by the QAR without deficiencies.Site 4b - The site was accepted by OAR contingent upon completion of the attached punchlist .Site 4d - The site was accepted by QAR contingent upon completion of the attached punchlist .Site 5 - The site was accepted by the QAR without deficiencies .Site 8 - The site was accepted by QAR contingent upon completion of the attached punchlist .Was the deficiency racking tit updated this daleField Sampling and TeeingHas Reld testing been perbrmed this date?Type d testY .e 0No aYes D No eMetlrod/Matrix Quantity of samples ResultsNO FIELD TESTING TODAYHave Data Quality Objectives been achieved? WAHave Samples Soon Cofcted for Laboratory Analysis ?Type d Tat EPA TestYesoNo(:)Y.sO MooMedvd/MatruQuarmtyofSamplesNO SAMPLING TODAYHave required amount of QC tip blanks and rmsates been achieved?NAOYesONoDHave appropriate QC laboratory tests been ordered 7 ( matrix spikes . method blanks . surrogates . reference standards . etc) N/AOYesONoDHave QA erect QC samples been collected i n the speared guantiyt Not requi ed by Delivery order wAOYesONo(Have samples been prop" labele d and packaged?NADYesONoDHealth and SafetyWorker protection kveis In daft : Level A D Level B 0 Level C 0 Level 0 e wADWas any work acbwty Conducted wenin a conch ed space ?Yes 0 NoeWas any work activity conducted wietin an are d determined 10 be immediately dangerous to life and he i h?Yes 0 MooWere approved decartanwkaeon procedures Used an workers and equipment as required ?Yes 0 NoeSalety Canrnents: (Include any i.Nractlons d approved safety plan. and include instructions from Go eroment Personnel . Speay correClhe action taken.)The Superintendent stressed the importance of radio communication and strict adherence to the buddy system for crewsworking in remote sections of the tundra . Planned work include collecting Navy signal cable from remote areas of thetundra. Crews working in pairs must insure that the buddy system would always been in effect and that effective radiocommunication was always maintained .GAR SAFETY COMMENTS:U c>ON-'tst 5 .w 4' t ,e-i'-f 0'&!z _Isue= ETY keve, Low SEnvironmental Quality Control/Quality Assurance Report(ER °151-302)Continuation SheetYllort Activ11ee petorm.d This OMsReference (NAS b WT .c+ Spec 9)Acsvlty & Locationouanerystained Sod Rsmo.S (NAS 0 0019 . 02050)No stained sod was conecled or processed .40065 10 d Stained sod removed to date p pw OeHTW RsmovM (NM 0 0022 .02050)No HTW was collected or processed49 .247 b d 11TW removed 10 date poleci .wideDebris Remove/ (NAS 0 0020 . 02030)Debris removal acbvlbes nduded demokbon of 6w NavyCable shack and renoud of ew Navy signal wire kymSine 10105 .237 Ib d Oebns ramo* .d to date pro e,:1,0eCo *avmnated Sod (NAS 11) 0016 . 022201Removal of suppon facibes at Me excavation sine wined103 .969 Ib of contaminated Sod weighed to daisThis rlem completeManpoww and EqutpnnsrRLaborNumbertProlecs thawCQC Sysldn Marlaper1111supwwftx tOpaOMLaborers0Total Hours :EquipmentTyperanHoursCorwacsNumberHours Used124 wnee/er4461313121205Cat 425 loaderArgoNodwettPickupCat 966 LoaderCat 973 Track Loader10406e1110610148Total Hours 102Yatrucoons Given by the Government to tM Contractor (Include names . reac>ioru. and remarks .)verbal• Wrltsn ONONEYes O No aYes O No aYes O No aw11ort progress Are Here any Contractor caused delays or potential Iinrting of tautAre there any GovemmeM steed delays or potential tndirg d fociAre there any kxdoreseeable or weather related delays')Remarks (rhduda any vtibrs to project and misceaneous remarks pertinent Io work)The scheduled visit by the Resident Engineer from the Fairbanks Resident Office , USACE was cancelled .I certify that the above report is complete and correct and that ad materials and equipment used . work performed erd tests conduced during 6rs penod were in s61Ctcomprance with the conaaa pons and speaflcab9 S except as npteSaepveGovernment Quanty Assurance CommentsCantaas with to QC report?AdQktional c r nman or MCGO ins ::1 K/LANtYsr,,N c- f+ L L4 r' 'S ~ c °v G01 ~L 2a~'7 c w r ~S D k° 'cAgopwZ> 0 8 ct~-~-~ 'n ES i1-r" (7 S~`~`+ P L_ t ~~ vr~ 17 t .v'~t`~ v~ .o DS o_A- (2t1QLZT-zc'7~ .~-t~ Lp ~~Tt e f= /t~t_ L9i4i-o/3-s~9 -GSM D/7 -s/fey-?7 36 /Sv~~:-,9 -6 .9 -fz9% 6,9A1 /7 S~Relinquished by : (Printed )(Signature)/ /v3o ySD ate /TimeReceived by: (Printed)(Signature)Relinquished by: (Printed)Received by : (Printed)(Signature)(Signature)Dispatched by: (Printed)Received at laboratory by :(Signature)Me thod of Shipment :Condition of ContainersComments:Good Fair PoorReceived TomEnvironmental Quality Control/Quality Assurance ReportrQcontred Number ! Delivery Order Number :s.t°xatUPC/P"*ectTM:.QACASS- R-0-001010 . 0. 0004 Debrb Removal and Contain erized Hazardous and Toxic Waste RemovalCGC Report Number Date or Time P.Aod loutfon end TomW1319fGambell , Alaska99--0{tCondlllwrsContractoryre.rherTemp Low 44VAnd SpedTemp H111 - 1a KnobConditions Iba a .m ., sunny o m .On spin Coemufdndft ktc.O,&" Control InspedfonS Perfonrrd This Date (rrdude i specbons . resorts . degcevwies observed . and correctrie scow.)1111"ab,y 0 am .aarrrr4 dbeeaatrwal0 as* s0 ectmd tdwaaarrFollow-up 0Was fvo dercpar q vas nq Ibt updated t hisdateYea0NoFlow semparr4 and Testl qVieQNoHas km bsfno been pafbnmed Otia date?Meelod tit slz ouarvly d samples ResultTwo d ledaNONEVisa No•" own Quality 00)ernea been ad eved7 WAHenMay. Ssnpies Seen collected for Laboratory Ana"?EPATest MeecdMarbEType d TomVisa No•ouer" d SamoaNONEWACYnONoCWACYee(NoIWAOYssOMoOWACYnQNOCHave re *ed sn td d QC Mq bterrb and rinsates been aclweved9Have pproprl.b QC 4borabq haft been ordered 7 (mabbr spikes. method blanks, wrrogates . reference standards . sue..)Have GA and QC samples been coaxted In the specMed Oraidty?Have samptw been propelly labeled a nd/teeth are So"Warkr polac7fon levels fileclaimLevel A O Lever a Q Level C 0 Lave oYea O No•Was anywork adrAy condur.'t.d W M a ooryMrd spas?Yes Q No•Wee tryeemt acth Iy oonduCtad all an area dMOI &htod b be h e atefy danger . a b tie and healthyWare apprued dsoord . *w1lon proosdurM mend on workers aid .quipment as regrirard?Safety Cor merr (Include arty I *actfa +a d approved sandy plan , and include Instruraons from Gores menu peiso wYea O No•. Spedfy COrred9ve ad ion take n.)The Superintendent emphasized the need for teamwork as fundamental to a safe work environment The concept goesbeyond simply the buddy system and correct use of spotters when operating equipment . He urged personnel keep awareof their complete working environment. Communication of potential hazards to coworkers , synchronization of tasksbetween personnel working In dose proximity , and general awareness of what those around were doing are vital to a safeworking environment for everybody .GAR SAFETY COM9aENMOAR NOT ON SITEWW%Ac& Perronr .d This OdeRa/Yrerm (HAS D .ITed+ Spec 0)Arlvfy&Locasonotsr+fbConlraclorSite cleanup work completed . Weighing and loading of cleanup material completed today . Cleanup of contractor'sstaging area completed today. Packing of contractor's tools started today .uanpaw.r . nd EgrrtpnrntLaborc1b"McatdonPsolad Marlowcoc systarm amarrpersuperM~MrdwtPichednidtowswtaboorsEquipmentNumber11I17ManHoursType12II13047$4 wheelerCat 424 ioederArgoNadwaPkierpCat 904 LoaderCat 977 Trsclt LoaderTool Hours:120NumberHours Used4$041f11II4440104Tao/ Hours :114M aft uceonee Given by the 0ovenrarr* In 610 Contr .dor (Ir chide names, resdos, and remarks .)NONEfMork Flowsea Ate two any Ca *scor emmed delays or potsn6el M&V d fact?Me fin arty Oov vneik esmed delays or polenfel fti* g d IoWMe two any to* rsenabla or omens related dsMye?QYea E3Yea Q0NoNo 11No~aviroa mental Quality Costrol/Quality Assurance Report .(E/141 -1-Continuation SheetRemaru (1ncAida &V rlalbrs b prci aand m1,adaneam rartlab par U.0 b work)The Project Archeologist . OAR. and one operator left the site today .and 8%M M matartata and spuiprnant aced, wont parlonned and Mate conducted " tt+is penod wen in WICI oarWy &W M …oa raporl h owmplaa and ool'oomomm s win t o C0 110-t plans and spacMcaiOM COWGovanmant OAft Msuranee CormnnbCanaats wm ft OC rapo l?rea D No Q .Addltlonal CarrtnNnb ar a)capUa s:OAR NOT ON SITEOIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous WasteRemovalProject Site Location :and ToxicGambell , AlaskaTime : q GdBriefing Location:U42 GTopic : ____Topic:Topic:BrieferTopic:Topic:Topic:AttendeesDate:1999f4Environmental Quality Control/Quality Assurance ReportER .fir1Consract Number / 13wt .ery Order Numberwh.,UPCiProfect TitleD.bds Removal and Containerized Hazardous and Toxic Waste RemovalOACASS- 97-0 d010IO .O . 0 004COC Report NumberDate or Time PeriodLocation and Team99.0428/16/99Gambel, AlaskaWeatherr ConditionsTemp Low 44 Temp HI 46KnotsIS-20Wind SpeedContractorConditions fog a m Sunny o mOil Spill Consultants . IncQuality Control Inspections Performed This Date (Include Inspections results del c+enc es ooserved and corrective act,on,Preparatory 0 s.. attached ch.ckasthrISMO ..e . itached ch.ckastFollows-1 .1%)0Was the deficie ncy tracking li st updated this dateField Sampling and TestingHas field testing peenType of lestyes Q Noperformedthisdate'YesMetrod/Matn : Ouantny of samplesONoResultsNONEHave Data Qualify Objectives been achieved?N/AYesOMaeHave Samples Been Collected for Laboratory Malysks?TypeofTestEPAYes0 MooTestMemod /Matrix Quantity of SampiesNONEHave regtared amount d QC trip blanks and nnsates been achieved?MAOYesONOCHare appropriate QC laboratory tests been ordered) (matron spikes . method blanks . surrogates . reference standards . etcIN/ACYesCNoOQAandOCsamplesbeencollectedinftspecifiedquantity?N/AOYhONoCHaverrtylabeledandpackaged?MAOYHare sampes been p ope.sONoDH..Rh and Safetyworker proaction levels tss daft Level A O Level B O Level C O Level DWas any work actrety conducted within aconfinedspace?YesOWas any work actrvey conducted within an area determured lobe immediately dangerous to life and healm?Yes0Were approved decontamination procedures used on workers and equipment asrequired?YesOSafely Comments ( Include any infractions of approved safety plan . and include instructions from Government personnel Specify corrective action taken )MAONo•No•Ho•The Superintendent stressed the need to use care while operating ATVs on the tundra . This was important in light of theday's planned activities which included spreading fertilizer on the disturbed portions of the tundra Drivers should not bedistracted by the fertilizer spreading , maintaining their concentration on driving . The proper PPE for handling fertilizerwas also discussed . This included gloves and dust mask type respirators .OAR SAFETY COMMENTS :QAR NOT ON SITEWoAt Activities Performed This DateReference (NAS o !/Tech Spec e)Acbety &LocationQuantityContractorSpreading fertilizer was complete today .Manpower and EquipmentLaborClassificationProtect ManagerCOC System ManagerSupennMndentArcheologistLaborersTotal HoursNumbertManHoutsEquipmentTypetta wheelert11Cat 426 loader1t06120ArgoNodwellCat 973 Track Loader615892Instructions Given by the Government to the Contractor (Include names . reactions, andremarks)NumberHours Usedr480IToo hoursr.0092Verbal O Wrf1t'n ONONEWore Progress Are there any Contractor caused delays or potential finding of fad?Arc there arty Government caused delays or potential finding d fact?Are there any unforeseeable or weather related delays?Yes OYes OYes 0Remarks (include any, nsiton b protect and miscellaneous remarks pertinent to work)2 laborers left the site todayINoNoNoEnvironmental Quality Control/Quality Assurance ReportIt 41S- I .3m)Continuation SheetI cart y f e+. .bove report b comp/N . and corre ct and o at M mae .Aa1. and .qu *m .nt u ..d . work p.r*xm.d and sets c0nduct .d dunnq ews parod were n stnscampiarr‡ wfel e s oon trsd plans and spsciecaeon s s kept as, pasd abotis.Gov .mm.nt Quataty Assurance CommentsConcurs wref e s QC rspori?Add*onal comments or exceptions .Yet 0No0CHAR NOT ON SITEQAR Sagnatur.Dab99-042Sup. rvboes baud2OIL SPILL CONSULTANTS, INC .209 E . 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title :Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location :Gambell , AlaskaActivities Planned :1999 Time : (37x)/.fƒ~iirsZ1,0.1rjBriefing Location :6 0Topic: 0424Briefer.Topic:'~Pz~i/'z~fnTopic:Topic:Briefer:Topic:Topic:~l.~/~~p~~c f7oNAttendeesICC0 d 1- 0 1 6c,Site Healthand Safety Officer,Date :1999. 4///~-Environmental Quality Control/Quality Assurance Reporthot 41 s 1 .14:1UPCfihx4 eCt TAIeContact Number I Dekvery Order NumberDACABS- 97-0-0010 /D.O. 0004 Oebsls Removal and Containe rized Hazardous and T o xi c Waste RemovalCOC Report Number Date or Time Period Location and Team8/1 7/99Ga mbeil . Al as ka99 41143WeatherConditionsContractorTemp Low 44 Temp HI 44Wind SpeedConditions loo, cloudy . intermmtteM acrg ramcalm - 10 KnollOil Spill Consultants, Inc .Quality Control Inspections Performed This Date (khdude inspecbons . results defoenues observed . and correctwe action)Preparasory 0 s . e aftachad ch.ckletIrbal 0 see amdhod thicksetFollow-Up0Material TrackingThe regulatory specialist and the COC performed final correction of the database, re-checking against all original weightickets . The final corrected numbers 142 , 324 lb for debris, 53,738 lb for HTW items , 39,889 lb for stained soil and103 .885 lb of contaminated soil removed by the project .Was the dehoenc7 tracJung list upd ated thus dateField Sampling and TestingHas leld testing been performed tens dale?Type of testYes 0 NoYes o NoMethodi%atnxQuanrty of samplesResultsNONEHey. Data Quality Objedbes been achie ved? WAHave Samples Been Collect ed for Laboratory Analysis?Type of Test EPATest kMethod/tAathuYes(:]No•YssONo•Quantity of SamplesNONEN/AOYesDNoOHave required amount of OC lnp blanks and nnsates been acrieied ?Have apprrphate QC laboratory tests been ordered 7 (matrix spikes . method blanks . s:n*ogates, reference standards . etc 1 WAOY9s0NooHays QA and OC samples been collected in the specified quanta?N/ADYesDNoOWAOYesONOQHave samples been properly labeled and pack s e~Q?Health and SafetyLevel A 0 Level B 0 Level C 0 Level 0 • WADWorker protection levels this date :Yes D No•Was any work activity conducted within a confined space ?Yes 0 MOBWas any work activity conducted within an area determined to be immediately dangers b fife and heaith7Were approved decontamination procedures used on workers and equipment as re„rired ?Yes0NomSafety Comments. (Include any infractions of approved safety plan . and include i hmAons from Government personnel Specify corrective action taken )The Superintendent stressed the need to use care while operating ATVs on the tundra . This was important in light of theday's planned activities which included spreading fertilizer on the disturbed portions of the tundra Drivers should not bedistracted by the fertilizer spreading, maintaining their concentration on driving . The proper PPE for handling fertilizerwas also discussed . This included gloves and dust mask type respirators .QAR SAFETY COMMENTS :QAR NOT ON SITEWork ActlvItles Performed This DataReferent. (NAS ID *Tech Spec 6) Activity & LocationQuantityContractorSeeding was completed today . The silt fence was not installed ( see remarks section) . All contract work for the project iscomplete . All punch list items were completed today . Mobikzation started today .Manpower and EquipmentLaborclasdlicadonProled ManagerNumberCQC System WanagerSupairAendentArcheologistLaborersTotal Hours'EquipmentTypeManHoursNumberNoun Us.d1112144 wheelerCat 426 loader4124105905792ArgoNodwellCat 973 Track Loader601Total Hours160040m and remarks )Insttudfons Given by the Government to the Contractor (Include names . reactionsNONEIverbal0 Written 00Environmental Quality ControUQuality Assurance Report(ER 415 - 1 .302)Continuation SheetYesAre awe any unforeseeable or weattw related Mays)C3NoRemsvts (1neJude any wsnors to protect' and miscellaneous remartcs perbnent b workThe project manager for the sub contractor arrived today .After seeding the crew started erecting silt fence across the few areas of potential erosion . Concerns were raised by themembers of the crew who were local residents that placement of fence across trails might posed a hazard to ATV ridersusing the trails . During the lunch break the CQC . Superintendent, and members of the crew consulted with the ProjectLiaison, Burt Oosevaseuk . The Liaison confirmed that the silt fence could be a danger to those in the area . He alsoadded that local residents would probably remove much of the fencing to salvage the materials . He confirmed that itwould be in the best interest of the local community not to install any silt fencing . Sift fence installation was deleted atthe request of the Project Liaisonii cart,ty mat e+e above repon a complete and correct and ttlat all matenals and equipment used , work Performed and tests conducted dunng this psnod were in sahacom liance coral ale contract plans and specjfcabons exep( as /bled /borecontrol Manager'tJ/,BSignatureDateGovernment Quality A ssurance CommentsCa+CUrswMAddbonal comments or ex epbonstheQCreporrrYes0QAR NOT ON SITEQAR SignatureMeSupervisors initialNo0OIL SPILL CONSULTANTS, INC .209 E. 51st AvenueAnchorage , Alaska 99503(907) 562-7169Safety Meeting MinutesProject Title : Debris Removal and Containerized Hazardous Waste and ToxicRemovalProject Site Location : Gambell, AlaskaDate:i 1999 Time :C) 7 X)Briefing Location :ez&Activities Planned :v+~~ TBriefer:? L~ 14Topic :Topic :Topic :Briefer:Topic :Topic :Topic :AttendeesDSite Healthand Safety Officer :mDate :1999Weight SummaryDebris removal and Containerized HTW RemovalDebrisHTWActualWeight toDateAciuau LaWeight to csite*Datec40Contaminated SoilStained soilActualIActualWeight to c Weight toDatec0i 39 1 DateSite 21600020024982Site 3770188060011500Site 4/Area 4A541012348214024241877Site 4/Area 489051052223017840Site4/Area 4D1000696806008463Site 5315826804700Area t)enAoeeA-- 'site 5 and 3551441100Site 63501748078970Site 7150Site 81150001080906200128074790Site 1013001388230012516540Site 12100798255087027237Site 133003430001040001038850Totals 127255 142324 16140 53738Percent of Con tract Wt 112 %333%Page 140000 39889 104000 103885100%100%Asof8/17/99 .8 54 PMRA: :CGY EASLEYrVANDY EASLEYL O'r NUMBER425.081399L%-'T NUMBER...~4NT. DESCRIPTIONArctared FescueAnnual RyePERCENTDESCRIPTION '48 .28 %Norran Tufts,a Mavgrass39 .10%Arctared Fescue9 .91%Annual RyeGERM ORIGIN T .C° r%tran Tu/te1 Harrgrass4r5-(a130g65% AK Feb-9985% CAN Mar-9990% ORJar-99OTHER CROP SEECINERT MATTERr- C8%2 J8%OTHER CROP SEEDINERT MATTERQ..25100 00°.:WEED SEEDGEF*' r85% AK Nb.Fe;985% CAN `far . ;;90°%. OR Jan- ; :Wt~.t r) SEEDNO NOXIOUS WEEDSNET WEIGHTNO NOXIOUS WEEDSNET WEIGHT30 LBS:r'/ LBSALASKA GARDEN & PET St°F-,f14 N ORCA s r .ALASKA GARDEN & PET SUPPLY114 N . ORCA STANr'HC 1 r. RE . AK 99`01RANDY EASLEY.01 r'4UlVu,tRPERCENT48 .28%39 .10%9 .91%0 .08%2.38%026DESCRIPTION GERM . ORIGINNortran Tufted Ha:grass 85%AKArctared Fescue 85% CANAnnual Rye90% OROTHER CROP SEEDINERT MATTERWEED SEED425-081399LOT NUMBER425-081399PERCENT48 . 20%39 .10%911%0 .03%2 .38%T/DFeb-99Mar-99Jan-990.26%DESCR IPTION GERM .Nortran Tufted Hai rgrass 85%Arctared Fe scueAnnual RyeOTHER CR OP SEEDORIGINAKT: DFeb-9CANORMar-9Jan-985%90%INERT MATTERWEED SEE D100 .00%100.00%'J I^°'NEFDSr.~wRANDY EASLEYRANDY EASLEYLOT NUMBERDESCRIPTION/PERCENTNo Iran Tufted Haugrass48 .28%Arctared Fescue39 .10%Annual Rye9 .91%OTHER CROP SEED0 .08%INERT MATTER2 .38%WEED SEFO0.25$100 .00% -425-081399GERM .85%85%90%LOT NUMBER :425-081399PERCENT DESCRIPTIONGERM . ORIGIN85% AK85% CAN90% ORORIGIN:T/ONorlran Tufleo Hrrgrass4328%39 .10% Arctared Fescu=.CANORMar-_9 .91% Annual Rye0 .08% OTHER CROP SEEDJam-992 .38% INERT MATTERQ2 WEED SEED' 00 .00%NO NOX OUS WEEDSNET WEIGHT 30 LBSALb.SKA GARDEN & PET SUPPLYT/DFeb-9cMar-9EJan-99Appendix ELaboratory Data SummaryAppendix ETable of ContentsDescriptionTableNo.TCLP VOA Results by EPA Method 8260 for Waste Identification Samples5ATCLP SVOA Results by EPA Method 8270 for Waste Identification Samples5BTCLP PCB Results by EPA Method 8082 for Waste Identification Samples5C-1TCLP PCB Results by EPA Method 8082 for Transformer Wipe Samples5C-2TCLP Pesticide Results by EPA Method 8081A for Waste Identification Samples5DTCLP Herbicide Results by EPA Method 8150 for Waste Identification Samples5EVOA Results by EPA Method 8260 for Confirmation Samples (mg/kg)6A-1VOA Results by EPA Method 8260 for Confirmation Samples (mg/L)6A-2SVOA Results by EPA Method 8270 for Confirmation Samples6BPCB Results by EPA Method 8082 for Confirmation Samples6CPesticide Results by EPA Method 8081A for Confirmation Samples6DTable 5ATCLP VOA Results by EPA Method 8260 for Waste Identification SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : July 19, 1999UnitsRegulatoryLimitsSample No.99-GAM-001-SL(Site 8Sample No .99-GAM-002-SL(Site 12Sample No .99-GAM-003-SL(Site 12Sample No .99-GAM-004-SL(Site 2Sample No .99-GAM-005-SLSite 4/46Benzenemg /L0 .5U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)Carbon tetrachloridemg/L0 .5U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)Chlorobenzenemg/L100 .0U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)Chloroformmg/L6 .0U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)1,4-Dichlorobenzenemg/L7 .5U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)1,2-Dichloroethanemg/L0 .5U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)1,1-Dichloroethenemg/L0 .7U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)2-Butanone ( MEK)mg /L200 .0U (0 .50)U (0 .50)U (0 .50)U (0 .50)U (0 .50)Tetrachloroethenemg/L0 .7U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)Trichloroethenemg/L0 .5U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)Vinyl chloridemg/L0 .2U (0 .10)U (0 .10)U (0 .10)U (0 .10)U (0 .10)Anal esNotes:1.2.mg/L means milligrams per liter ."U" means undetected . The number in parenthesis is the laboratory detection limit .3.Laboratory data sheets are provided in Appendix F.4.5.TCLP extraction by EPA 1311 was performed for VOA .Regulatory limits are from 40 CFR 261 .30, Table 1 .Table 5BTCLP SVOA Results by EPA Method 8270 for Waste Identification SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : July 19, 1999UnitsRegulatoryLimitsSample No .99-GAM-001-SL(Site 8Sample No .99-GAM-002-SL(Site 12Sample No .99-GAM-003-SL(Site 12Sample No .99-GAM-004-SL(Site 2Sample No .99-GAM-005-SL(Site 4/4B2-Methylphenol (o-Cresol)mg/L200 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)3&4-Methylphenol (p&m-Cresol)mg/L200 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)2,4-Dinitrotoluenemg/L0 .13U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)Hexachlorobenzenemg/L0.13U (0.017)U (0.018)U (0 .015)U (0 .014)U (0 .022)Hexachlorobutadienemg/L0 .5U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)Hexachloroethanemg/L3.0U (0 .017)U (0 .018)U (0.015)U (0 .014)U (0 .022)Nitrobenzenemg/L2 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)Pentachlorophenolmg/L100 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)Pyridinemg/L5 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)2,4,5-Trichlorophenolmg/L400 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)2,4,6-Trichlorophenolmg/L2 .0U (0 .017)U (0 .018)U (0 .015)U (0 .014)U (0 .022)Anal esNotes :1.2.3.4.mg/L means milligrams per liter ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .TCLP extraction by EPA 1311 was performed for SVOA.5.Regulatory limits are from 40 CFR 261 .30, Table 1 .Table 5C-1TCLP PCB Results by EPA Method 8082 for Waste Identification SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : July 19, 1999UnitsRegulatoryLimitsSample No .99-GAM-001-SL(Site 8Sample No .99-GAM-002-SL(Site 12Sample No .99-GAM-003-SL(Site 12Sample No .99-GAM-004-SLSite 2Sample No .99-GAM-005-SL(Site 4/46Aroclor-1016pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Aroclor-1221pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Aroclor-1232pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Aroclor-1242pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Aroclor-1248pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Aroclor-1254pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Aroclor-1260pg/L0 .5U (0 .179)U (0 .190)U (0 .151)U (0 .105)U (0 .279)Anal esNotes:1.2.3.4.5.pg/L means microgram per liter."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .TCLP extraction by EPA 1311 was performed for PCB .Regulatory limit for PCBs obtained from 18 AAC 75 .341, Table C .Table 5C-2TCLP PCB Results by EPA Method 8082for Transformer Wipe SamplesDebris Removal and-Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : July 19, 1999Sample No .99-GAM-006-W(Site 4Sample No .99-GAM-007-WSite 4Sample No .99-GAM-008-W(Site 4Anal esUnitsRegulatoryLimitsAroclor-1016pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Aroclor-1221pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Aroclor-1232pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Aroclor-1242pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Aroclor-1248pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Aroclor-1254pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Aroclor-1260pg/wipe10 mg/100 cmZU (1 .00)U (1 .00)U (1 .00)Notes :1 . pg/wipe means micrograms per 100 cmZ wipe .2 . "U" means undetected . The number in parenthesis is the laboratory detection limit .3. Laboratory data sheets are provided in Appendix F .4 . TCLP extraction by EPA 1311 was performed for PCB .5 . Sample collected by wiping the internal wall with a hexane wipe prepared by the projectlaboratory .6 . Regulatory limit for PCBs obtained from 40 CFR 761 .3.Table 5DTCLP Pesticide Results by EPA Method 8081A for Waste Identification SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : July 19, 1999RegulatoryLimitsSample No .99-GAM-001-SL(Site 8Sample No .99-GAM-002-SL(Site 12Sample No .99-GAM-003-SL(Site 12Sample No .99-GAM-004-SL(Site 2Sample No .99-GAM-005-SL(Site 4/4BAnal esUnitsgamma -Chlordanepg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)alpha-Chlordanepg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)alpha-BHCpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)beta-BHCpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)gamma -BHC(Lindane)pg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)delta-BHCpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Heptachlorpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Aldrinpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Heptachlor epoxidepg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Endosulfan Ipg/LU (0 .0179)U (0 .0190)pg/LU (0 .0179)U (0 .0190)U (0 .0105)U (0 .0105)U (0 .0279)4,4'-DDEU (0 .0151)U (0 .0151)Dieldrinpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Endrinpg/L0 .0395U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Endosulfan IIpg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)4,4'-DDDpg/L0 .0486U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Endrin aldehydepg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)4,4'-DDTpg/L0 .0274U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Endosulfan sulfatepg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Endrin ketonepg/LU (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Methoxychlorpg/L10 .0U (0 .0179)U (0 .0190)U (0 .0151)U (0 .0105)U (0 .0279)Toxaphenepg/L0 .5U (1 .79)U (1 .90)U (1 .51)U (1 .05)U (2 .79)Notes :1.2.3.4.5.6.0 .0080 .008pg/L means micrograms per liter ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .TCLP extraction by EPA 1311 was performed for pesticides .Regulatory limits are from 40 CFR 261 .30, Table 1 .Blank space in regulatory limits column means that no limit is cited in 40 CFR 261 .30, Table 1 .U (0 .0279)Table 5ETCLP Herbicide Results by EPA Method 8150 for Waste Identification SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : July 19, 1999UnitsRegulatoryLimitsSample No .99-GAM-001-SL(Site 8Sample No.99-GAM-002-SL(Site 12Sample No .99-GAM-003-SL(Site 12Sample No .99-GAM-004-SL(Site 2Sample No .99-GAM-005-SL(Site 4/4B2,4-Dmg/L10U (0 .010)U (0 .010)U (0 .010)U (0 .010)U (0 .010)Silvex (2,4,5-TP)mg/L1 .0U (0 .010)U (0 .010)U (0 .010)U (0 .010)U (0 .010)Anal esNotes :1.mg/L means milligrams per liter .2.3."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .4.5.TCLP extraction by EPA 1311 was performed for herbicides .Regulatory limits are from 40 CFR 261 .30, Table 1 .Table 6A-1VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No. DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-009-SL(Site 12Sample No .99-GAM-010-SL(Site 12Sample No .99-GAM-011-SL(Site 12Dichlorodifluoromenthanemg/kgU (0 .034)U (0 .022)U (0 .019)Chloromethanemg/kgU (0 .034)U (0 .022)U (0 .019)Vinyl chloridemg/kgU (0 .034)U (0 .022)U (0 .019)Bromomethanemg/kgU (0 .34)U (0 .22)U (0 .19)Chloroethanemg/kgU (0 .34)U (0 .22)U (0 .19)Trichlorofluoromethanemg/kgU (0 .034)U (0 .022)U (0 .019)1,1-Dichloroethenemg/kgU (0 .034)U (0 .022)U (0 .019)Carbon disulfidemg/kg17U (0 .34)U (0 .22)U (0 .19)Methylene chloridemg/kg0 .015U (0 .17)U (0 .11)U (0 .093)U (0 .034)U (0 .022)U (0.019)U (0 .034)U (0 .022)U (0.019)trans-l,2-Dichloroethenemg/kg1,1-Dichloroethanemg/kg2-Butanone (MEK)mg/kgU (0 .34)U (0 .22)U (0 .19)2,2-Dichloropropanemg/kgU (0 .034)U (0 .022)U (0 .019)cis-1,2-Dichloroethenemg/kgU (0 .034)U (0 .022)U (0 .019)Bromochloromethanemg/kg0 .35U (0 .034)U (0 .022)U (0 .019)Chloroformmg/kg0 .34U (0 .034)U (0 .022)U (0 .019)1,1,1-Trichloroethanemg/kg1 .0U (0 .034)U (0 .022)U (0 .019)Carbon tetrachloridemg/kg0 .03U (0 .034)U (0 .022)U (0 .019)1,1-Dichloropropenemg/kgU (0 .034)U (0 .022)U (0 .019)Benzenemg/kg0 .02U (0 .034)U (0 .022)U (0 .019)1,2-Dichloroethanemg/kg0 .015U (0 .034)U (0 .022)U (0 .019)Trichloroethenemg/kgU (0 .034)U (0 .022)U (0 .019)1,2-Dichloropropanemg/kgU (0 .034)U (0 .022)U (0 .019)Dibromomethanemg/kgU (0 .034)U (0 .022)U (0 .019)Bromodichloromethanemg/kgU (0 .034)U (0 .022)U (0 .019)2-Chloroethyl Vinyl Ethermg/kgU (0 .34)U (0 .22)U (0 .19)cis-1,3-Dichloropropenemg/kgU (0 .034)U (0 .022)U (0 .019)4-Methyl-2-pentanone (MIBK)mg/kgU (0 .34)U (0 .22)U (0 .19)Toluenemg/kgU (0 .0593)U (0 .022)U (0 .019)trans-l,3-Dichloropropenemg/kgU (0 .034)U (0 .022)U (0 .019)1,1,2-Trichloroethanemg/kgU (0 .034)U (0 .022)U (0 .019)Tetrachloroethenemg/kgU (0 .034)U (0 .022)U (0 .019)1,3-Dichloropropanemg/kgU (0 .034)U (0 .022)U (0 .019)2-Hexanonemg/kgU (0 .34)U (0 .22)U (0 .19)120 .0175 .40 .017Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date: August 14, 1999Anal esUnitsRegulatoryLimitsSample No.99-GAM-009-SL(Site 12Sample No .99-GAM-010-SL(Site 12Sample No .99-GAM-011-SL(Site 12Dibromochloromethanemg/kgU (0 .034)U (0 .022)U (0 .019)1,2-Dibromoethanemg/kgu (0 .034)U (0 .022)U (0 .019)Chlorobenzenemg/kgU (0 .034)U (0 .022)U (0 .019)1,1,1,2-Tetrachloroethanemg/kgU (0 .034)U (0 .022)U (0 .019)Ethylbenzenemg/kg5 .5U (0 .034)U (0 .022)U (0 .019)P&M-Xylenemg/kg78U (0 .034)U (0 .022)U (0 .019)o-Xylenemg/kg78U (0 .034)U (0 .022)U (0 .019)Stryrenemg/kg1 .3U (0 .034)U (0 .022)U (0 .019)Bromoformmg/kg0 .38U (0 .034)U (0 .022)U (0 .019)Isopropyl benzene (Cumene)mg/kgU (0 .034)U (0 .022)U (0 .019)Bromobenzenemg/kgU (0 .034)U (0 .022)U (0 .019)1,1,2,2-Tetrachloroethanemg/kgU (0 .034)U (0 .022)U (0 .019)1,2,3-Trichloropropanemg/kgU (0 .034)U (0 .022)U (0 .019)n-Propylbenzenemg/kgU (0 .034)U (0 .022)U (0 .019)2-Chlorotoluenemg/kgU (0 .034)U (0 .022)U (0 .019)4-Chlorotoluenemg/kgU (0 .034)U (0 .022)U (0 .019)1,3,5-Trimethylbenzenemg/kgU (0 .034)U (0 .022)U (0 .019)tert-Butylbenzenemg/kgU (0 .034)U (0 .022)U (0 .019)1,2,4-Trimethylbenzenemg/kgU (0 .034)U (0 .022)U (0 .019)sec-Butylbenzenemg/kgU (0 .034)U (0 .022)U (0 .019)1,3-Dichlorobenzenemg/kgU (0 .034)U (0 .022)U (0 .019)4-Isopropyltoluenemg/kgU (0 .034)U (0 .022)U (0 .019)1,4-Dichlorobenzenemg/kgU (0 .034)U (0 .022)U (0 .019)U (0 .034)U (0 .022)U (0 .019)U (0 .019)1,2-Dichlorobenzenemg/kg1100 .87n-Butylbenzenemg/kgU (0 .034)U (0 .022)1,2-Dibromo-3-chloropropanemg/kgU (0 .34)U (0 .22)U (0 .19)1,2,4-Trichlorobenzenemg/kgU (0 .034)U (0 .022)U (0 .019)Hexachlorobutadienemg/kgU (0 .034)U (0 .022)U (0 .019)Naphthalenemg/kgU (0 .034)U (0 .022)U (0 .019)1,2,3-Trichlorobenzenemg/kgU (0 .034)U (0 .022)U (0 .019)Notes :2431 . mg/kg means milligrams per kilogram .2 . "U" means undetected . The number in parenthesis is the laboratory detection limit .3 . Laboratory data sheets are provided in Appendix F .4 . Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .5 . Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryLimitsSample No .99-GAM-012-SL(Site 8Sample No .99-GAM-013-SLSite 8Anal esUnitsDichlorodifluoromenthanemg/kgU (0 .018)U (0 .019)Chloromethanemg/kgU (0 .018)U (0 .019)Vinyl chloridemg/kgU (0 .018)U (0 .019)Bromomethanemg/kgU (0 .18)U (0 .19)Chloroethanemg/kgU (0 .18)U (0 .19)Trichlorofluoromethanemg/kgU (0 .018)U (0 .019)1,1-Dichloroethenemg/kgU (0 .018)U (0 .019)Carbon disulfidemg/kg17U (0 .18)U (0 .19)Methylene chloridemg/kg0 .015U (0 .090)U (0 .095)trans-l,2-Dichloroethenemg/kgU (0 .018)U (0.019)1,1-Dichlorethanemg/kgU (0 .018)U (0.019)2-Butanone (MEK)mg/kgU (0 .18)U (0 .19)2,2-Dichloropropanemg/kgU (0 .018)U (0 .019)cis-1,2-Dichloroethenemg/kgU (0 .018)U (0 .019)Bromochloromethanemg/kg0 .35U (0 .018)U (0 .019)Chloroformmg/kg0 .34U (0 .018)U (0 .019)1,1,1-Trichloroethanemg/kg1 .0U (0 .018)U (0 .019)Carbon tetrachloridemg/kg0 .03U (0 .018)U (0 .019)1,1-Dichloropropenemg/kgU (0 .018)U (0 .019)Benzenemg/kg0 .02U (0 .018)U (0 .019)1,2-Dichloroethanemg/kg0 .015U (0 .018)U (0 .019)Trichloroethenemg/kgU (0 .018)U (0 .019)1,2-Dichloropropanemg/kgU (0 .018)U (0 .019)Dibromomethanemg/kgU (0 .018)U (0 .019)Bromodichloromethanemg/kgU (0 .018)U (0 .019)2-Chloroethyl Vinyl Ethermg/kgU (0 .18)U (0 .19)cis-1,3-Dichloropropenemg/kgU (0 .018)U (0 .019)4-Methyl-2-pentanone ( MIBK)mg /kgU (0 .18)U (0 .19)Toluenemg/kgU (0 .018)U (0 .019)trans -l,3-Dichloropropenemg/kgU (0 .018)U (0 .019)1,1,2-Trichloroethanemg/kgU (0 .018)U (0 .019)Tetrachloroethenemg/kgU (0 .018)U (0 .019)1,3-Dichloropropanemg/kgU (0 .018)U (0 .019)2-Hexanonemg/kgU (0 .18)U (0 .19)120 .0175 .40 .017Table 6A -1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-001 0, Gambell, AlaskaSample Date : August 14, 1999RegulatoryLimitsSample No .99-GAM-012-SL(Site 8Sample No .99-GAM-013-SL(Site 8Anal esUnitsDibromochloromethanemg/kgU (0 .018)U (0 .019)1,2-Dibromoethanemg/kgU (0 .018)U (0 .019)Chlorobenzenemg/kgU (0 .018)U (0 .019)1,1,1,2-Tetrachloroethanemg/kgu (0 .018)U (0 .019)Ethylbenzenemg/kg5 .5U (0 .018)U (0 .019)P&M-Xylenemg/kg78U (0 .018)U (0 .019)o-Xylenemg/kg78U (0 .018)U (0 .019)Stryrenemg/kg1 .3U (0 .018)U (0 .019)Bromoformmg/kg0 .38U (0 .018)U (0 .019)Isopropylbenzene (Cumene)mg/kgU (0 .018)U (0 .019)Bromobenzenemg/kgU (0 .018)U (0 .019)1,1,2,2-Tetrachloroethanemg/kgU (0 .018)U (0 .019)1,2,3-Trichloropropanemg/kgU (0 .018)U (0 .019)n-Propylbenzenemg/kgU (0 .018)U (0 .019)2-Chlorotoluenemg/kgU (0 .018)U (0 .019)4-Chlorotoluenemg/kgu (0 .018)U (0 .019)1,3,5-Trimethylbenzenemg/kgU (0 .018)U (0 .019)tert-Butylbenzenemg/kgU (0 .018)U (0 .019)1,2,4-Trimethylbenzenemg/kgU (0 .018)U (0 .019)sec-Butylbenzenemg/kgU (0 .018)U (0 .019)1,3-Dichlorobenzenemg/kgU (0 .018)U (0 .019)4-Isopropyltoluenemg/kgU (0 .018)U (0 .019)1,4-Dichlorobenzenemg/kg0 .8U (0 .018)U (0 .019)1,2-Dichlorobenzenemg/kg7U (0 .018)U (0 .019)n-Butylbenzenemg/kgU (0 .018)U (0 .019)1,2-Dibromo-3-chloropropanemg/kgU (0 .18)U (0 .19)1,2,4-Trichlorobenzenemg/kgU (0 .018)U (0 .019)Hexachlorobutadienemg/kgU (0 .018)U (0 .019)Naphthalenemg/kgU (0 .018)U (0 .019)1,2,3-Trichlorobenzenemg/kgU (0 .018)U (0 .019)Notes :1102431 . mg/kg means milligrams per kilogram .2 . "U" means undetected . The number in parenthesis is the laboratory detection limit .3 . Laboratory data sheets are provided in Appendix F .4 . Regulatory limits are from 18 AAC 75 .341, Table B1 , Method 2 .5 . Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Table 6A -1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-001 0, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-014-SL(Site 4A/Area 4A)Sample No .99-GAM-015-SL(Site 4A/Area 4A)Sample No .99-GAM-016-SL(Site 4A/Area 4A)Dichlorodifluoromethanemg/kgU (0 .030)U (0 .030)U (0 .075)Chloromethanemg/kgU (0 .030)U (0 .030)U (0 .160)Vinyl chloridemg/kgU (0 .030)U (0 .030)U (0 .130)Bromomethanemg/kgU (0 .30)U (0 .30)U (0 .160)Chloroethanemg/kgU (0 .30)U (0 .30)U (0 .087)Trichlorofluoromethanemg/kgU (0 .030)U (0 .030)U (0 .160)1,1-Dichloroethenemg/kgU (0 .030)U (0 .030)U (0 .024)Carbon disulfidemg/kg17U (0 .30)U (0 .30)U (0 .022)Methylene chloridemg/kg0 .015U (0 .15)U (0 .15)U (0 .031)trans-l,2-Dichloroethenemg/kgU (0 .030)U (0 .030)U (0 .025)1,1-Dichloroethanemg/kgU (0 .030)U (0 .030)U (0 .021)2-Butanone (MEK)mg/kgU (0 .30)U (0 .30)U (0 .150)2,2-Dichloropropanemg/kgU (0 .030)U (0 .030)U (0 .027)cis-1,2-Dichloroethenemg/kgU (0 .030)U (0 .030)U (0 .018)Bromochloromethanemg/kg0 .35U (0 .030)U (0 .030)U (0 .030)Chloroformmg/kg0 .34U (0 .030)U (0 .030)U (0 .015)1,1,1-Trichloroethanemg/kg1 .0U (0 .030)U (0 .030)U (0 .017)Carbon tetrachloridemglkg0 .03U (0 .030)U (0 .030)U (0 .020)1,1-Dichloropropenemg/kgU (0 .030)U (0 .030)U (0 .015)Benzenemg /kg0 .02U (0 .030)U (0 .030)U (0 .018)1,2-Dichloroethanemg/kg0 .015U (0 .030)U (0 .030)U (0 .045)Trichloroethenemg/kgU (0 .030)U (0 .030)U (0 .015)1,2-Dichloropropanemg/kgU (0 .030)U (0 .030)U (0 .020)Dibromomethanemg/kgU (0 .030)U (0 .030)U (0 .019)Bromodichloromethanemg/kgU (0 .030)U (0 .030)U (0 .025)2-Chloroethyl Vinyl Ethermg/kgU (0 .30)U (0 .30)U (0 .056)cis-1,3-Dichloropropenemg/kgU (0 .030)U (0 .030)U (0 .015)4-Methyl-2-pentanone (MIBK)mg/kgU (0 .30)U (0 .30)U (0 .095)Toluenemg/kgU (0 .030)U (0 .030)U (0 .015)trans -l,3-Dichloropropenemg/kgU (0 .030)U (0 .030)U (0 .016)1,1,2-Tnchloroethanemg/kgU (0 .030)U (0 .030)U (0 .015)Tetrachloroethenemg/kgU (0 .030)U (0 .030)U (0 .016)1,3-Dichloropro panemg/kgU (0 .030)U (0 .030)U (0 .023)2-Hexanonemg/kgU (0 .30)U (0 .30)U (0 .110)120 .0175 .40 .017Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-014-SL(Site 4A/Area 4A)Sample No .99-GAM-015-SL(Site 4A/Area 4A)Sample No .99-GAM-016-SL(Site 4A/Area 4A)Dibromochloromethanemg/kgU (0 .030)U (0 .030)U (0 .021)1,2-Dibromoethanemg/kgU (0 .030)U (0 .030)U (0 .029)Chlorobenzenemg/kgU (0 .030)U (0 .030)U (0 .015)1, 1, 1,2-Tetrachloroethanemg/kgU (0 .030)U (0 .030)U (0 .015)Ethylbenzenemg/kgU (0 .030)U (0 .030)U (0 .015)U (0 .030)1105 .5P&M-Xylenemg/kg78U (0 .030)U (0 .030)o-Xylenemg/kg78U (0 .030)U (0 .030)U (0 .015)Stryrenemg/kg1 .3U (0 .030)U (0 .030)U (0 .016)Bromoformmg/kg0 .38U (0 .030)U (0 .030)U (0 .024)Isopropylbenzene (Cumene)mg/kgU (0 .030)U (0 .030)U (0 .015)Bromobenzenemg/kgU (0 .030)U (0 .030)U (0 .021)1,1,2,2-Tetrachloroethanemg/kgU (0 .030)U (0 .030)U (0 .068)1,2,3-Thchloropropanemg/kgU (0 .030)U (0 .030)U (0 .017)n-Propylbenzenemg/kgU (0 .030)U (0 .030)U (0 .022)2-Chlorotoluenemg/kgU (0 .030)U (0 .030)U (0 .015)4-Chlorotoluenemg/kgU (0 .030)U (0 .030)U (0 .017)U (0 .030)U (0 .030)U (0 .022)U (0 .018)1,3,5-Trimethylbenzenemg/kgtert-Butylbenzenemg/kgU (0 .030)U (0 .030)1,2,4-Trimethylbenzenemg/kgU (0 .030)U (0 .030)U (0 .018)sec-Butylbenzenemg/kgU (0 .030)U (0 .030)U (0 .021)1,3-Dichlorobenzenemg/kgU (0 .030)U (0 .030)U (0 .015)4-Isopropyltoluenemg/kgU (0 .030)U (0 .030)U (0 .020)1,4-Dichlorobenzenemg/kg0 .8U (0 .030)U (0 .030)U (0 .015)1,2-Dichlorobenzenemg/kg7U (0 .030)U (0 .030)U (0 .015)n-Butylbenzenemg/kgU (0 .030)U (0 .030)U (0 .029)1,2-Dibromo-3-chloropropanemg/kgU (0 .30)U (0 .30)U (0 .067)U (0 .030)U (0 .030)U (0 .044)U (0 .030)U (0 .030)U (0 .077)U (0 .030)U (0 .030)U (0 .047)U (0 .030)U (0 .030)U (0 .052)1,2,4-Tnchlorobenzenemg/kgHexachlorobutadienemg/kgNaphthalenemg/kg1,2,3-Trichlorobenzenemg/kg243Notes : 1 . mg/kg means milligrams per kilogram .2. "U" means undetected . The number in parenthesis is the laboratory detection limit .3. Laboratory data sheets are provided in Appendix F .4. Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .5. Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .6. Samples 99-GAM-014-SL, 99-GAM-015-SL, and 99-GAM-016-SL are parts of a triplicatesample where 99-GAM-014 is the project sample, 99-GAM-015-SL is the quality controlsample, and 99-GAM-016-SL is the quality assurance sample .Table 6A -1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-017-SL(Site 4A/Area 4A)Sample No .99-GAM-018-SL(Site 4A/Area 4A)Sample No .99-GAM-019-SL(Site 4A/Area 4A)Dichlorodifluoromethanemg/kgU (0 .019)U (0 .027)U (0 .029)Chloromethanemg/kgU (0 .019)U (0 .027)U (0 .029)Vinyl chloridemg/kgU (0 .019)U (0 .027)U (0 .029)Bromomethanemg/kgU (0 .19)U (0 .27)U (0 .29)Chloroethanemg/kgU (0 .19)U (0 .27)U (0 .29)Trichlorofluoromethanemg/kgU (0 .019)U (0 .027)U (0 .029)1,1-Dichloroethenemg/kgu (0 .019)U (0 .027)U (0 .029)Carbon disulfidemg/kg17U (0 .19)U (0 .27)U (0 .29)Methylene chloridemg/kg0 .015U (0 .094)U (0 .13)U (0 .14)trans-l,2-Dichloroethenemg/kgu (0 .019)U (0 .027)U (0 .029)1,1-Dichloroethanemg/kgU (0 .019)U (0 .027)U (0 .029)2-Butanone (MEK)mg/kgu (0 .19)U (0 .27)U (0 .29)2,2-Dichloropropanemg/kgU (0 .019)U (0 .027)U (0 .029)cis-1,2-Dichloroethenemg/kgU (0 .019)U (0 .027)U (0 .029)Bromochloromethanemg/kg0 .35U (0 .019)U (0 .027)U (0 .029)Chloroformmg/kg0 .34U (0 .019)U (0 .027)U (0 .029)1,1,1-Trichloroethanemg/kg1 .0U (0 .019)U (0 .027)U (0 .029)Carbon tetrachloridemg/kg0 .03U (0 .019)U (0 .027)U (0 .029)1,1-Dichloropropenemg/kgU (0 .019)U (0 .027)U (0 .029)Benzenemg/kg0 .02U (0 .019)U (0 .027)U (0 .029)1,2-Dichloroethanemg/kg0 .015U (0 .019)U (0 .027)U (0 .029)Trichloroethenemg/kgu (0 .019)U (0 .027)U (0 .029)1,2-Dichloropropanemg/kgU (0 .019)U (0 .027)U (0 .029)Dibromomethanemg/kgU (0 .019)U (0 .027)U (0 .029)Bromodichloromethanemg/kgu (0 .019)U (0 .027)U (0 .029)2-Chloroethyl Vinyl Ethermg/kgu (0 .19)U (0.27)U (0 .29)cis-1,3-Dichloropropenemg/kgU (0 .019)U (0 .027)U (0 .029)4-Methyl-2-pentanone (MIBK)mg/kgU (0 .19)U (0 .27)U (0 .29)Toluenemg/kgU (0 .019)U (0 .027)U (0 .029)trans -l,3-Dichloropropenemg/kgU (0 .019)U (0 .027)U (0 .029)1,1,2-Trichloroethanemg/kgU (0 .019)U (0 .027)U (0 .029)Tetrachloroethenemg/kgU (0 .019)U (0 .027)U (0 .029)1,3-Dichloropropanemg/kgU (0 .019)U (0 .027)U (0 .029)2-Hexanonemg/kgU (0 .19)U (0 .27)U (0 .29)120 .0175 .40 .017Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date: August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-017-SL(Site 4A/Area 4A)Sample No .99-GAM-018-SL(Site 4A/Area 4A)Sample No .99-GAM-019-SL(Site 4A/Area 4A)Dibromochloromethanemg/kgU (0 .019)U (0 .027)U (0 .029)1,2-Dibromoethanemg/kgU (0 .019)U (0 .027)U (0 .029)Chlorobenzenemg/kgU (0 .019)U (0 .027)U (0 .029)1,1,1,2-Tetrachloroethanemg/kgu (0 .019)U (0 .027)U (0 .029)Ethylbenzenemg/kg5 .5U (0 .019)U (0 .027)U (0 .029)P&M-Xylenemg/kg78U (0 .019)U (0 .027)U (0 .029)o-Xylenemg/kg78U (0 .019)U (0 .027)U (0 .029)Stryrenemg/kg1 .3U (0 .019)U (0 .027)U (0 .029)Bromoformmg/kg0 .38U (0 .019)U (0 .027)U (0 .029)Isopropylbenzene (Cumene)mg/kgu (0 .019)U (0 .027)U (0 .029)Bromobenzenemg/kgu (0 .019)U (0 .027)U (0 .029)1,1,2,2-Tetrachloroethanemg/kgu (0 .019)U (0 .027)U (0 .029)1,2,3-Trichloropropanemg/kgu (0 .019)U (0 .027)U (0 .029)n-Propylbenzenemg/kgU (0 .019)U (0 .027)U (0 .029)2-Chlorotoluenemg/kgU (0 .019)U (0 .027)U (0 .029)4-Chlorotoluenemg/kgU (0 .019)U (0 .027)U (0 .029)1,3,5-Trimethylbenzenemg/kgU (0 .019)U (0 .027)U (0 .029)tert-Butylbenzenemg/kgU (0 .019)U (0 .027)U (0 .029)1,2,4-Trimethylbenzenemg/kgU (0 .019)U (0 .027)U (0 .029)sec-Butylbenzenemg/kgu (0 .019)U (0 .027)U (0 .029)1,3-Dichlorobenzenemg/kgU (0 .019)U (0 .027)U (0 .029)4-Isopropyltoluenemg/kgU (0 .019)0 .0396U (0 .029)1,4-Dichlorobenzenemg/kg0 .8U (0 .019)U (0 .027)U (0 .029)1,2-Dichlorobenzenemg/kg7U (0 .019)U (0 .027)U (0 .029)n-Butylbenzenemg/kgU (0 .019)U (0 .027)U (0 .029)1,2-Dibromo-3-chloropropanemg/kgU (0 .19)U (0 .27)U (0 .29)1,2,4-Trichlorobenzenemg/kgU (0 .019)U (0 .027)U (0 .029)Hexachlorobutadienemg/kgU (0 .019)U (0 .027)U (0 .029)Naphthalenemg/kgU (0 .019)1 .20U (0 .029)1,2,3-Trichlorobenzenemg/kgU (0 .019)U (0 .027)U (0 .029)Notes :1.2.3.4.5.110243mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-001 0, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-020-SL(Site 4A/Area 4B)Sample No .99-GAM-021-SL(Site 4A/Area 4B)Sample No .99-GAM-022-SL(Site 4A/Area 4B)Dichlorodifluoromethanemg/kgU (0 .038)U (0 .039)NRChloromethanemg/kgU (0 .038)U (0 .039)NRVinyl chloridemg/kgU (0 .038)U (0 .039)NRBromomethanemg/kgU (0 .38)U (0 .39)NRChloroethanemg/kgU (0 .38)U (0 .39)NRTrichlorofluoromethanemg/kgU (0 .038)U (0 .039)NR1,1-Dichloroethenemg/kgU (0 .038)U (0 .039)NRCarbon disulfidemg/kg17U (0 .38)U (0 .39)NRMethylene chloridemg/kg0 .015U (0 .19)U (0 .20)NRtrans-l,2-Dichloroethenemg/kgU (0 .038)U (0 .039)NR1,1-Dichloroethanemg/kgU (0 .038)U (0 .039)NR2-Butanone (MEK)mg/kgU (0 .38)U (0 .39)NR2,2-Dichloropropanemg/kgU (0 .038)U (0 .039)NRcis-1,2-Dichloroethenemg/kgU (0 .038)U (0 .039)NRBromochloromethanemg/kg0 .35U (0 .038)U (0 .039)NRChloroformmg/kg0 .34U (0 .038)U (0 .039)NR1,1,1-Trichloroethanemg/kg1 .0U (0 .038)U (0 .039)NRCarbon tetrachloridemg/kg0 .030 .04960 .0442NR1,1-Dichloropropenemg/kgU (0 .038)U (0 .039)NRBenzenemg/kg0 .02U (0 .038)U (0 .039)NR1,2-Dichloroethanemg/kg0 .015U (0 .038)U (0 .039)NRTrichloroethenemg/kgU (0 .038)U (0 .039)NR1,2-Dichloropropanemg/kgU (0 .038)U (0 .039)NRDibromomethanemg/kgU (0 .038)U (0 .039)NRBromodichloromethanemg/kgU (0 .038)U (0 .039)NR2-Chloroethyl Vinyl Ethermg/kgU (0 .38)U (0 .39)NRcis-1,3-Dichloropropenemg/kgU (0 .038)U (0 .039)NR4-Methyl-2-pentanone (MIBK)mg/kgU (0 .38)U (0 .39)NRToluenemg/kgU (0 .038)U (0 .039)NRtrans-1,3-Dichloroprope nemg/kgU (0 .038)U (0 .039)NR1,1,2-Trichloroethanemg/kgU (0 .038)U (0 .039)NRTetrachloroethenemg/kgU (0 .038)U (0 .039)NR1,3-Dichloropropanemg/kgU (0 .038)U (0 .039)NR2-Hexanonemg/kgU (0 .38)U (0 .39)NR120 .0175 .40 .017Table 6A -1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-020-SL(Site 4A/Area 4B)Sample No .99-GAM-021-SL(Site 4A/Area 48Sample No .99-GAM-022-SL(Site 4A/Area 4BU (0 .038)U (0 .039)NRU (0 .038)U (0 .039)NRU (0 .038)U (0 .039)NRU (0 .038)U (0 .039)NRDibromochloromethanemg/kg1,2-Dibromoethanemg/kgChlorobenzenemg/kg1,1,1,2-Tetrachloroethanemg/kgEthylbenzenemg/kg5 .5U (0 .038)U (0 .039)NRP&M-Xylenemg/kg78U (0 .038)U (0 .039)NRo-Xylenemg/kg78U (0 .038)U (0 .039)NRStryrenemg/kg1 .3U (0 .038)U (0 .039)NRBromoformmg/kg0 .38U (0 .038)U (0 .039)NRIsopropylbenzene (Cumene)mg/kgU (0 .038)U (0 .039)NRBromobenzenemg/kgU (0 .038)U (0 .039)NR1,1,2,2-Tetrachloroethanemg/kgU (0 .038)U (0 .039)NRNR1101,2,3-Tnchloropropanemg/kgU (0 .038)U (0 .039)n-Propylbenzenemg/kgU (0 .038)U (0 .039)NR2-Chlorotoluenemg/kgU (0 .038)U (0 .039)NR4-Chlorotoluenemg/kgU (0 .038)U (0 .039)NR1,3,5-Trimethylbenzenemg/kg0 .04810 .0430NRtert-Butylbenzenemg/kg0 .04050 .0414NR1,2,4-Trimethylbenzenemg/kgU (0 .038)U (0 .039)NRsec-Butylbenzenemg/kgU (0 .038)U (0 .039)NR1,3-Dichlorobenzenemg/kgU (0 .038)U (0 .039)NR4-Isopropyltoluenemg/kg0 .09610 .0998NR1,4-Dichlorobenzenemg/kgU (0 .038)U (0 .039)NR1,2-Dichlorobenzenemg/kgU (0 .038)U (0 .039)NRn-Butylbenzenemg/kgU (0 .038)U (0 .039)NR1,2-Dibromo-3-chloropropanemg/kgU (0 .38)U (0 .39)NRU (0 .038)U (0 .039)NRU (0 .038)U (0 .039)NR0 .3820 .371NRU (0 .038)U (0 .039)NR1,2,4-Trichlorobenzenemg/kg'Hexachlorobutadienemg/kgNaphthalenemg/kg1,2,3-Trichlorobenzenemg/kgNotes :1.2.3.4.5.6.7.8.0 .87243mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appenadix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Samples 99-GAM-020-SL, 99-GAM-021-SL, and 99-GAM-022-SL are parts of a triplicate samplewhere 99-GAM-020 is the project sample, 99-G ;AM-021-SL is the quality control sample, and 99-GAM022-SL is the quality assurance sample .Based on Modification No . 04P4, VOA analyeas were not required for Sample No . 99-GAM-020-SLthrough 99-GAM-025-SL ."NR" means not run .Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatorySample No .99-GAM-023-SL(Site 4A/Area 4B)Sample No .99-GAM-024-SL(Site 4A/Area 4B)Anal esUnitsDichlorodifluoromethanemg/kgU (0 .027)U (0 .022)Chloromethanemg/kgU (0 .027)U (0 .022)Vinyl chloridemg/kgU (0 .027)U (0 .022)Bromomethanemg/kgU (0 .27)U (0 .22)Chloroethanemg/kgU (0 .27)U (0 .22)Trichlorofluoromethanemg/kgU (0 .027)U (0 .022)1,1-Dichloroethenemg/kgU (0 .027)U (0 .022)Carbon disulfidemg/kg17U (0 .27)U (0 .22)Methylene chloridemg/kg0 .0150 .1640 .141trans-l,2-Dichloroethenemg/kgU (0 .027)U (0 .022)1,1-Dichloroethanemg/kgU (0 .027)U (0 .022)2-Butanone (MEK)mg/kgU (0 .27)U (0 .22)2,2-Dichloropropanemg/kgU (0 .027)U (0 .022)cis-1,2-Dichloroethenemg/kgU (0 .027)U (0 .022)Bromochloromethanemg/kg0 .35U (0 .027)U (0 .022)Chloroformmg/kg0 .34U (0 .027)U (0 .022)1,1,1-Trchloroethanemg/kg1 .0U (0 .027)U (0 .022)Carbon tetrachloridemg/kg0.03U (0 .027)U (0 .022)1,1-Dichloropropenemg/kgU (0 .027)U (0 .022)Benzenemg/kg0 .02U (0 .027)U (0 .022)1,2-Dichloroethanemg/kg0.015U (0 .027)U (0 .022)Trichloroethenemg/kgU (0 .027)U (0 .022)1,2-Dichloropropanemg/kgU (0 .027)U (0 .022)Dibromomethanemg/kgU (0 .027)U (0 .022)Bromodichloromethanemg/kgU (0 .027)U (0 .022)2-Chloroethyl Vinyl Ethermg/kgU (0 .27)U (0 .22)cis-1,3-Dichloropropenemg/kgU (0 .027)U (0 .022)4-Methyl-2-pentanone (MIBK)mg/kgU (0 .27)U (0 .22)Toluenemg/kgU (0 .027)U (0 .022)trans-l,3-Dichloropropenemg/kgU (0 .027)U (0 .022)1,1,2-Trichloroethanemg/kgU (0 .027)U (0 .022)Tetrachloroethenemg/kgU (0 .027)U (0 .022)1,3-Dichloropropanemg/kgU (0 .027)U (0 .022)2-Hexanonemg/kgU (0 .27)U (0 .22)Limits120 .0175_ .40 .6117Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryLimitsSample No .99-GAM-023-SL(Site 4A/Area 4B)Sample No .99-GAM-024-SL(Site 4A/Area 4B)Anal esUnitsDibromochloromethanemg/kgU (0 .027)U (0 .022)1,2-Dibromoethanemg/kgU (0 .027)U (0 .022)Chlorobenzenemg/kgU (0 .027)U (0 .022)1,1,1,2-Tetrachloroethanemg/kgU (0 .027)U (0 .022)Ethylbenzenemg/kg5 .5U (0 .027)U (0 .022)P&M-Xylenemg/kg78U (0 .027)U (0 .022)o-Xylenemg/kg78U (0 .027)U (0 .022)Stryrenemg/kg1 .3U (0 .027)U (0 .022)Bromoformmg/kg0 .38U (0 .027)U (0 .022)Isopropylbenzene (Cumene)mg/kgU (0 .027)U (0 .022)Bromobenzenemg/kgU (0 .027)U (0 .022)1,1,2,2-Tetrachloroethanemg/kgU (0 .027)U (0 .022)1,2,3-Tnchloropropanemg/kgU (0 .027)U (0 .022)n-Propylbenzenemg/kgU (0 .027)U (0 .022)2-Chlorotoluenemg/kgU (0 .027)U (0 .022)4-Chlorotoluenemg/kgU (0 .027)U (0 .022)1,3,5-Tnmethylbenzenemg/kgU (0 .027)U (0 .022)tert-Butylbenzenemg/kgU (0 .027)U (0 .022)1,2,4-Tnmethylbenzenemg/kgU (0 .027)U (0 .022)sec-Butylbenzenemg/kgU (0 .027)U (0 .022)1,3-Dichlorobenzenemg/kgU (0 .027)U (0 .022)4-Isopropyltoluenemg/kg0 .0327U (0 .022)1,4-Dichlorobenzenemg/kg0 .8U (0 .027)U (0 .022)1,2-Dichlorobenzenemg/kg7U (0 .027)U (0 .022)n-Butylbenzenemg/kgU (0 .027)U (0 .022)1,2-Dibromo-3-chloropropanemg/kgU (0 .27)U (0 .22)1,2,4-Trichlorobenzenemg/kgU (0 .027)U (0 .022)Hexachlorobutadienemg/kgU (0 .027)U (0 .022)Naphthalenemg/kgU (0 .027)U (0 .022)1,2,3-Trichlorobenzenemg/kgU (0 .027)U (0 .022)Notes :1.2.3.4.5.6.110243mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1 , Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Numbers printed in boldface exceed regulatory limit .Table 6A-1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-025-SL(Site 4A/Area 4B)Sample No .99-GAM-026-SL(Site 6Sample No .99-GAM-027-SLMethanol Field BlankDichlorodifluoromethanemg/kgU (0 .020)U (0 .014)U (0 .0262)Chloromethanemg/kgU (0 .020)U (0 .014)U (0 .0262)Vinyl chloridemg/kgU (0 .020)U (0 .014)U (0 .0262)Bromomethanemg/kgU (0 .20)U (0 .14)U (0 .262)Chloroethanemg/kgU (0 .20)U (0 .14)U (0 .262)Trichlorofluoromethanemg/kgU (0 .020)U (0 .014)U (0 .0262)1,1-Dichloroethenemg/kgU (0 .020)U (0 .014)U (0 .0262)Carbon disulfidemg/kg17U (0 .20)U (0 .14)U (0 .262)Methylene chloridemg/kg0 .015U (0 .10 )0 .101U (0 .131)trans-l,2-Dichloroethenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,1-Dichloroethanemg/kgU (0 .020)U (0 .014)U (0 .0262)2-Butanone (MEK)mg/kgU (0 .20)U (0 .14)U (0 .262)2,2-Dichloropropanemg/kgU (0 .020)U (0 .014)U (0 .0262)cis-1,2-Dichloroethenemg/kgU (0 .020)U (0 .014)U (0 .0262)Bromochloromethanemg/kg0 .35U (0 .020)U (0 .014)U (0 .0262)Chloroformmg/kg0 .34U (0 .020)U (0 .014)U (0 .0262)1,1,1-Trichloroethanemg/kg1 .0U (0 .020)U (0 .014)U (0 .0262)Carbon tetrachloridemg/kg0 .03U (0 .020)U (0 .014)U (0 .0262)1,1-Dichloropropenemg/kgU (0 .020)U (0 .014)U (0 .0262)Benzenemg/kg0 .02U (0 .020)U (0 .014)U (0 .0262)1,2-Dichloroethanemg/kg0 .015U (0 .020)U (0 .014)U (0 .0262)Trichloroethenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,2-Dichloropropanemg/kgU (0 .020)U (0 .014)U (0 .0262)Dibromomethanemg/kgU (0 .020)U (0 .014)U (0 .0262)Bromodichloromethanemg/kgU (0 .020)U (0 .014)U (0 .0262)2-Chloroethyl Vinyl Ethermg/kgU (0 .20)U (0 .14)U (0 .262)cis-1,3-Dichloropropenemg/kgU (0 .020)U (0 .014)U (0 .0262)4-Methyl-2-pentanone (MIBK)mg/kgU (0 .20)U (0 .14)U (0.262)Toluenemg/kgU (0 .020)U (0 .014)U (0 .0262)trans-l,3-Dichloropropenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,1,2-Trichloroethanemg/kgU (0 .020)U (0 .014)U (0 .0262)Tetrachloroethenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,3-Dichloropropanemg/kgU (0 .020)U (0 .014)U (0 .0262)2-Hexanonemg/kgU (0 .20)U (0 .14)U (0 .262)120 .0175 .40 .017Table 6A -1 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-025-SL(Site 4A/Area 4B)Sample No .99-GAM-026-SL(Site 6Sample No .99-GAM-027-SLMethanol Field BlankDibromochloromethanemg/kgU (0 .020)U (0 .014)U (0 .0262)1,2-Dibromoethanemg/kgU (0 .020)U (0 .014)U (0 .0262)Chlorobenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,1,1,2-Tetrachloroethanemg/kgU (0 .020)U (0 .014)U (0 .0262)Ethylbenzenemg/kg5 .5U (0 .020)U (0 .014)U (0 .0262)P&M-Xylenemg/kg78U (0 .020)U (0 .014)U (0 .0262)o-Xylenemg/kg78U (0 .020)U (0 .014)U (0 .0262)Stryrenemg/kg1 .3U (0 .020)U (0 .014)U (0 .0262)Bromoformmg/kg0 .38U (0 .020)U (0 .014)U (0 .0262)Isopropylbenzene (Cumene)mg/kgU (0 .020)U (0 .014)U (0 .0262)Bromobenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,1,2,2-Tetrachloroethanemg/kgU (0 .020)U (0 .014)U (0 .0262)1,2,3-Trichloropropanemg/kgU (0 .020)U (0 .014)U (0 .0262)n-Propylbenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)2-Chlorotoluenemg/kgU (0 .020)U (0 .014)U (0 .0262)4-Chlorotoluenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,3,5-Trimethylbenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)tert-Butylbenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,2,4-Trimethylbenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)sec-Butylbenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,3-Dichlorobenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)4-Isopropyltoluenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,4-Dichlorobenzenemg/kg0 .8U (0 .020)U (0 .014)U (0 .0262)1,2-Dichlorobenzenemg/kg7U (0 .020)U (0 .014)U (0 .0262)n-Butylbenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)1,2-Dibromo-3-chloropropanemg/kgU (0 .20)U (0 .14)U (0 .262)1,2,4-Trichlorobenzenemg/kgU (0 .020)U (0 .014)U (0 .0262)Hexachlorobutadienemg/kgU (0 .020)U (0 .014)U (0 .0262)Naphthalenemg/kgU (0 .020)U (0 .014)U (0 .0262)U (0 .020)U (0 .014)U (0 .0262)1,2,3-TrichlorobenzeneNotes :1.2.3.4.5.6.mg/kg110243mg/kg means milligrams per kilogram ." U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341 , -Fable B1 , Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Numbers printed in boldface exceed regulattory limits .Table 6A-2VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-001 0, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-028-SLMethanol Trip BlankDichlorodifluoromethanemg/LU (0 .00100)Chloromethanemg/LU (0 .00100)Vinyl chloridemg/LBromomethanemg/LU (0 .00100)Chloroethanemg/LU (0 .00100)Trichlorofluoromethanemg/LU (0 .00100)1,1-Dichloroethenemg/LU (0 .00100)Carbon disulfidemg/LU (0 .0100)Methylene chloridemg/LU (0 .00500)trans-l,2-Dichloroethenemg/LU (0 .00100)1, 1 -Dichloroethanemg/L2-Butanone (MEK)mg/LU (0 .0100)2,2-Dichloropropanemg/LU (0 .00100)cis-1,2-Dichloroethenemg/LU (0 .00100)Bromochloromethanemg/LU (0 .00100)Chloroformmg/L1,1,1-Tdchloroethanemg/LU (0 .00100)Carbon tetrachloridemg/LU (0 .00100)1,1-Dichloropropenemg/LU (0 .00100)Benzenemg/L0 .5U (0 .00100)1,2-Dichloroethanemg/L0 .5U (0 .00100)Trichioroethenemg/LU (0 .00100)1,2-Dichloropropanemg/LU (0 .00100)Dibromomethanemg/LU (0 .00100)Bromodichloromethanemg/LU (0 .00100)2-Chloroethyl Vinyl Ethermg/LU (0 .0100)cis-1,3-Dichloropropenemg/LU (0 .00100)4-Methyl-2-pentanone (MIBK)mg/LU (0 .0100)Toluenemg/LU (0 .00100)trans-l,3-Dichloropropenemg/LU (0 .00100)1,1,2-Trichioroethanemg/LU (0 .00100)Tetrachloroethenemg/LU (0 .00100)1,3-Dichloropropanemg/LU (0 .00100)2-Hexanonemg/LU (0 .0100)0 .20 .56 .0U (0 .00100)U (0 .00100)U (0 .00100)Table 6A-2 (Continued)VOA Results by EPA Method 8260 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-028-SLMethanol Tri BlankDibromochloromethanemg/LU (0 .00100)1,2-Dibromoethanemg/LU (0 .00100)Chlorobenzenemg/L1,1,1,2-Tetrachloroethanemg/LU (0 .00100)Ethylbenzenemg/LU (0 .00100)P&M-Xylenemg/LU (0 .00100)o-Xylenemg/LU (0 .00100)Stryrenemg/LU (0 .00100)Bromcformmg/LU (0 .00100)Isopropylbenzene (Cumene)mg/LU (0 .00100)Bromobenzenemg/LU (0 .00100)1,1,2,2-Tetrachloroethanemg/LU (0 .00100)1,2,3-Trichloropropanemg/LU (0 .00100)n-Propylbenzenemg/LU (0 .00100)2-Chlorotoluenemg/LU (0 .00100)4-Chlorotoluenemg/LU (0 .00100)1,3,5-Trimethylbenzenemg/LU (0 .00100)tert-Butylbenzenemg/LU (0 .00100)1,2,4-Trimethylbenzenemg/LU (0 .00100)sec-Butylbenzenemg/LU (0 .00100)1,3-Dichlorobenzenemg/LU (0 .00100)4-Isopropyltoluenemg/LU (0 .00100)1,4-Dichlorobenzenemg/LU (0 .00100)1,2-Dichlorobenzenemg/Ln-Butylbenzenemg/LU (0 .00100)1,2-Dibromo-3-chloropropanemg/LU (0 .00100)1,2,4-Trichlorobenzenemg/LU (0 .00100)Hexachlorobutadienemg/LNaphthalenemg/LU (0 .00100)1,2,3-Trichlorobenzenemg/LU (0 .00100)100 .07 .50 .5U (0 .00100)U (0 .00100)U (0 .00100)Notes : 1 . mg/L means milligrams per liter.2 . "U" means undetected . The number in parenthesis is thelaboratory detection limit .3 . Laboratory data sheets are provided in Appendix F .4. Regulatory limits are from 40 CFR 261 .30, Table 1 .5 . Blank space in regulatory 6imits column means that no limit iscited in 20 CFR 261 .30 .Table 6BSVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Sample No .99-GAM-009-SL(Site 12Sample No .99-GAM-010-SL(Site 12Sample No .99-GAM-011-SL(Site 12N-Nitrosodimethylaminemg/kgU (11)U (0 .35)U (0 .35)Pyridinemg/kgU (11)U (0 .35)U (0 .35)Anilinemg/kgu (11)U (0 .35)U (0 .35)Phenolmg/kg67U (11)U (0 .35)U (0 .35)Bis(2-Chloroethyl)ethermg/kg0 .002U (11)U (0 .35)U (0 .35)U (11)U (0 .35)U (0 .35)u (11)U (0 .35)U (0 .35)U (11)U (0 .35)U (0 .35)U (11)U (0 .35)U (0 .35)Anal esUnitsRegulatoryLimits2-Chlorophenolmg/kg1 .41,3-Dichlorobenzenemg/kg1,4-Dichlorobenzenemg/kgBenzyl Alcoholmg/kg1,2-Dichlorobenzenemg/kg7U (11)U (0 .35)U (0 .35)2-Methylphenol (o-Cresol)mg/kg7U (11)U (0 .35)U (0 .35)U (0 .35)0 .8bis(2-chloroisopropyl)ethermg/kgu (11)U (0 .35)3&4-Methylphenol (p&m-Cresol)mg/kgU (11)U (0 .35)U (0 .35)N-Nitroso-di-n-propylaminemg/kg0 .00036U (11)U (0 .35)U (0 .35)Hexachloroethanemg/kg1 .6U (11)U (0 .35)U (0 .35)Nitrobenzenemg/kg0 .06U (11)U (0 .35)U (0 .35)Isophoronemg/kg3U (11)U (0 .35)U (0 .35)2-Nitrophenolmg/kgU (11)U (0 .35)U (0 .35)U (0 .35)2,4-Dimethylphenolmg/kg0 .2U (11)U (0 .35)Benzoic Acidmg/kg390U (56)U (1 .8)U (1 .8)Bis(2-Chloroethoxy)methanemg/kgU (11)U (0 .35)U (0 .35)1,2,4-Tnchlorobenzenemg/kg2U (11)U (0 .35)U (0 .35)Naphthalenemg/kg43U (11)U (0 .35)U (0 .35)4-Chloroanilinemg/kg0 .5U (22)U (0 .71)U (0 .71)U (0 .35)Hexachlorobutadienemg/kgu (11)U (0 .35)4-Chloro-3-methylphenolmg/kgU (22)U (0 .71)U (0 .71)2,4-Dichlorophenolmg/kgU (11)U (0 .35)U (0 .35)2-Methylnaphthalenemg/kgU (11)U (0 .35)U (0 .35)Hexachlorocyclopentadienemg/kg0 .45U (11)U (0 .35)U (0 .35)2,4,6-Trichlorophenolmg/kg0 .6U (11)U (0 .35)U (0 .35)2,4,5-Trichlorophenolmg/kg90U (11)U (0 .35)U (0 .35)U (0 .35)2-Chloronaphthalenemg/kgU (11)U (0 .35)2-Nitroanilinemg/kgU (56)U (1 .8)U (1 .8)Dimethylphthalatemg/kgU (11)U (0 .35)U (0 .35)Acenaphthylenemg/kgU (11)U (0 .35)U (0 .35)2,6-Dinitrotoluenemg/kgU (11)U (0 .35)U (0 .35)3-Nitroanilinemg/kgU (56)U (1 .8)U (1 .8)0 .0044Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsmg/kgAcenaphthene0 .2Sample No .99-GAM-009-SL(Site 12Sample No .99-GAM-010-SL(Site 12Sample No .99-GAM-011-SL(Site 12u (11)U (0 .35)U (0 .35)U (56)U (1 .8)U (1 .8)2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgU (56)U (1 .8)U (1 .8)Dibenzofuranmg/kgU (11)U (0 .35)U (0 .35)2,4-Dinitrotoluenemg/kgU (11)U (0 .35)U (0 .35)Diethylphthalatemg/kgU (11)U (0 .35)U (0 .35)4-Chlorophenyl-phenylethermg/kgU (11)U (0 .35)U (0 .35)Fluorenemg/kgU (11)U (0 .35)U (0 .35)U (0 .35)U (0 .35)0 .0052704-Nitroanilinemg/kgU (11)2-Methyl-4,6-dinitrophenolmg/kgU (56)U (1 .8)U (1 .8)N-Nitrosodiphenylaminemg/kgU (11)U (0 .35)U (0 .35)4-Bromophenyl-phenylethermg/kgU (11)U (0 .35)U (0 .35)Hexachlorobenzenemg/kg0 .73U (11)U (0.35)U (0 .35)Pentachlorophenolmg/kg0 .01U (56)U (1 .8)U (1 .8)U (11)U (0.35)U (0 .35)3 .4Phenanthrenemg/kgAnthracenemg/kg4,300U (11)U (0 .35)U (0 .35)Di-n-butylphthalatemg/kg1,700U (11)U (0.35)U (0 .35)Fluoranthenemg/kg2,100U (11)U (0 .35)U (0 .35)Pyrenemg/kg1,500U (11)U (0 .35)U (0 .35)Azobenzenemg/kgu (11)U (0 .35)U (0 .35)Butylbenzylphthalatemg/kgU (11)U (0 .35)U (0 .35)U (0 .71)5,6003,3-Dichlorobenzidinemg/kg0 .02U (22)U (0 .71)Benzo(a)Anthracenemg/kg6U (11)U (0 .35)U (0 .35)Chrysenemg/kg620U (11)U (0 .35)U (0 .35)bis(2-Ethylhexyl)phthalatemg/kg1,200U (11)U (0 .35)U (0 .35)Di-n-octylphthalatemg/kg810,000U (11)U (0 .35)U (0 .35)Benzo[b]Fluoranthenemg/kg20U (11)U (0 .35)U (0 .35)U (0 .35)U (0 .35)Benzo[k]fluoranthenemg/kg200U (11)Benzo[a]pyrenemg/kg3U (11)U (0 .35)U (0 .35)Indeno[1,2,3-c,d]pyrenemg/kg54U (11)U (0 .35)U (0 .35)Dibenzo(a,h]anthracenemg/kg6U (11)U (0 .35)U (0 .35)Benzo(g,h,i]perylenemg/kgU (11)U (0 .35)U (0 .35)Notes :1.2.3.4.5.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means no limit was cited in 18 AAC 75 .341 .Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-012-SL(Site 8Sample No.99-GAM-013-SL(Site 8N-Nitrosodimethylaminemg/kgU (0 .32)U (0 .32)Pyridinemg/kgU (0 .32)U (0 .32)Anilinemg/kgU (0 .32)U (0 .32)Phenolmg/kg67U (0 .32)U (0 .32)Bis(2-Chloroethyl)ethermg/kg0 .002U (0 .32)U (0 .32)2-Chlorophenolmg/kg1 .4U (0 .32)U (0 .32)1,3-Dichlorobenzenemg/kgU (0 .32)U (0 .32)1,4-Dichlorobenzenemg/kgU (0 .32)U (0 .32)Benzyl Alcoholmg/kgU (0 .32)U (0 .32)1,2-Dichlorobenzenemg/kg7U (0 .32)U (0 .32)2-Methylphenol (o-Cresol)mg/kg7U (0 .32)U (0 .32)bis(2-chloroisopropyl)ethermg/kgU (0 .32)U (0 .32)3&4-Methylphenol (p&m-Cresol)mg/kgU (0 .32)U (0 .32)N-Nitroso-di-n-propylaminemg/kg0.,00036U (0 .32)U (0 .32)Hexachloroethanemg/kg1 .6U (0 .32)U (0 .32)Nitrobenzenemg/kg0 .06U (0 .32)U (0 .32)Isophoronemg/kg3U (0 .32)U (0 .32)2-Nitrophenolmg/kgU (0 .32)U (0 .32)2,4-Dimethylphenolmg/kg0 .2U (0 .32)U (0 .32)Benzoic Acidmg/kg390U (1 .6)U (1 .6)Bis(2-Chloroethoxy)methanemg/kgU (0 .32)U (0 .32)1,2,4-Tnchlorobenzenemg/kg2U (0 .32)U (0 .32)0 .8Naphthalenemg/kg43U (0 .32)U (0 .32)4-Chloroanilinemg/kg0 .5U (0 .65)U (0 .65)Hexachlorobutadienemg/kgU (0 .32)U (0 .32)4-Chloro-3-methylphenolmg/kgU (0 .65)U (0 .65)2,4-Dichlorophenolmg/kgU (0 .32)U (0 .32)2-Methylnaphthalenemg/kgU (0 .32)U (0 .32)Hexachlorocyclopentadienemg/kg0 .45U (0 .32)U (0 .32)2,4,6-Trichlorophenolmg/kg0 .6U (0 .32)U (0 .32)2,4,5-Trichlorophenolmg/kg90U (0 .32)U (0 .32)2-Chloronaphthalenemg/kgU (0 .32)U (0 .32)2-Nitroanilinemg/kgU (1 .6)U (1 .6)Dimethylphthalatemg/kgU (0 .32)U (0 .32)Acenaphthylenemg/kgU (0 .32)U (0 .32)2,6-Dinitrotoluenemg/kgU (0 .32)U (0 .32)3-Nitroanilinemg/kgU (1 .6)U (1 .6)0 . .0044Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-001 0, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-012-SL(Site 8Sample No .99-GAM-013-SL(Site 8U (0 .32)U (0 .32)U (1 .6)U (1 .6)Acenaphthenemg/kg2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgU (1 .6)U (1 .6)Dibenzofuranmg/kgU (0 .32)U (0 .32)2,4-Dinitrotoluenemg/kgU (0 .32)U (0 .32)Diethylphthalatemg/kgU (0 .32)U (0 .32)4-Chlorophenyl-phenylethermg/kgU (0 .32)U (0 .32)Fluorenemg/kgU (0 .32)U (0 .32)4-Nitroanilinemg/kgU (0 .32)U (0 .32)2-Methyl-4,6-dinitrophenolmg/kgU (1 .6)U (1 .6)N-Nitrosodiphenylaminemg/kgU (0 .32)U (0 .32)4-Bromophenyl-phenylethermg/kgU (0 .32)U (0 .32)Hexachlorobenzenemg/kg0 .73U (0 .32)U (0 .32)Pentachlorophenolmg/kg0 .01U (1 .6)U (1 .6)U (0 .32)U (0 .32)0 .20-0052703 .4Phenanthrenemg/kgAnthracenemg/kg4,300U (0 .32)U (0 .32)Di-n- butyl phtha latemg/kg1 .700U (0 .32)U (0 .32)Fluoranthenemg/kg2,100U (0 .32)U (0 .32)Pyrenemg/kg1,500U (0 .32)U (0 .32)Azobenzenemg/kgU (0 .32)U (0 .32)Butylbenzylphthalatemg/kg5,600U (0 .32)U (0 .32)U (0 .65)3,3-Dichlorobenzidinemg/kg(}-02U (0 .65)Benzo(a)Anthracenemg/kg6U (0 .32)U (0 .32)Chrysenemg/kg620U (0 .32)U (0 .32)bis(2- Ethyl hexyl)phthalatemg/kg1,200U (0 .32)U (0 .32)Di-n-octylphthalatemg/kg810,000U (0 .32)U (0 .32)U (0 .32)Benzo[b]Fluoranthenemg/kg20U (0 .32)Benzo[k]fluoranthenemg/kg200U (0 .32)U (0 .32)Benzo[a]pyrenemg/kg3U (0 .32)U (0 .32)lndeno[1,2,3-c,d]pyrenemg/kg'54U (0 .32)U (0 .32)Dibenzo[a,h]anthracenemg/kg6U (0 .32)U (0 .32)Benzo[g,h,i]perylenemg/kgU (0 .32)U (0 .32)Notes :1.2.3.4.5.mg/kg means milligrams per kilogram ." U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provides in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means no limit was cited in 18 AAC 75 .341 .Table 6B ( Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-014-SL(Site 4A/Area 4ASample No .99-GAM-015-SL(Site 4A/Area 4ASample No .99-GAM-016-SL(Site 4A/Area 4AN-Nitrosodimethylaminemg/kgU (9 .1)U (9 .0)U (1 .200)Pyridinemg/kgU (9 .1)U (9 .0)U (0 .890)Anilinemg/kgU (9 .1)U (9 .0)U (0 .700)Phenolmg/kg67U (9 .1)U (9 .0)U (0 .620)Bis(2-Chloroethyl)ethermg/kg0 .002U (9 .1)U (9 .0)U (0 .680)2-Chlorophenolmg/kg1 .4U (9 .1)U (9 .0)U (0 .650)1,3-Dichlorobenzenemg/kgU (9 .1)U (9 .0)U (0 .660)1,4-Dichlorobenzenemg/kgU (9 .1)U (9 .0)U (0 .580)Benzyl Alcoholmg/kgU (9 .1)U (9 .0)U (0 .920)1,2-Dichlorobenzenemg/kg7U (9 .1)U (9 .0)U (0 .500)2-Methylphenol (o-Cresol)mg/kg7U (9 .1)U (9 .0)U (0 .990)bis(2-chloroisopropyl)ethermg/kgU (9 .1)U (9 .0)U (0 .790)3&4-Methylphenol (p&m-Cresol)mg/kgU (9 .1)U (9 .0)NRN-Nitroso-di-n-propylaminemg/kg0 .00036U (9 .1)U (9 .0)U (0 .750)Hexachloroethanemg/kg1 .6U (9 .1)U (9 .0)U (0 .850)Nitrobenzenemg/kg0 .06U (9 .1)U (9 .0)U (0 .590)Isophoronemg/kg3U (9 .1)U (9 .0)U (0 .680)2-Nitrophenolmg/kgU (9 .1)U (9 .0)U (0 .900)2,4-Dimethylphenolmg/kg0 .2U (9 .1)U (9 .0)U (0 .590)Benzoic Acidmg/kg390U (46)U (46)U (1 .200)Bis(2-Chloroethoxy)methanemg/kgU (9 .1)U (9 .0)U (0.720)1,2,4-Trichlorobenzenemg/kg2U (9 .1)U (9 .0)U (0 .680)Naphthalenemg/kg43U (9 .1)U (9 .0)U (0 .620)4-Chloroanilinemg/kg0 .5U (18)U (18)U (0 .790)Hexachlorobutadienemg/kgU (9 .1)U (9 .0)U (1 .700)4-Chloro-3-methylphenolmg/kgU (18)U (18)U (0 .940)2,4-Dichlorophenolmg/kgU (9 .1)U (9 .0)U (0 .960)2-Methyl naphthalenemg/kgU (9 .1)U (9 .0)U (0 .660)Hexachlorocyclopentadienemg/kg0 .45U (9 .1)U (9 .0)U (0.540)2,4,6-Trichlorophenolmg/kg0 .6U (9 .1)U (9 .0)U (0.740)2,4,5-Trichlorophenolmg/kg90U (9 .1)U (9 .0)U (0 .800)2-Chloronaphthalenemg/kgU (9 .1)U (9 .0)U (0 .520)2-Nitroanilinemg/kgU (46)U (46)U (0 .650)Dimethylphthalatemg/kgU (9 .1)U (9 .0)U (0 .540)Acenaphthylenemg/kgu (9 .1)U (9 .0)U (0 .710)2,6-Dinitrotoluenemg/kgU (9 .1)U (9 .0)U (0 .910)3-Nitroanilinemg/kgU (46)U (46)U (0 .770)0 .80 .0044Table 6B ( Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsAcenaphthenemg/kg2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgRegulatoryLimits0 .2Sample No .99-GAM-014-SL(Site 4ASample No.99-GAM-015-SL(Site 4ASample No .99-GAM-016-SL(Site 4AU (9 .1)U (9 .0)U (0 .610)U (46)U (46)U (0 .570)U (46)U (46)U (0 .570)U (9 .1)U (9 .0)U (0 .560)U (9 .1)U (9 .0)U (0 .690)Dibenzofuranmg/kg2,4-Dinitrotoluenemg/kgDiethylphthalatemg/kgU (9 .1)U (9 .0)U (0 .460)4-Chlorophenyl-phenylethermg/kgU (9 .1)U (9 .0)U (0 .540)Fluorenemg/kgU (9 .1)U (9 .0)U (0 .470)4-Nitroanilinemg/kgU (9 .1)U (9 .0)U (0 .720)2-Methyl-4,6-dinitrophenolmg/kgU (46)U (46)U (0 .650)U (9 .1)U (9 .0)U (0 .920)U (9 .1)U (9 .0)U (0 .780)U (9 .0)U (0 .450)0 .005270N-Nitrosodiphenylaminemg/kg3 .44-Bromophenyl-phenylethermg/kgHexachlorobenzenemg/kg0 .73U (9 .1)Pentachlorophenolmg/kg0 .01U (46)U (46)U (0 .800)U (9 .1)U (9 .0)U (0 .370)Phenanthrenemg/kgAnthracenemg/kg4,300U (9 .1)U (9 .0)U (0 .580)Di-n-butylphthalatemg/kg1,700U (9 .1)U (9 .0)U (0 .610)Fluoranthenemg/kg2,100U (9 .1)U (9 .0)U (0 .520)U (9 .1)U (9 .0)U (0 .760)U (9 .1)U (9 .0)U (0 .690)U (9 .0)NRPyrenemg/kg1,500Azobenzenemg/kgButylbenzylphthalatemg/kg5,600U (9 .1)3,3-Dichlorobenzidinemg/kg0 .02U (18)U (18)U (8 .600)U (9 .0)U (0 .590)Benzo(a)Anthracenemg/kg6U (9 .1)Chrysenemg/kg620U (9 .1)U (9 .0)U (0 .540)bis(2-Ethylhexyl)phthalatemg/kg1,200U (9 .1)U (9 .0)U (0 .780)U (9 .0)U (0 .540)Di-n-octylphthalatemg/kg810,000U (9 .1)Benzo[b]Fluoranthenemg/kg20U (9 .1)U (9 .0)U (0 .610)Benzo[k]fluoranthenemg/kg200U (9 .1)U (9 .0)U (0 .620)U (0 .550)Benzo[a]pyrenemg/kg3U (9 .1)U (9 .0)Indeno[1,2,3-c,d]pyrenemg/kg54U (9 .1)U (9 .0)U (0 .520)Dibenzo[a,h]anthracenemg/kg6U (9 .1)U (9 .0)U (0 .570)Benzo[g,h,i]perylenemg/kgU (9 .1)U (9 .0)U (0 .570)Notes :1.2.3.4.5.6.7.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means no limit was cited in 18 AAC 75 .341 .Samples 99-GAM-017-SL are parts of a triplicate sample where 99-GAM-014-SL in the projectsample, 99-GAM-015-SL is the quality control sample and 99-GAM-016-SL is the qualityassurance sample ."NR" means not run .Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-001 0, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-017-SL(Site 4A/Area 4ASample No .99-GAM-018-SL(Site 4A/Area 4ASample No .99-GAM-019-SL(Site 4A/Area 4AN-Nitrosodimethylaminemg/kgU (0 .34)U (18)U (8 .4)Pyridinemg/kgU (0 .34)U (18)U (8 .4)Anilinemg/kgU (0 .34)U (18)U (8 .4)Phenolmg/kg67U (0 .34)U (18)U (8.4)Bis(2-Chloroethyl)ethermg/kg0 .002U (0 .34)U (18)U (8 .4)2-Chlorophenolmg/kg1 .4U (0 .34)U (18)U (8 .4)1,3-Dichlorobenzenemg/kgU (0 .34)U (18)U (8 .4)U (0 .34)U (18)U (8 .4)U (0 .34)U (18)U (8 .4)1,4-Dichlorobenzenemg/kg0 .8Benzyl Alcoholmg/kg1,2-Dichlorobenzenemg/kg7U (0 .34)U (18)U (8 .4)2-Methylphenol (o-Cresol)mg/kg7U (0 .34)U (18)U (8.4)bis(2-chloroisopropyl)ethermg/kgU (0 .34)U (18)U (8 .4)3&4-Methylphenol (p&m-Cresol)mg/kgU (0 .34)U (18)U (8 .4)N-Nitroso-di-n-propylaminemg/kgU (0 .34)U (18)U (8 .4)U (8 .4)0 .00036Hexachloroethanemg/kg1 .6U (0 .34)U (18)Nitrobenzenemg/kg0 .06U (0 .34)U (18)U (8 .4)Isophoronemg/kg3U (0 .34)U (18)U (8 .4)2-Nitrophenolmg/kgU (0 .34)U (18)U (8 .4)2,4-Dimethylphenolmg/kg0 .2U (0 .34)U (18)U (8 .4)Benzoic Acidmg/kg390U (1 .7)U (89)U (43)Bis(2-Chloroethoxy)methanemg/kgU (0 .34)U (18)U (8 .4)1,2,4-Tnchlorobenzenemg/kg2U (0 .34)U (18)U (8 .4)Naphthalenemg/kg43U (0 .34)U (18)U (8 .4)4-Chloroanilinemg/kg0 .5U (0 .69)U (36)U (17)Hexachlorobutadienemg/kgU (0 .34)U (18)U (8 .4)4-Chloro-3-methylphenolmg/kgU (0 .69)U (36)U (17)U (8 .4)2,4-Dichlorophenolmg/kgU (0 .34)U (18)2-Methylnaphthalenemg/kgU (0 .34)U (18)U (8 .4)Hexachlorocyclopentadienemg/kg0 .45U (0 .34)U (18)U (8 .4)2,4,6-Trichlorophenolmg/kg0 .6U (0 .34)U (18)U (8 .4)2,4,5-Trichlorophenolmg/kg90U (0 .34)U (18)U (8 .4)2-Chloronaphthalenemg/kgU (0 .34)U (18)U (8 .4)2-Nitroanilinemg/kgU (1 .7)U (89)U (43)mg/kgU (0 .34)U (18)U (8 .4)Acenaphthylenemg/kgU (0 .34)U (18)U (8 .4)2,6-Dinitrotoluenemg/kgU (0 .34)U (18)U (8 .4)3-Nitroanilinemg/kgU (1 .7)U (89)U (43)Dimethylphthalate0 .0044Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-017-SL(Site 4A/Area 4ASample No .99-GAM-018-SL(Site 4A/Area 4ASample No .99-GAM-019-SL(Site 4A/Area 4AU (0 .34)U (18)U (8 .4)U (1 .7)U (89)U (43)Acenaphthenemg/kg2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgU (1 .7)U (89)U (43)Dibenzofuranmg/kgU (0 .34)U (18)U (43)2,4-Dinitrotoluenemg/kgU (0 .34)U (18)U (8 .4)Diethylphthalatemg/kgU (0 .34)U (18)U (8 .4)4-Chlorophenyi-phenylethermg/kgU (0 .34)U (18)U (8 .4)Fluorenemg /kgU (0 .34)U (18)U (8 .4)4-Nitroanilinemg/kgU (0 .34)U (18)U (8 .4)2-Methyl-4,6-dinitrophenolmg/kgU (1 .7)U (89)U (43)N-Nitrosodiphenylaminemg/kgU (0 .34)U (18)U (8 .4)4-Bromophenyl-phenylethermg/kgU (0 .34)U (18)U (8 .4)Hexachlorobenzenemg/kg0 .73U (0 .34)U (18)U (8 .4)Pentachlorophenolmg/kg0 .01U (1 .7)U (89)U (43)U (0 .34)U (18)U (8 .4)0 .20 .0052703 .4Phenanthrenemg/kgAnthracenemg/kg4,300U (0 .34)U (18)U (8 .4)Di-n-butylphthalatemg/kg1,700U (0 .34)U (18)U (8 .4)Fluoranthenemg/kg2,100U (0 .34)17 .4U (8 .4)Pyrenemg/kg1,500U (0 .34)25 .2U (8 .4)Azobenzenemg/kgU (0 .34)U (18)U (8 .4)Butyl benzylphtha latemg/kg5,600U (0 .34)U (18)U (8 .4)3,3-Dichlorobenzidinemg/kg0 .02U (0 .69)U (36)U (17)Benzo (a)Anthracenemg/kg6U (0 .34)U (18)U (8 .4)Chrysenemg/kg620U (0 .34)U (18)U (8.4)bis(2-Ethylhexyl)phthalatemg/kg1,200U (0 .34)U (18)U (8 .4)Di-n-octylphthalatemg/kg810,000U (0 .34)U (18)U (8 .4)Benzo[b]Fluoranthenemg/kg20U (0 .34)21 .4U (8 .4)Benzo[k]fluoranthenemg/kg200U (0.34)U (18)U (8 .4)Benzo[a]pyrenemg/kg3U (0.34)U (18)U (8 .4)Indeno[1,2,3-c,d]pyrenemg/kg54U (0 .34)U (18)U (8 .4)Dibenzo[a,h]anthracenemg/kg6U (0 .34)U (18)U (8 .4)Benzo[g ,h,i]perylenemg/kgU (0 .34)U (18)U (8 .4)Notes :1.2.3.4.5.6.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit ."NR" means not run by laboratory .Laboratory data sheets are provided in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means no limit was cited in 18 AAC 75 .341 .Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-020-SL(Site 4A/Area 413)Sample No .99-GAM-021 -SLSite 4A/Area 413)Sample No .99-GAM-022-SL(Site 4A/Area 4BN-Nitrosodimethylaminemg/kgU (9.4)U (3 .5)NRPyridinemg/kgU (9 .4)U (3 .5)NRAnilinemg/kgU (9 .4)U (3 .5)NRPhenolmg/kg67U (9 .4)U (3 .5)NRU (3 .5)NRBis(2-Chloroethyl)ethermg/kg0 .002U (9 .4)2-Chlorophenolmg/kg1 .4U (9 .4)U (3 .5)NR1,3-Dichlorobenzenemg/kgU (9 .4)U (3 .5)NR1,4-Dichlorobenzenemg/kgU (9 .4)U (3 .5)NRBenzyl Alcoholmg/kgU (9 .4)U (3 .5)NR1,2-Dichlorobenzenemg/kg7U (9 .4)U (3 .5)NR2-Methylphenol (o-Cresol)mg/kg7U (9 .4)U (3 .5)NRU (3 .5)NR0 .8bis(2-chloroisopropyl)ethermg/kgU (9 .4)3&4-Methylphenol (p&m-Cresol)mg/kgU (9 .4)U (3 .5)NRN-Nitroso-di-n-propylaminemg/kg0 .00036U (9 .4)U (3 .5)NRHexachloroethanemg/kg1 .6U (9 .4)U (3 .5)NRNitrobenzenemg/kg0 .06U (9 .4)U (3 .5)NRIsophoronemg/kg3U (9 .4)U (3 .5)NR2-Nitrophenolmg/kgU (9 .4)U (3 .5)NRNR2,4-Dimethylphenolmg/kg0 .2U (9 .4)U (3 .5)Benzoic Acidmg/kg390U (48)U (18)NRBis(2-Chloroethoxy)methanemg/kgU (9 .4)U (3 .5)NR1,2,4-Trichlorobenzenemg/kg2U (9 .4)U (3 .5)NRNaphthalenemg/kg43U (9 .4)U (3 .5)NR4-Chloroanilinemg/kg0 .5U (19)U (7 .2)NRHexachlorobutadienemg/kgU (9 .4)U (3 .5)NR4-Chloro-3-methylphenolmg/kgU (19)U (7 .2)NR2,4-Dichlorophenolmg/kgU (9 .4)U (3 .5)NR2-Methylnaphthalenemg/kgU (0 .69)U (3 .5)NRHexachlorocyclopentadienemg/kg0 .45U (9 .4)U (3 .5)NR2,4,6-Trichlorophenolmg/kg0 .6U (9 .4)U (3 .5)NRU (9 .4)U (3 .5)NRNR2,4,5-Trichlorophenolmg/kg902-Chloronaphthalenemg/kgU (9 .4)U (3 .5)2-Nitroanilinemg/kgU (48)U (18)NRDimethylphthalatemg/kgU (9 .4)U (3 .5)NRAcenaphthylenemg/kgU (9 .4)U (3 .5)NR2,6-Dinitrotoluenemg/kgU (9 .4)U (3 .5)NR3-Nitroanilinemg/kgU (48)U (18)NR0 .0044Table 6B ( Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-020-SL(Site 4A/Area 48Sample No .99-GAM-021-SLSite 4A/Area 48)Sample No.99-GAM-022-SL(Site 4A/Area 46U (9 .4)U (3 .5)NRU (48)U (18)NRAcenaphthenemg/kg2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgU (48)U (18)NRDibenzofuranmg/kgU (9 .4)U (3 .5)NR2,4-Dinitrotoluenemg/kgU (9 .4)U (3 .5)NRDiethylphthalatemg/kgU (9 .4)U (3 .5)NR4-Chlorophenyl-phenylethermg/kgU (9 .4)U (3 .5)NRFluorenemg/kgU (9 .4)U (3 .5)NR4-Nitroanilinemg/kgU (9 .4)U (3 .5)NR2-Methyl-4,6-dinitrophenolmg/kgU (48)U (18)NRN-Nitrosodiphenylaminemg/kgU (9 .4)U (3 .5)NR4-Bromophenyl-phenylethermg/kgU (9 .4)U (3 .5)NRHexachlorobenzenemg/kg0 .73U (9 .4)U (3 .5)NRPentachlorophenolmg/kg0 .01U (48)U (18)NRPhenanthrenemg/kgU (9 .4)U (3 .5)NRAnthracenemg/kg4,300U (9 .4)U (3 .5)NRDi-n-butylphthalatemg/kg1,700U (9 .4)U (3 .5)NRFluoranthenemg/kg2,100U (9 .4)U (3 .5)NRPyrenemg/kg1,500U (9 .4)U (3 .5)NRNR0 .20 .0052703 .4Azobenzenemg/kgU (9 .4)U (3 .5)Butylbenzylphthalatemg/kg5,600U (9 .4)U (3 .5)NR3,3-Dichlorobenzidinemg/kg0 .02U (19)U (7 .2)NRBenzo (a)Anthracenemg/kg6U (9 .4)U (3 .5)NRNRChrysenemg/kg620U (9 .4)U (3 .5)bis(2-Ethylhexyl)phthalatemg/kg1,200U (9 .4)U (3 .5)NRDi-n-octylphtha latemg/kg810,000U (9 .4)U (3 .5)NRU (3 .5)NRBenzo [b]Fluoranthenemg/kg20U (9 .4)Benzo[k]fluoranthenemg/kg200U (9 .4)U (3 .5)NRBenzo[a]pyrenemg/kg3U (9 .4)U (3 .5)NRNRIndeno[1,2,3-c,d]pyrenemg/kg54U (9 .4)U (3 .5)Dibenzo[a,h]anthracenemg/kg6U (9 .4)U (3 .5)NRU (9 .4)U (3 .5)NRmg/kgBenzo[g ,h,i]perylene1.mg/kg means milligrams per kilogram .Notes :7."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means no limit was cited in 18 AAC 75 .341 .Samples 99-GAM-023-SL are parts of a triplicate sample where 99-GAM-020-SL is the project sample,99-GAM-021-SL is the quality control sample and 99-GAM-022-SL is the quality assurance sample .Based on Modification No . 04P4, SVOA analyes were not required for Sample No . 99-GAM-020-SL8.through 99-GAM-025-SL ."NR" means not run .2.3.4.5.6.Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryLimitsSample No .99-GAM-023-SL(Site 4A/Area 4BAnal esUnitsN-Nitrosodimethylaminemg/kgU (0 .33)Pyridinemg/kgU (0 .33)Anilinemg/kgU (0 .33)Phenolmg/kg67U (0 .33)Bis(2-Chloroethyl)ethermg/kg0 .002U (0 .33)2-Chlorophenolmg/kg1 .4U (0 .33)1,3-Dichlorobenzenemg/kg1,4-Dichlorobenzenemg/kgBenzyl Alcoholmg/kg1,2-Dichlorobenzenemg/kg7U (0 .33)2-Methylphenol (o-Cresol)mg/kg7U (0 .33)bis(2-chloroisopropyl)ethermg/kgU (0 .33)3&4-Methylphenol (p&m-Cresol)mg/kgU (0 .33)N-Nitroso-di-n-propylaminemg/kg0 .00036U (0 .33)Hexachloroethanemg/kg1 .6U (0 .33)Nitrobenzenemg/kg0 .06U (0 .33)Isophoronemg/kg3U (0 .33)2-Nitrophenolmg/kg2,4-Dimethylphenolmg/kgg0 .2U (0 .33)Benzoic Acidmg/kg390U (1 .7)Bis(2-Chloroethoxy)methanemg/kg1,2,4-Trichlorobenzenemg/kg2U (0 .33)Naphthalenemg/kg43U (0 .33)4-Chloroanilinemg/kg0 .5U (0 .67)Hexachlorobutadienemg/kgU (0 .33)4-Chloro-3-methylphenolmglkgU (0 .67)2,4-Dichlorophenolmg/kgU (0 .33)2-Methylnaphthalenemg/kgU (0 .33)Hexachlorocyclopentadienemg/kg0 .45U (0 .33)2,4,6-Trichlorophenolmg/kg0 .6U (0 .33)2,4,5-Trichlorophenolmg/kg90U (0 .33)2-Chloronaphthalenemg/kgU (0 .33)2-Nitroanilinemg/kgU (1 .7)Dimethylphthalatemg/kgU (0 .33)Acenaphthylenemg/kg2,6-Dinitrotoluenemg/kg3-Nitroanilinemg/kgU (0 .33)0 .8U (0 .33)U (0 .33)U (0 .33)U (0 .33)U (0 .33)0 .0044U (0 .33)U (1 .7)Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-023-SL(Site 4A/Area 4BAcenaphthenemg/kg2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgU (1 .7)Dibenzofuranmg/kgU (0 .33)2,4-Dinitrotoluenemg/kgDiethylphthalatemg/kgU (0 .33)4-Chlorophenyl-phenylethermg/kgU (0 .33)Fluorenemg/kg4-Nitroanilinemg/kgU (0 .33)2-Methyl-4,6-dinitrophenolmg/kgU (1 .7)N-Nitrosodiphenylaminemg/kg4-Bromophenyl-phenylethermg/kgHexachlorobenzenemg/kg0 .73U (0 .33)Pentachlorophenolmg/kg0 .01U (1 .7)Phenanthrenemg/kgAnthracenemg/kg4,300U (0 .33)Di-n-butylphthalatemg/kg1,700U (0 .33)Fluoranthenemg/kg2,100U (0 .33)Pyrenemg/kg1,500U (0 .33)Azobenzenemg/kgButylbenzylphthalatemg/kg5,600U (0 .33)3,3-Dichlorobenzidinemg/kg0 .02U (0 .67)Benzo(a)Anthracenemg/kg6U (0 .33)Chrysenemg/kg620U (0 .33)bis(2-Ethylhexyl)phthalatemg/kg1,2000 .384Di-n-octylphthalatemg/kg810,000U (0 .33)Benzo[b]Fluoranthenemg/kg20U (0 .33)Benzo[k]fluoranthenemg/kg200U (0 .33)Benzo[a]pyrenemg/kg3U (0 .33)lndeno[1,2,3-c,d]pyrenemg/kg54U (0 .33)Dibenzo[a,h]anthracenemg/kg6U (0 .33)Benzo(g ,h,i]perylenemg/kgNotes :1.2.3.4.5.U (0 .33)0 .20 .0052703 .4U (1 .7)U (0 .33)U (0 .33)U (0 .33)U (0 .33)U (0 .33)U (0 .33)U (0 .33)mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratorydetection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table BI, Method 2 .Blank space in regulatory limits column means no limit was cited in 18AAC 75 .341 .Table 6B (Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryAnal esUnitsLimitsSample No .99-GAM-024-SL(Site 4A/Area 4BSample No .99-GAM-025-SLSite 4A/Area 48Sample No .99-GAM-026-SL(Site 4A/Area 4BN-Nitrosodimethylaminemg/kgU (0 .31)U (0 .33)U (0 .31)Pyridinemg/kgU (0 .31)U (0 .33)U (0 .31)Anilinemg/kgU (0 .31)U (0 .33)U (0 .31)Phenolmg/kgU (0 .31)U (0 .33)U (0 .31)U (0 .31)67Bis(2-Chloroethyl)ethermg/kg0 .002U (0 .31)U (0 .33)2-Chlorophenolmg/kg1 .4U (0 .31)U (0 .33)U (0 .31)1,3-Dichlorobenzenemg/kgU (0 .31)U (0 .33)U (0 .31)1,4-Dichlorobenzenemg/kgU (0 .31)U (0 .33)U (0 .31)Benzyl Alcoholmg/kgU (0 .31)U (0 .33)U (0 .31)1,2-Dichlorobenzenemg/kg7U (0 .31)U (0 .33)U (0 .31)2-Methylphenol (o-Cresol)mg/kg7U (0 .31)U (0 .33)U (0 .31)bis(2-chloroisopropyl)ethermg/kgU (0 .31)U (0 .33)U (0 .31)3&4-Methylphenol (p&m-Cresol)mg/kgU (0 .31)U (0 .33)U (0 .31)N-Nitroso-di-n-propylaminemg/kg0 .00036U (0 .31)U (0 .33)U (0 .31)Hexachloroethanemg/kg1 .6U (0 .31)U (0 .33)U (0 .31)Nitrobenzenemg/kg0 .06U (0 .31)U (0 .33)U (0 .31)Isophoronemg/kg3U (0 .31)U (0 .33)U (0 .31)2-Nitrophenolmg/kgu (0 .31)U (0 .33)U (0 .31)2,4-Dimethylphenolmg/kg0 .2U (0 .31)U (0 .33)U (0 .31)Benzoic Acidmg/kg390U (1 .6)U (1 .7)U (1 .6)Bis(2-Chloroethoxy)methanemg/kgU (0 .31)U (0 .33)U (0 .31)1,2,4-Tnchlorobenzenemg/kg2U (0 .31)U (0 .33)U (0 .31)Naphthalenemg/kg43U (0 .31)U (0 .33)U (0 .31)U (0 .64)0 .84-Chloroanilinemg/kgU (0 .63)U (0 .68)Hexachlorobutadienemg/kgU (0 .31)U (0 .33)U (0 .31)4-Chloro-3-methylphenolmg/kgU (0 .63)U (0 .68)U (0 .64)2,4-Dichlorophenolmg/kgU (0 .31)U (0 .33)U (0 .31)2-Methylnaphthalenemg/kgU (0 .31)U (0 .33)U (0 .31)Hexachlorocyclopentadienemg/kgU (0 .31)U (0 .33)U (0 .31)0 .6U (0 .31)U (0 .33)U (0 .31)90U (0 .31)U (0 .33)U (0 .31)0 .50 .452,4,6-Tdchlorophenolmg/kg2,4,5-Tdchlorophenolmg/kg2-Chloronaphthalenemg/kgU (0 .31)U (0 .33)U (0 .31)2-Nitroanilinemg/kgU (1 .6)U (1 .7)U (1 .6)Dimethylphthalatemg/kgU (0 .31)U (0 .33)U (0 .31)Acenaphthylenemg/kgU (0 .31)U (0 .33)U (0 .31)2,6-Dinitrotoluenemg/kgU (0 .31)U (0 .33)U (0 .31)3-Nitroanilinemg/kgU (1 .6)U (1 .7)U (1 .6)0 .0044Table 613 ( Continued)SVOA Results by EPA Method 8270 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999RegulatoryesAnalUnitsLimitsSample No .99-GAM-024-SLSite 4A/Area 46Sample No .99-GAM-025-SLSite 4A/Area 413)Sample No .99-GAM-026-SL(Site 4A/Area 46U (0 .31)U (0 .33)U (0 .31)U (1 .6)U (1 .7)U (1 .6)Acenaphthenemg/kg2,4-Dinitrophenolmg/kg4-Nitrophenolmg/kgU (1 .6)U (1 .7)U (1 .6)Dibenzofuranmg/kgU (0 .31)U (0.33)U (0 .31)2,4-Dinitrotoluenemg/kgU (0 .31)U (0 .33)U (0 .31)Diethylphthalatemg/kgU (0 .31)U (0 .33)U (0 .31)4-Chlorophenyl-phenylethermg/kgU (0 .31)U (0 .33)U (0 .31)Fluorenemg/kgU (0 .31)U (0 .33)U (0 .31)4-Nitroanilinemg/kgU (0 .31)U (0 .33)U (0 .31)2-Methyl-4,6-dinitrophenolmg/kgU (1 .6)U (1 .7)U (1 .6)N-Nitrosodiphenylaminemg/kgU (0 .31)U (0 .33)U (0 .31)4-Bromophenyl-phenylethermg/kgU (0 .31)U (0.33)U (0 .31)U (0 .31)0 .20 .0052703 .4Hexachlorobenzenemg/kg0 .73U (0 .31)U (0 .33)Pentachlorophenolmg/kg0 .01U (1 .6)U (1 .7)U (1 .6)Phenanthrenemg/kgU (0 .31)U (0 .33)U (0 .31)Anthracenemg/kg4,300U (0 .31)U (0 .33)U (0 .31)Di-n-butyIphthalatemg/kg1,700U (0 .31)U (0 .33)U (0 .31)Fluoranthenemg/kg2,100U (0 .31)U (0 .33)U (0 .31)Pyrenemg/kg1,500U (0 .31)U (0 .33)U (0 .31)Azobenzenemg/kgU (0 .31)U (0 .33)U (0 .31)Butylbenzylphthalatemg/kg5,600U (0 .31)U (0 .33)U (0 .31)3,3-Dichlorobenzidinemg/kg0 .02U (0 .63)U (0 .68)U (0 .64)Benzo(a)Anthracenemg/kg6U (0 .31)U (0 .33)U (0 .31)Chrysenemg/kg620U (0 .31)U (0 .33)U (0 .31)bis(2-Ethylhexyl)phthalatemg/kg1,200U (0 .31)U (0 .33)U (0 .31)Di-n-octylphthalatemg/kg810,000U (0 .31)U (0 .33)U (0 .31)Benzo[b]Fluoranthenemg/kg20U (0 .31)U (0 .33)U (0 .31)Benzo[k]fluoranthenemg/kg200U (0 .31)U (0 .33)U (0 .31)Benzo[a]pyrenemg/kg3U (0 .31)U (0 .33)U (0 .31)lndeno[1,2,3-c,d]pyrenemg/kg54U (0 .31)U (0 .33)U (0 .31)Dibenzo[a,h]anthracenemg/kg6U (0 .31)U (0 .33)U (0 .31)Benzo[g,h,i]perylenemg/kgU (0 .31)U (0 .33)U (0 .31)Notes :1.2.3.4.5.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits obtained from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means no limit was cited in 18 AAC 75 .341 .Table 6CPCB Results by EPA Method 8082 for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999No .Sample No .SiteAroclor-1016mg/kgAroclor-1221mg/kgAroclor-1232m /kAroclor-1242m /kAroclor-1248m /kAroclor-1254m /kAroclor-1260m /k199-GAM-009-SL12U (0 .0477)U (0 .0477)U (0 .0477)U (0 .0477)U (0 .0477)U (0 .0477)U (0 .0477)299-GAM-010-SL12U (0 .0365)U (0 .0365)U (0 .0365)U (0.0365)U (0 .0365)U (0 .0365)U (0 .0365)399-GAM-011-SL12U (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)499-GAM-012-SL8U (0 .00319)U (0 .00319)U (0 .00319)U (0 .00319)U (0 .00319)U (0 .00319)U (0 .00319)599-GAM-013-SL8U (0 .00329)U (0 .00329)U (0 .00329)U (0 .00329)U (0 .00329)U (0 .00329)U (0 .00329)U (0 .00338)U (0 .00338)U (0 .00338)U (0 .00338)0 .0317699-GAM-014-SL (1)4AU (0 .00338)U (0 .00338)799-GAM-015-SL (1)4AU (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)U (0 .00353)0 .0111899-GAM-016-SL (1)4AU (0 .0033)U (0 .0037)U (0 .0088)U (0 .013)U (0 .0089)U (0 .0038)U (0 .0020)999-GAM-017-SL4AU (0 .00325)U (0 .00325)U (0 .00325)U (0 .00325)U (0 .00325)U (0 .00325)U (0 .00325)1099-GAM-018-SL4AU (0 .349)U (0,349)U (0 .349)U (0 .349)U (0 .349)U (0 .349)U (0 .349)1199-GAM-019-SL4AU (0 .0314)U (0 .0314)U (0 .0314)U (0 .0314)U (0 .0314)U (0 .0314)U (0 .0314)U (0 .0390)U (0 .0390)U (0 .0390)1299-GAM-020-SL (2)4BU (0 .0390)U (0 .0390)U (0 .0390)U (0 .0390)1399-GAM-021-SL (2)4BU (0 .0386)U (0 .0386)U (0 .0386)U (0 .0386)U (0 .0386)U (0 .0386)U (0 .0386)1499-GAM-022-SL (2)4BNRNRNRNRNRNRNR1599-GAM-023-SL4BU (0 .00343)U (0 .00343)U (0 .00343)U (0 .00343)U (0 .00343)U (0 .00343)U (0 .00343)1699-GAM-024-SL4BU (0 .00317)U (0 .00317)U (0 .00317)U (0 .00317)U (0 .00317)U (0 .00317)U (0 .00317)U (0 .00341)U (0 .00341)U (0 .00341)1799-GAM-025-SL4BU (0 .00341)U (0 .00341)U (0 .00341)U (0 .00341)1899-GAM-026-SL6U (0 .00326)U (0 .00326)U (0 .00326)U (0 .00326)U (0 .00326)U (0 .00326)U (0 .00326)1999-GAM-027-SLMFBNRNRNRNRNRNRNRNRNRNRNRNRNRNR111112099-GAM-028-SLMTBADEC Regulatory Limit - 18 AAC 75 .341, Table B111.Samples 99 -GAM-017- SL are parts of a triplicate sample where1Notes :99-GAM-014-SL is the project sample, 99-GAM-015-SL is the qualitycontrol sample, and 99-GAM-016-SL is the quality assurance sample .2 . Samples 99-GAM-023-SL are parts of a triplicate sample where99-GAM-020-SL is the project sample, 99-GAM-021-SL is the qualitycontrol sample, and 99-GAM-022-SL is the quality assurance sample .3 . mg/kg means milligrams per kilogram .4 . "U" means undetected . The number in parenthesis is the laboratorydetection limit .5 . "MFB" means methanol field blank .6 . "MTB" means methanol trip blank .7 . Laboratory data sheets are provided in Appendix F .8 . Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .9 . Based on Note 9 for Table B1 in 18 AAC 75 .341, PCB limit is 1 mg/kg forresidential areas .10 . "NR" means not run . (PCB analysis was not required for Sample Numbers99-GAM-020-SL, 99-GAM-021-SL, and 99-GAM-022-SL for per Modification No . 04P4 .Table GDPesticide Results by EPA Method &081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-009-SL(Site 12Sample No .99-GAM-010-SL(Site 12Sample No .99-GAM-011-SL(Site 12alpha-BHCmg/kgU (0 .00477)U (0 .00364)U (0 .000353)beta-BHCmg/kg0 .09210 .0438U (0 .000353)gamma-Chlordanemg/kgl .? (0 .00477)U (0 .00364)U (0 .000353)alpha-Chlordanemg/kgU (0 .00477)U (0 .00364)U (0 .000353)gamma-BHC (Lindane)mg/kgU (0 .00477)U (0 .00364)U (0 .000353)delta-BHCmg/kg0 .00668U (0 .00364)U (0 .000353)Heptachlormg/kg8U (0 .00477)U (0 .00364)U (0 .000353)Aldrinmg/kg1 .6U (0 .00477)U (0 .00364)U (0 .000353)Heptachlor epoxidemg/kg0 .2U (0 .00477)U (0 .00364)U (0 .000353)Endosulfan Img/kgU (0 .00477)U (0 .00364)U (0 .000353)4,4'-DDEmg/kgU (0 .00477)U (0 .00364)U (0 .000353)Dieldrinmg/kg0 .015U (0 .00477)U (0 .00364)U (0 .000353)Endrinmg/kg0 .3U (0 .00477)U (0 .00364)U (0 .000353)Endosulfan IImg/kgU (0 .00477)U (0 .00364)U (0 .000353)4,4'-DDDmg/kg0 .0100U (0.00364)0 .000494Endrin aldehydemg/kgU (0 .00477)U (0.00364)U (0 .000353)4,4'-DDTmg/kg0.00668U (0 .00364)0 .000953Endosulfan sulfatemg/kgU (0 .00477)U (0 .00364)U (0 .000353)Endrin ketonemg/kgU (0 .00477)U (0 .00364)U (0 .000353)Methoxychlormg/kg52U (0 .00477)U (0 .00364)U (0 .000353)Toxaphenemg/kg10U (0 .477)U (0 .364)U 0 .0353Notes :1 . mg/kg means milligrams per kilogram .2 . "U" means undetected . The number i n parenthesis is the laboratory detection limit .3. Laboratory data sheets are provided in Appendix F .4 . Regulatory limits are from 18 AAC 75.341, Table B1 , Method 2 .5 . Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Table 6D (Continued)Pesticide Results by EPA Method 8081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-012-SL(Site 8)Sample No.99-GAM-013-SL(Site 8alpha-BHCmg/kgU (0 .00319)U (0 .000329)beta-BHCmg/kg0 .0332U (0 .000329)gamma-Chlordanemg/kgU (0 .00319)U (0 .000329)alpha-Chlordanemg/kgU (0 .00319)U (0 .000329)gamma-BHC (Lindane)mg/kgU (0 .00319)U (0 .000329)delta-BHCmg/kgU (0 .00319)U (0 .000329)Heptachlormg/kg8U (0 .00319)U (0 .000329)Aldrinmg/kg1 .6U (0 .00319)U (0 .000329)Heptachlor epoxidemg/kg0 .2U (0 .00319)U (0 .000329)Endosulfan Img/kgU (0 .00319)U (0 .000329)4,4'-DDEmg/kgU (0 .00319)U (0 .000329)Dieldrinmg/kg0 .015U (0 .00319)U (0 .000329)Endrinmg/kg0 .3U (0 .00319)U (0 .000329)Endosulfan IImg/kgU (0 .00319)U (0 .000329)4,4'-DDDmg/kgU (0 .00319)U (0 .000329)Endrin aldehydemg/kgU (0 .00319)U (0 .000329)4,4'-DDTmg/kgU (0 .00319)U (0 .000329)Endosulfan sulfatemg/kgU (0 .00319)U (0 .000329)Endrnn ketonemg/kgU (0 .00319)U (0 .000329)Methoxychlormg/kg52U (0 .00319)U (0 .000329)Toxaphenemg/kg10U (0 .319)U (0 .0329)Notes :1.2.3.4.5.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratorydetection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means that no limit is cited in 18AAC 75 .341 .Table 6D (Continued)Pesticide Results by EPA Method 8081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-014-SL(Site 4A/Area 413)Sample No .99-GAM-015-SL(Site 4A/Area 413)Sample No.99-GAM-016-SL(Site 4A/Area 46alpha-BHCmg/kgU (0 .00507)U (0 .00177)U (0 .00020)beta-BHCmg/kgU (0 .00507)U (0 .00177)U (0 .00047)gamma-Chlordanemg/kgU (0 .00507)U (0 .00177)NRalpha-Chlordanemg/kgU (0 .00507)U (0 .00177)NRgamma-BHC (Lindane)mg/kgU (0 .00507)U (0 .00177)U (0 .00020)delta-BHCmg/kgU (0 .00507)U (0 .00177)U (0 .00020)Heptachlormg/kg8U (0 .00507)U (0 .00177)U (0 .00023)Aldrinmg/kg1 .6U (0 .00507)U (0 .00177)U (0 .00020)Heptachlor epoxidemg/kg0 .2U (0 .00507)U (0 .00177)U (0 .00020)Endosulfan Img/kgU (0 .00507)U (0 .00177)U (0 .00020)4,4'-DDEmg/kgU (0 .00507)U (0 .00177)U (0 .00020)Dieldrinmg/kg0 .015U (0 .00507)U (0 .00177)U (0 .00020)Endhnmg/kg0 .3U (0 .00507)U (0 .00177)U (0 .00020)Endosulfan IImg/kgU (0 .00507)U (0 .00177)U (0 .00044)4,4'-DDDmg/kgU (0 .00507)U (0 .00177)U (0 .00024)Endrin aldehydemg/kgU (0 .00507)U (0 .00177)U (0 .00021)4,4'-DDTmg/kgU (0 .00507)U (0 .00177)U (0 .00044)Endosulfan sulfatemg/kgU (0 .00507)U (0 .00177)U (0 .00021)Endrin ketonemg/kgU (0 .00507)U (0 .00177)U (0 .00021)Methoxychlormg/kg52U (0 .00507)U (0 .00177)U (0 .00076)Toxaphenemg/kg10U (0 .507)U (0 .177)U (0 .0030)Notes :1.2.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .3.Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Samples 99-GAM-014-SL, 99-GAM-015-SL, and 99-GAM-016-SL are parts of a triplicatesample where 99-GAM-014 is the project sample, 99-GAM-015-SL is the quality controlsample, and 99-GAM-016-SL is the quality assurance sample .Based on Modification No . 04P4, pesticide analyes were not required for Sample No .99-GAM-020-SL through 99-GAM-025-SL ."NR" means not run .4.5.6.7.8.Table 6D (Continued)Pesticide Results by EPA Method 8081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-017-SL(Site 4A/Area 4BSample No .99-GAM-018-SL(Site 4A/Area 48)Sample No .99-GAM-019-SL(Site 4A/Area 4Balpha-BHCmg/kgU (0 .000325)U (0 .697)U (0 .0110)beta-BHCmg/kgU (0 .000325)U (0 .697)U (0 .0110)gamma-Chlordanemg/kgU (0 .000325)U (0 .697)U (0 .0110)alpha-Chlordanemg/kgU (0 .000325)U (0 .697)U (0 .0110)gamma-BHC (Lindane)mg/kgU (0 .000325)U (0 .697)U (0 .0110)delta-BHCmg/kgU (0 .000325)U (0 .697)U (0 .0110)Heptachlormg/kg8U (0 .000325)U (0 .697)U (0 .0110)Aldrinmg/kg1 .6U (0 .000325)U (0 .697)U (0 .0110)Heptachlor epoxidemg/kg0 .2U (0 .000325)U (0 .697)U (0 .0110)Endosulfan Img/kgU (0 .000325)U (0 .697)U (0 .0110)4,4'-DDEmg/kgU (0 .000325)U (0 .697)U (0 .0110)Dieldrinmg/kg0 .015U (0.000325)U (0 .697)U (0 .0110)Endrinmg/kg0 .3U (0.000325)U (0 .697)U (0 .0110)Endosulfan IImg/kgU (0 .000325)U (0 .697)U (0 .0110)4,4'-DDDmg/kgU (0.000325)U (0.697)U (0 .0110)Endrin aldehydemg/kgU (0 .000325)U (0.697)U (0 .0110)4 .4'-DDTmg/kg0 .000358U (0.697)U (0 .0110)Endosulfan sulfatemg/kgU (0 .000325)U (0.697)U (0 .0110)Endrin ketonemg/kgU (0 .000325)U (0 .697)U (0 .0110)Methoxychlormg/kg52U (0 .000325)U (0 .697)U (0 .0110)Toxaphenemg/kg10U (0 .0325)U (69 .7)U (1 .10)Notes :1.2.3.4.5.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2.Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Table 6D (Continued)Pesticide Results by EPA Method 8081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-020-SL(Site 4A/Area 4BSample No .99-GAM-021-SLSite 4A/Area 413)Sample No .99-GAM-022-SL(Site 4A/Area 46alpha-BHCmg/kgU (0 .0117)U (0 .0116)NRbeta-BHCmg/kgU (0 .0117)U (0 .0116)NRgamma-Chlordanemg/kgU (0 .0117)U (0 .0116)NRalpha-Chlordanemg/kgU (0 .0117)U (0 .0116)NRgamma-BHC (Lindane)mg/kgU (0 .0117)U (0 .0116)NRdelta-BHCmg/kgU (0 .0117)U (0 .0116)NRHeptachlormg/kg8U (0 .0117)U (0 .0116)NRAldrinmg/kg1 .6U (0 .0117)U (0 .0116)NRHeptachlor epoxidemg/kg0 .2U (0 .0117)U (0 .0116)NREndosulfan Img/kgU (0 .0117)U (0 .0116)NR4,4'-DDEmg/kgU (0 .0117)U (0 .0116)NRDieldrinmg/kg0 .015U (0 .0117)U (0 .0116)NREndrinmg/kg0 .3U (0 .0117)U (0 .0116)NREndosulfan IImg/kgU (0 .0117)U (0 .0116)NR4,4'-DDDmg/kgU (0 .0117)U (0 .0116)NREndrin aldehydemg/kgU (0 .0117)U (0 .0116)NR4,4'-DDTmg/kgU (0 .0117)U (0 .0116)NREndosulfan sulfatemg/kgU (0 .0117)U (0 .0116)NREndrin ketonemg/kgU (0 .0117)U (0 .0116)NRMethoxychlormg/kg52U (0 .0117)U (0 .0116)NRToxaphenemg/kg10U (1 .17)U (1 .16)NRNotes :1.2.3.4.5.6.7.8.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Samples 99-GAM-020-SL, 99-GAM-021-SL, and 99-GAM-022-SL are parts of a triplicatesample where 99-GAM-020 is the project sample, 99-GAM-021-SL is the quality controlsample, and 99-GAM-022-SL is the quality assurance sample .Based on Modification No . 04P4, pesticide analyses were not required for Sample No .99-GAM-020-SL through 99-GAM-025-SL ."NR" means not run .Table 6D (Continued)Pesticide Results by EPA Method 8081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No .99-GAM-024-SL(Site 48/Ares 413)Sample No.99-GAM-025-SL(Site 4B/Ares 4BSample No .99-GAM-023-SLSite 4B/Ares 46alpha-BHCmg/kgU (0 .000317)U (0 .000341)U (0 .00171)beta-BHCmg/kgU (0 .000317)U (0.000341)U (0 .00171)gamma-Chlordanemg/kgU (0 .000317)U (0 .000341)U (0 .00171)alpha-Chlordanemg/kgU (0 .000317)U (0 .000341)U (0 .00171)gamma-BHC (Lindane)mg/kgU (0 .000317)U (0 .000341)U (0 .00171)delta-BHCmg/kgU (0 .000317)U (0 .000341)U (0 .00171)Heptachlormg/kg8U (0 .000317)U (0 .000341)U (0 .00171)Aldrinmg/kg1 .6U (0 .000317)U (0 .000341)U (0 .00171)Heptachlor epoxidemg/kg0 .2U (0 .000317)U (0 .000341)U (0 .00171)Endosulfan Img/kgU (0 .000317)U (0 .000341)U (0 .00171)4,4'-DDEmg/kgU (0 .000317)U (0 .000341)U (0 .00171)Dieldrinmg/kg0 .015U (0 .000317)U (0 .000341)U (0 .00171)Endrinmg/kg0 .3U (0 .000317)U (0 .000341)U (0 .00171)Endosulfan IImg/kgU (0 .000317)U (0 .000341)U (0 .00171)4,4'-DDDmg/kgU (0 .000317)U (0 .000341)U (0 .00171)Endrin aldehydemg/kgU (0 .000317)U (0 .000341)U (0 .00171)4,4'-DDTmg/kgU (0 .000317)U (0 .000341)U (0 .00171)Endosulfan sulfatemg/kgU (0 .000317)U (0 .000341)U (0 .00171)Endrin ketonemg/kgU (0 .000317)U (0 .000341)U (0 .00171)Methoxychlormg/kg52U (0 .000317)U (0 .000341)U (0 .00171)Toxaphenemg/kg10U (0 .0317)U (0 .0341)U (0 .171)Notes :1.2.3.4.5.mg/kg means milligrams per kilogram ."U" means undetected . The number in parenthesis is the laboratory detection limit .Laboratory data sheets are provided in Appendix F .Regulatory limits are from 18 AAC 75 .341, Table B1, Method 2 .Blank space in regulatory limits column means that no limit is cited in 18 AAC 75 .341 .Table 6D (Continued)Pesticide Results by EPA Method 8081A for Confirmation SamplesDebris Removal and Containerized Hazardous and Toxic Waste RemovalDelivery Order 0004, Contract No . DACA85-97-D-0010, Gambell, AlaskaSample Date : August 14, 1999Anal esUnitsRegulatoryLimitsSample No.99-GAM-026-SL(Site 6alpha-BHCmg/kgU (0 .000326)beta-BHCmg/kgU (0 .000326)gamma-Chlordanemg/kgU (0 .000326)alpha-Chlordanemg/kgU (0 .000326)gamma-BHC (Lindane)mg/kgU (0 .000326)delta-BHCmg/kgU (0 .000326)Heptachlormg/kg8U (0 .000326)Aldrinmg/kg1 .6U (0 .000326)Heptachlor epoxidemg /kg0 .2U (0 .000326)Endosulfan Img/kgU (0 .000326)4,4'-DOEmg/kgU (0 .000326)Dieldrinmg/kg0 .015U (0 .000326)Endrinmg/kg0 .3U (0 .000326)Endosulfan IImg/kgU (0.000326)4,4'-DDDmg/kgU (0 .000326)Endrin aldehydemg/kgU (0 .000326)4,4'-DDTmg/kgU (0 .000326)Endosulfan sulfatemg /kgU (0 .000326)Endrin ketonemg/kgU (0 .000326)Methoxychlormg/kg52U (0 .000326)Toxaphenemg/kg10U (0 .0326)Notes : 1 . mg/kg means milligrams per kilogram .2 . "U" means undetected . The number in parenthesis is thelaboratory detection limit .3. Laboratory data sheets are provided in Appendix F .4. Regulatory limits are from 18 AAC 75 .341, Table B1 , Method 2 .5 . Blank space in regulatory limits column means that no limit iscited in 18 AAC 75 .341 .Appendix FChain of Custody and Laboratory Data Reports'3`3-3E'S4Page 1 ofChain of CustodyAuthorization Numbs. .Debris Removal & Containerized Hazardous & Toxic Waste RemovalGambell, AlaskaContract No : DACA 85-97-0-0010, Delivery Order #4a1 y C FS/ySamplers:Clientr'urchase Order No . 913Oil Spill Consultants, Inc .Th . Environmental Cleanup Company209 E . 51st. Avenue, Anchorage , Alaska 99503Tel : (907) 562-7169 Fax: ( 907) 562-7225Anal sis RequiredAnalysis Required by :oC'00YdeldSampleScreenSample Number Date-64M-00 -99-3VI-C02 _SZ--Relinquished by : (Printed)(Signature)Relinquished by : (Printed)(Signature)Dispatched by : (Printed)(Signature)Method of Shipment:Comments:17-19-?9Time PID ReadingType# of6Cont .8Ydrawa-a _Po C; cN~~~ a• CaC5 C; -r- 0Lo oU `8 vCd,ea. 608aCE--D w:r501v v vso /VrVSONrvvs~s/rd/ r.'r/'s -~~/wGo(i 'a ~ q1 ~~'0 o. - r'na t- oCL a .w co ov'/ QCRequiredl77/9 -9Date / fCT ime'2? re~'11Gv1/Received by : (Printed)(Signature)Received by : (Printed)(Signature)R:-3i at aboratyry by:r, I1Condition of Contalner1Fair&lPoorReceived Tamp:2. 3993654CT& E Environmental Services Inc .iurwiuasiiviiSAMPLE RECEIPT FORMAre samples RUSH, priority, or within 72 hrs of hold time?If yes, have you done e-mail notification?Arc samples within 24 firs of hold time or due date?If yes, have you spoken with Supervisor?Are there any problems (e .g ., ids , analyses)?Were samples preserved correctly and pH verified?CT&E WON :Due Date :Received Date/Time :Cooler Temperature :Sample Condition :Maof each Sample :Good / Poor°Has Project Manager been notified of problems?Is this an ACOE/AFCEE/ADEC project?Will a data package be required?If this is for PWS, provide PWSID .Is there a quote for this project?Will eoudler charges apply?4', U 1,r` PL,` 1 ) 'r 5Completed by (sign ) :Trip BlankMS/MSDAdditional Sample RemarkAK 101 s / 8260s field pres'd?Field -filtered for dissolved ?Lab-filter for dissolvedRef Lab required ?Notes :The following must be completed for all ACOE & AFCEE projects : "'Yesx Is coolerNoNotes :temperature 4 + C? ~, 3thermometer used :T 1~ L_3Was there an airbill , etc? note N :Was cooler scaled with custody seals?N/where?r('c,y GoQYl er~Were seals intact upon arrival?X( Was there a COC with cooler?Was the COC filled out properly?Did the COC indicate ACOE/AFCEE project?Did the COC and samples correspond?X _Were samples screened with Geiger counter?Were all samples packed to prevent brec?Xpacking material :to-AC,Were all samples unbroken and clearly labelled?Were all samples scaled in separate plastic bags?Were all bottles for volatiles free of headspace?Were correct container/ sample sizes submitted?Was client notified of problems? (specify below)N of each Container Received :950 ml amber unpres'd950 ml amber w/ IICI500 ml amber w/ 112SO41L cubiesunpres'd1L cubiesw/ IIN031L cubiesw/ 112SO41L cubiesw/ NuOll + ZnAc120 ml colibottles60 mlNalg8ozamberunpres'dc4 oz amberunpres'd4 oz w / septa w/ McOH40 ml vialsOther (specify)Other (specify)Individual contacted :n'A' .&Tine-Phone/FaxN:N/log In Proofed by :w/ I ICIAL.CT&E Environmental Services Inc .Laboratory Division200 W. Potter DriveAnchorage, AK 99518-1605Tel : (907) 562-2343Fax : (907) 561-5301Oil Spill Consultantsattention : Randy Easley209 E 51stAnchorage, AK 99503Account: Oil Spill ConsultantsContact: Randy EasleyProject: Gambell DACA85-97-D-0010 DO 4Received: 07/21/99 15:50CT&E Ref# : 99.3654Print Date : 08/20/99 10 :59Work order 99 .3654 was analyzed for Dioxinsby Triangle Laboratories of Durham, NC 27713-4411Locations NCHAIN OF CU JDY RECORD. At..k.. .dpan‚ CAU10(r" Now Jersey‚ Colƒado ‚ Ohio‚ Maryland ‚ West VkgtJaCT&E Environmental Services Inc .Laboratory Division #,'" AwArA'ArAwAwAwAw Aww ArAwAwAwAwArM W MWAWMM " AW " AW " AW " M ,Zmt,koh,1CUE Reference :CLIENTCONTACT :'{1 ,I° II~PROJECT : D r\ (rSjPAGE-J_,OF_PHONE NO : ( -)) 4,<1„i~ ()No .(1, i l~l ~ 7 I A N I)E I IREPORTS TO:lFAX'INO : (+1 ' ~-INVOICE TO :,~1<WB NO.SDATEC.NCOMPAIG .GRABTIMEJMATRIX~ ~T ' ri jr.DateSDateTimeREMARKSIw4Received By :Shipping Carrier :i ; .l J~(:~Relinquished By : (2)MwR~q~rdr~-1 rj1~ ~~ ~Zp p~C0PO . NUMBER :SAMPLE IDENTIFICATIONL.Weoi~lAelirpuished By : (1)Pia.nauv .SAMPLE uwdTYPEReceived By:TimeDateReceived By :Samples Received Cold? (Girds) YES NOShipping Tidcei No~~l iTemperatureData Deliveribles Required/Chain of Custody Seal : (Girds)Level IRelinquished By : (3)t-{-~ 1~Level II Levell llCCINTACTC:BROKENABSENTRequested Turnaround Time and Special Instructions :~' (I a c ( fl-r-Relnqulshed By : (4)F-+DaTimeReceived For Laborat By :I/qW 200 W . Potter Drive Anchorage , AK 99518 Tel : (907) 562 .2343 Fax : (907)o-e- o -A ak oo7n1 TAI' /9n71 474-R(i58 Fax : (9071474-9685561-5301While- RetaMwd by Lab (Project FY.) Ye llow - Returned with ReportPink - Retairrd by Sam pierCustody SealPresent/IntactChain of CustodyPresentSample TagsAbsentSample Tay Numbers : Nut Listed on chain ofSMO Forms: N/A# ice ChestTRIANGLE LABORATORIES , INC . -- TAG IN RECORD /CHAIN OF CUSTODYSample Seals : Present I TLI Project Number 49151Container . . . :IntactIClient : CTE06 - CT 6 E EnvironmentalServicesICustody.1%ICE PACKS -I Date Received 1 07/24/99+Temp 6 .0 CI By -II Carrier and Number I FedEx/iHT L1 Number . .rmR / H :CPM .#242-60 - 1#. . . . . . .Client Sample ID . . . . . . . . . . . . . . . . . . . . . Matrix). . . . . . . . Client COC ID . . . . . . . . . . Location . . . . . . . I99GAM - 005-Sl ,- 993654 -599 . 1654 -5To I .AB I To STORAGEIDate / Init I Date/Toil ITo LABDate/InitTo STORAGEIDate/Lull ITo LABDate/InitI To STORAGEI To LABI Date/Init I Date/InitI To STORAGEI DISPOSEDI Date / Init I Date/InitSOILICO 1I~( ,I`~ a(`INN'uNNIrIIIIIIIIII+IIIIII}lINIIN4IurNNNINNNINuMIIIIIIIIIIIII+II'II+IIIIIIIIINN1IrIfIInIIIIHi%V--1n~INReceiving Remarks :IArchive Remarks :II-Form Revised 05/27 / 1997I--Page 1 OF 1. age 1 ofChain of CustodyPr *d: Debris Removal & Containerized Hazardous S Toxic Waste R.movalOamb.11, Alaska Contract No: DACASS47-D 0010, Delivery Order *4Client:Oil Spill Consultants, Inc.The Envk+onmsnW Cleanup Company209 E . 51st. Avenue, Anchorage, Alaska 99503Tel : (907) 562-7169 Fax : (907) 562-7225Anal sis RequiredAnalysis R.qulr d by:aweldSampleScreen Sam Number Date TimePIO ReadingT# ofCont .ONO0nb~adOU^LOadad'00. C)a r•oN1 00-Z3w0C2 44 N0010 00y Nm p a• d a ,,a a00 > w11u- •u-1C-2Y/!./ ACRequiredEll"'‚ 30Data(Signature)Relinquished by : (Printed)S natureDispatched by: (Printed)S turoMethod of Shipment : 46, . 4/Comments :aon'IReltrp ulshed by : (Printed)wE(n CqP 4,-2- - D -coITimeReceived bv: ( Printed)Received by: (Printed)(Signaturd)Received at Laboratory by :Condition of Containers I./yr/~rf993834Fair Poor'ReceivedTa mp_ `' 0993630",r.'tsl0kCT& E Environmental Services Inc .rSAMPLE RECEIPT FORMAre samples RUSH , priority, or within 72 hrs of hold time?If yes, have you done e-mail notification?Ark samples within 24 firs of hold time or due date?If yes, have you spoken with Supervisor?Are there any problems (e .g ., ids , analyses)?Were samples preserved correctly and pH verified?CT&E WOO :"W"f`1Due Date :Received Date /Time :Cooler Temperature :Sample Condition :Matrix of each Sample:-i11,uu PoorN11 "Has Project Manager been notified of problems?Is this an ACOE/AFCEE/ADEC project?Will a data package be required?If this is for PWS, provide PWSID .Is there a quote for this project?Trip BlankMS/MSD _Additional Sample Remarks :AK101s / 8260s field pres'd?Field- filtered for dissolved_ ?courier charges apply?Completed by (sign) :* * The followingYes No(print):be completed for all ACOE & AFCEE projects: . . .Notes :Is cooler temperature 4 + C?thermometer used :Was there an airbill, etc? note # :Was cooler sealed with custody seals?#/where?Were seals intact upon arrival?Was there a COC with cooler?Was the COC filled out properly?Did the COC indicate ACOE/AFCEE project?Did the COC and samples correspond?Were samples screened with Oelger counter?Were all samples packed to prevent breakage?packing material :Were all samples unbroken and clearly labelled?Were all samples scaled in separate plastic bags?Were all bottles for volatiles free of headspace?Were correct container/sample sizes submitted?Was client notified of problems? (specify below)Lab-filter for dissolved____Refb required?Notes :W1I of each Container Received :950 ml amber unpres'd950 ml amber w/ Lid500 ml amber w/ 112SO41L cubiesunpres'd1 L cubiesw/ IiNO31 L cubiesw/ 112SO41 L cubiesw/ NaOH + ZnAc120 ml colibottles60 mlNulg8 oz amberunpres'd4 oz amberunpres'd44 oz w/ septa w/ McOll40 ml vialsw/ 110Other (specify)Other (specify)Individual contacted :Date & Time :Phone/ Fax # :N /Log In Proofed by :t w/n Numbw f oO42Chain of CustodyProject :Debris Removal & Containerized Hazardous & Toxic Waste RemovalG amb ell , A laska Contract No : DACA85 -97-D-0010 , Delivery O rder #4Page 1 ofAuthorization Number : OSCI Purchase Order No . 913Samplers :Client:RandyE . EasleyOil Spill Consultants, Inc .The Environmental Cleanup Company(Signature)Witness : 0,.-i_ i c/209 E . 51st . Avenue, Anchorage, Alaska 99503Tel : (907) 562-7169 Fax : (907) 562-7225~,994255(Signature)Analysis Required by :Analysis RequiredOFieldSampleSample NumberDate#TimePID Readingl`-9- "/V -o4%-SL'9-/ Y -f '9120,0109119-e5 ,9, 111- o/o -fi-~q•zo99-G~it'/-O/l -'rZt/ -9/.2 190,70TypeCont.G.uh262~'-/5'-yy _ _Grc6- "W-D/ Y fZc- ' 9,? 0 5'DGr~~zlq9-G /y1-o/5- Szo/ 7 -sZ-fLf7'V-9o yoGr~62~~Y-yy 3s /Sz9'9-G~ih-oly -'CZyi~-~i 3o yS___Gr~.6G1~6Relinquished by : (Printed )(Signature)Relinquished by : (Pri?Sted)4~ndy dt /V 79 3; 30,~-ls e?r-(Signature)Dispatched by : (Printed)(Signature)Method of Shipment :Comments :~~IN44QA/Requiredvv!~v~-vvQCvi//,vvvvi/22Date I TimeI, -,? 5 t?of4iZt1ov-GiV/-o% ? SLu\kZOh4Z,Screen-6L)''ZReceived by : (Printed)-i '9y(Signature)Received by: (Printed)(Signature)Received at Laboratory by :/B1tnae 2 1 l8 `i5Condition of Containers2a/P/Good Fair PoorReceived TernLPage 1 ofChain of CustodyProject :Debris Removal & Containerized Hazardous & Toxic Waste RemovalGambell , Alaska Contract No : DACA85-97-D-0010 , Delivery Order #4Client:Authorization Number :OSCI Purchase Order No . 913(Samplers:E . EasleyRandyOil Spill Consultants, Inc .99 4255The Environmental Cleanup Company209 E . 51st . Avenue , Anchorage , AlaskaTel : (907) 562-7169 Fax : (907) 562-722599503Witness : p,,,, ,/ /L . Re-la/'(Signature )4Analysis Requir edAnalysis Required by :VtiQFieldSampleScreenSample Number Date TimePID ReadingType# ofCont .l 9- GSM -02 O SL8=/v-95;•30Gr4 l3Jr ' G~9r 7 o.2/-SL9 -6F/PI -023-5f /~7'-1ya J0GrG399-6:All -02V -,SG~/y 9 S•`oO6rcl399 Gf9M 027 sZ9-G -o2~ SL~iy ' ' 7 ' 00__Relinquish(SignatureRelinquis(SignaturevIspaicneo uy : trnnreu )Date / Timey li--#vvl'vv'-'-'AI Requiredv'-Received by : (Printed)(Signature)Received by : (Printed)(Signature)Received at Laboratory by :g( Signature)Method of Shipment :Comments :QA / OC'V"Condition of on1 inersGood Fair PoorReceived Temp :Page 1 ofChain of CustodyProject :Debris Removal & Containerized Hazardous & Toxic Waste RemovalGambell , Alaska Contract No : DACA85-97-D -0010, Delivery Order #4OSCI Purchase Order No . 913Authorization Number :ClientOil Spill Consultants, Inc .The Environmental Cleanup Company209 E . 51st . Avenue, Anchorage, Alaska 99503Tel : (907) 562-7169 Fax : (907) 562-7225Analysis Re uiredAnalysis Required by :FieldSample#Screen Sample Number Date Time PID Reading9 ‚Gj9iV/-O/ -sIRelinquished by : (Printed(Signature)Relinquished by: (Prin ed(Signature)Dispatched by: (Printed)(Signature)Method of Shipment :Comments :~ ~v-sG~~h20 YoDate / Time,f-/QA/QCRequiredofType Cont .J--- -79 y'2/…vReceived by : (Printed)(Signature)Received by: (Printed)(Signature)Received La oratory by :Condition of Containers!9942b5CT& E Environmenta l S e rvice s Inc .SAMPLE RECEIPT FORMALYesCT&E WO# :NoViAre samples RUSH , priority, or within 72 hrs of hold time?If yes, have you done e-mail notification?Are . samples within 24 firs of hold time or due date?If yes, have you spoken with Supervisor?Are there any problems (e .g ., ids, analyses)?Were samples preserved correctly and pH verified?Due Date :Has Project Manager been notified of problems?Is this an ACOE/AFCEE/ADEC project?Will a data package be required?If this is for PWS, provide PWSID .Is there a quote for this project?Will courier charges apply?2 1 Trip BlankMS/MSDAdditional Sample Remarks :AK101s/ 8260s field pres'd?Field-filtered for dissolved ?Lab-filter for dissolvedRef Lab required?h4aA4zaprinfl :_Received Date /Time :Cooler Temperature :Sample Condition:Matrix of each Sample :li11g-31-ql15 5700oor--1 _ - IQ v t fi 4* 5 11-/S_1o - ff-ar ' 7Cra/u /l e I 59 .2Terphenyl-d14 ?- Fluorobiphenyl < Surr>.- Fluorophenot < Surr>Nitrobenzene - d5 13063 .352 .659XXPCB's by GC ECDAroclor- 1016ArocLor-1221Aroclor-1232Aroctor-1242Aroclor-1248Aroctor-1254Aroclor-12600 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .003190 .003190 .003190 .003190 .003190 .003190 .00319mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846 8082SW846 8082SW846 808208/20/99 08 / 22/99 WAA08/20/99 08 / 22/99 WAA08/20/99 08 / 22/99 WAA08/20 /99 08/ 22/99 WAA08/20 /99 08 / 22/99 WAA08/20 /99 08/22/99 WAA08/20 / 99 08/ 22/99 WAAXSW846 8082mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8081ASW846 - 8081ASW846-8081ASW846 - 8081ASW846-8081A08/20/99 08/26/99 LZ08/20/99 08/ 26/99 LZ08/20/99 08/26/99 L208/20 / 99 08 / 26/99 LZ08 /20/99 08/26/99 LZmg/Kgmg/KgSW846 - 8081ASW846 - 8081A08/20 / 99 08/26/99 LZ08/20/99 08 /26/99 LZSurrogatesDecachlorobiphenyl 107( 53 .3-125) 08/20 / 99 08/22/99Pesticidesalpha - BHCbeta - BHCgamma - Chlordane0 .00319 U0 .03320 .00319 Ualpha - Chlordanegamma - BHC (Lindane)delta - BHCaptachlor0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .003190 .003190 .003190 .003190 .003190 .003190 .00319LTA. . ME Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID913Client PO#09/09/9916 :27Printed Date / TimeTime08/14/99Collected Date /11 :29Received Date/Time08/18/99 16 :35Technical Director : Stephen C . Ede994255004Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-012-SLSoil/SolidResultsParameter0 .00319 UAldrinHeptachlor epoxideEndosulfan I0 .00319 U0 .00319 U0 .00319 U0 .00319 U4,41-ODEDieldrinEndrinEndosulfan II4,41-DODEndrin aldehyde4,4'-DDT0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 U0 .00319 UEndosulfan sulfateEndrin ketoneMethoxychtorToxapheneUnitsMethod0 .003190 .003190 .003190 .00319mg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846 - 8081A0 .003190 .003190 .003190 .003190 .003190 .00319mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .003190 .003190 .003190 .319mg/Kgmg/Kgmg/Kgmg/KgSW846 - 8081ASW846-8081ASW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081ASW846-8081AXXSW846-8081ASW846-8081APOL0 .319 UAllowableLimitsPrepDateAnalysisDate Init08/20 /99 08/26/99 LZ08/20/99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20/99 08/ 26/99 LZSW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081A08/20 / 99 08/26/99 LZ08/20/ 99 08/26/99 LZ08/20/ 99 08/26/99 LZ08/20/ 99 08/26/99 LZ08/20/ 99 08/26/99 LZ08/ 20/99 08/ 26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20/99 08/26/99 LZSurrogatesDecachlorobiphenyl Tetrachloro - m-xylene < Surr>I118126(46-154 )( 25-120 )08/20 /99 08/26/9908/20 /99 08/26/99AL .CT&E Environmental Services Inc .CT&E Ref .#994255005ClientPO#913Client NameOil Spill ConsultantsPrinted Date/Time09/09/99 16 :27Project Name/# Gambell DACA85-97-D-0010 DO 4 Collected Date/ Time 08/14/99 11 :40Client Sample ID 99-GAM-013-SLReceived Date/Time08/18/99 16 :35Matrix Soil/SolidTechnical Directoi>StenheuC . EdeOrdered ByPWSIDReleased BySample Remarks :8270 - Internal standard phenanthrene-d12 is biased low . The samples are non-detect . The results are not affected .8270 - LCS/LCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .DRO/RRO - Pattern consistent with lube oil .DRO - Heavier hydrocarbons contributing to diesel range quantitation .ParameterTotal SolidsResultsPQL97 .2UnitsAllowableMethod LimitsPrepDateXSM18 2540G08/24/99 BJSAnalysisDateInitRCRA MetalsArsenic3 .60BariumCadmiumChromiumLeadMercury by Cold VaporSeleniumSilver12 .70 .01963 .6214 .30 .00676 U0 .192 U0 .0384 U0 .1924 .120 .01920 .1921 .920 .006760 .1920 .0384mg/Kgmg/ Kgmg/ Kgmg/Kgmg /Kgmg /Kgmg/Kgmg / KgSW846 7060SW846 60108SW846 - 7131SW846 - 7191SW846 -7421SW846 -7471SW846 -7740SW846 -776108/ 23/99 08/30/99 JMO08/26/99 08/31/99 WTA08/ 23/99 08/24/99 KGF08 /23/99 08/24/99 KGF08/23/99 08 /24/99 KGF08/25/99 08 / 25/99 RMV08/23/99 08/27/99 GCP08/23/99 08/24/99 KGFGasoline Range Organics1 .90 U1 .90mg/KgAK101 GRO08/14/99 08/ 24/99 DARXAK101 GROAK101 GROSurrogates4-Bromoftuorobenzene 1,4-Difluorobenzene 76 .895 .3X( 50-150 )( 50-150)08/14/99 08/24/9908/14/99 08/24/99Am FM-k -CT&E Environmental Services Inc .CT&E Ref.#994255005Client NameOil Spill ConsultantsProject Name/#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-013-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . Ede91309/09/99 16 :2708/14/99 11 :4008/18 /99 16 :35AllowableParameterResultsPQLUnitsMethodmg /KgSW846-8260SW846-8260LimitsPrepAnalysisDateDateInitVOA by GC/MS Method SW8260DichlorodifluoromethaneChloromethane'inyl chloridedromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneCarbon disulfideMethylene chloridetrans-l,2 - Dichloroethene1,1-Dichloroethane2-Butanone (MEK)2,2-Dichtoropropanecis-1,2-DichloroetheneBromochloromethaneChloroform1, 1, 1-TrichloroethaneCarbon tetrachloride1,1-DichloropropeneBenzene1,2-DichloroethaneTrichloroethene1,2-DichloropropaneDibromomethaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropene'-Methyl - 2-pentanone ( MIBK)oluene0 .019 U0 .019 U0 .0190 .0190 .019 U0 .19 U0 .19 U0 .019 U0 .019 U0 .19 U0 .095 U0 .019 U0 .019 U0 .0190 .190 .190 .0190 .0190 .190 .0950 .0190 .0190 .19 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .19 U0 .190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .019 U0 .19 U0 .019 U0 .0190 .190 .0190 .0190 .0190 .0190 .19mg /Kgmg /Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/ Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260mg/Kgmg/ Kgmg/Kg ,mg/ Kgmg/Kgmg /Kgmg/Kgmg/Kgmg / Kgmg / Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/ Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846 - 8260SW846 - 8260SW846- 8260SW846 - 8260SW846-8260mg /Kgmg/Kgmg /Kgmg /KgSW846 - 8260SW846 - 8260SW846 - 8260SW846 - 826008/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14 /99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14 /99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14 / 99 08/22/99 DRS08/ 14/99 08 / 22/99 DRS08/14/99 08/ 22/99 DRS08/ 14/99 08/ 22/99 DRS08/ 14/99 08/ 22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRSLlw-ck ~ CT&E Environmental Services Inc.CT&E Ref.#994255005Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-013-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . Ede91309/09/99 16 :2708/14/99 11 :4008/18 /99 16 :35AllowableParametertrans-1,3 - Dichtoropropene1,1,2-TrichloroethaneTetrachloroethene1,3-Dichloropropane2-Hexanoneibromochloromethanei,2-DibromoethaneChlorobenzene1,1,1,2-TetrachloroethaneEthytbenzeneP & M -Xyleneo-XyleneStyreneBromoformIsopropytbenzene ( Cumene )Bromobenzene1,1,2,2 - Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene2-Chtorotoluene4-Chlorotoluene1,3,5-Trimethylbenzenetert - Butylbenzene1,2,4-Trimethylbenzenesec-Butylbenzene1,3-Dichlorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butytbenzene',2-Dibromo - 3-chloropropane, 2,4-TrichlorobenzeneResults0 .019 U0 .019 U0 .019 U0 .019 U0 .19 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .19 U0 .019 UPQL0 .0190 .0190 .0190 .0190 .190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .019UnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0190 .0190 .019mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .190 .019mg/Kgmg/KgSW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846-8260SW846-8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846-8260SW846 -8260SW846 - 8260SW846-8260SW846 - 8260SW846- 8260LimitsPrepAnalysisDateDateInit08/ 14/99 08 / 22/99 DRS08/ 14/99 08 / 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08 / 22/99 DRS08/14/99 08/22/99 DRS08/ 14/99 08/ 22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08 / 22/99 DRS08/ 14/99 08 / 22/99 DRS08/14/99 08/ 22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08 /22/99 DRS08 / 14/99 08 /22/99 DRS08 / 14/99 08 / 22/99 DRSA&LCT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994255005Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-013-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterHexachlorobutadieneNaphthalene1,2,3-TrichlorobenzeneR esu l tsPQLUnitsMethod0 .019 U0 .019 U0 .019mg/Kg0 .019mg/Kg0 .019 U0 .019mg/KgSW846-8260SW846-8260SW846-8260XXSW846 - 8260SW846 - 8260XXSW846 - 8260SW846 - 8260mg/KgAK102 / 103mg/KgAK102 / 103XXAK102/103AK102/10391309/09/99 16 :2808/14/99 11 :4008/18/99 16 :35AllowablePrep AnalysisLimitsDate DateInit08/14 /99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRSSurrogates1,2-Dichtoroethane - D4 111Dibromoftuoromethane < surr>10210196 .1Toluene - d8 4-Bromofluorobenzene (74-123)(80-118)(79-130)(71-141)08/14/99 08/22/9908/ 14/99 08/22/9908/14/99 08/22/9908/ 14/99 08/22/99DRO/RRO CombinationDiesel Range OrganicsResidual Range Organics GC30 .070 .98 .8714 .608 / 24/99 08/28/99 PIMP08/ 24/99 08/28/99 MMPSurrogates5a Androstane < surr>d-Triacontane < Surr>102135( 50-150 )( 50-150 )08/24 /99 08/28/9908/24 /99 08/28/99Semivolatiles by GC/MSN-NitrosodimethylaminePyridineAnilinePhenolBis(2 - Chloroethyl ) ether2-Chlorophenol0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .320 .320 .320 .32mg/Kgmg/KgSW846 - 8270SW846 - 827008/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZmg/Kgmg/Kg0 .32mg/Kg0 .32 U0 .320 .320 .32mg/Kgmg/Kgmg/KgSW846- 8270SW846-8270SW846 - 8270SW846 - 827008/ 22/99 08/24/99 LZ08/ 22/99 08/ 24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ0 .32mg/KgSW846 - 8270SW846 - 8270SW846 - 827008 /22/99 08/24/99 LZ08 /22/99 08 / 24/99 LZ08 / 22/99 08 / 24/99 LZ1,3-Dichlorobenzene0 .32 U', 4-Dichlorobenzene,enzyl alcohol0 .32 U0 .32 UA11wMCT&E Environmental Services Inc .CT&E Ref.994255005Client NameOil Spill ConsultantsProject Name/#Client Sample IDGatnbell DACA85-97-D-0010 DO 499-GAM-013-SLMatrixOrdered ByPWSIDSoil/SolidClient PO#913Printed Date / Time09/09/99 16 :28Collected Date/Time 08/14/99 11 :40Received Date /Time 08/18/99 16 :35Technical Director : Stephen C . EdeAllowableParameter1,2-Dichlorobenzene2-Methylphenot (o-Cresol)bis(2-chloroisopropyt)ether3&4-Methylphenol (p&m-CresoL)N-Nitroso-di-n-propylamineiexachloroethanenitrobenzeneIsophorone2-Nitrophenol2,4-DimethylphenolBenzoic acidBis(2-Chloroethoxy)methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachLorobutadiene4-Chtoro-3-methylphenot2,4-Dichlorophenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphthene2,4-DinitrophenoL4-NitrophenolibenzofuranResults0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U1 .6 U0 .32 U0 .32 U0 .32 UPaLUnitsMethod0 .32mg/Kg0 .32mg/KgSW846-8270SW846-82700 .320 .320 .32mg/Kgmg/Kg0 .320 .320 .320 .320 .321 .60 .32mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .32mg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-82700 .32mg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-82700 .65 U0 .32 U0 .65 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U1 .6 U0 .32 U0 .650 .320 .650 .320 .32mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-82700 .32mg/Kg0 .32mg/Kg0 .320 .32mg/Kgmg/Kg1 .6mg/Kg0 .320 .32 U0 .32 U1 .6 U0 .32 U0 .320 .321 .60 .32mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-82701 .6 U1 .6 U0 .32 U1 .6mg/Kg1 .60 .32mg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270LimitsPrepAnalysisDateDate Init08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 /99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZAN I -CT&E Environmental Services Inc .CT&E Ref .#994255005Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-013-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameter2,4-DinitrotolueneDiethylphthalate4-Chlorophenyt - phenyletherFluorene4-Nitroaniline'-Methyl-4,6- dinitrophenol4-Nitrosodiphenylamine4-Bromophenyl - phenyletherHexachtorobenzenePentachlorophenolPhenanthreneAnthraceneOi-n-butylphthalateFluoranthenePyreneResu l tsPOL0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U1 .6 U0 .32 U0 .32 U0 .32 U0 .320 .320 .320 .320 .321 .60 .320 .320 .32UnitsMethodmg/KgSW846 - 8270SW846 - 8270SW846 - 8270SW846-8270mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgAzobenzeneButytbenzylphthalate3,3-Dichlorobenzidine0 .320 .320 .320 .320 .320 .320 .65mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgBenzo ( a)Anthracene0 .32 U0 .32mg/KgChrysenebis(2 -Ethylhexyl) phthalatedi-n-OctylphthatateBenzo[b] FluorantheneBenzo[k]fluoranthene0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .320 .32mg/Kgmg/Kg0 .32mg/Kg0 .320 .320 .320 .320 .320 .32mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270XSW846-8270Benzota ] pyreneIndeno[1 , 2,3-c,d] pyreneDibenzo[a , h]anthraceneBenzo[g , h,i]perylene1 .60 .32AllowablePrepAnalysisLimitsDateDate08/22/99 08/ 24/99 LZ08 /22/99 08/24/99 LZ08/22 / 99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08 / 24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/ 24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 / 99 08/ 24/99 LZ08/ 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZSurrogates, 4,6-Tribromophenot r-81 .2Init08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZSW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82701 .6 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .32 U0 .65 U91309/09/99 16 :2808/14/99 11 :4008/18/99 16 :35( 18-122)08/22/99 08/24/99A ..CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name/#Client Sample IDMatrixOrdered ByPWSID994255005Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-013-SLSoil/SolidParameterResultsPQLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/09/99 16 :2808 /14/99 11 :4008/18 /99 16 :35Technical Director : Stephen C . EdeAllowablePrepAnalysisUnitsMethodLimitsDateDate InitXXSW846 - 8270sW846 - 8270SW846 - 8270SW846- 8270SW846- 8270( 24-88 )( 21-142)( 30-103 )( 18-83)(18-109)08/22 /99 08/24/9908 / 22/99 08/24/9908/22 /99 08/24/9908 / 22/99 08/24/9908 / 22/99 08/24/99SurrogatesPhenol - d6 Terphenyl - d14 ?- Fluorobiphenyl 2-Fluorophenol Nitrobenzene -d5 7012574 .663 .470 .7XXXPCB's by GC ECDAroclor-1016ArocLor-1221Aroclor-1232Aroclor-1242Aroclor-12480 .00329 U0 .00329 U0 .00329 U0 .00329 U0 .00329 UAroclor - 12540 .00329 UAroclor-12600 .00329 U0 .003290 .003290 .00329mg/Kgmg/KgSW846 8082SW846 8082SW846 808208/20 / 99 08/22/99 WAA08/20/99 08/22/99 WAA08/20 / 99 08/22/99 WAASW846 8082SW846 808208/20/99 08/22/99 WAA08/20/99 08 / 22/99 WAA0 .003290 .00329mg/Kgmg/Kgmg/Kg0 .00329mg/KgSW846 808208/20/ 99 08 / 22/99 WAAmg/KgSW846 808208/20/99 08 / 22/99 WAAXSW846 8082mg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20 /99 08/ 25/99 LZ08/20 /99 08/ 25/99 LZ08/20 / 99 08/25/99 LZSW846-8081A08/20 / 99 08/25/99 LZSW646-8081ASW846-8081A08/20 / 99 08/25/99 LZ0 .00329SurrogatesDecachlorobiphenyl 94 .3( 53 .3-125 ) 08/20/99 08/22/99PesticidesaLpha-SHCbeta-BHCgamma- Chlordanealpha- Chlordanegamma-BHC ( Lindane)delta-BHC.eptachlor0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .0003290 .0003290 .0003290 .0003290 .0003290 .0003290 .000329mg/Kgmg/Kgmg/Kgmg/Kg08/20 / 99 08/25/99 LZ08/20/99 08/25/99 LZ/~ ~,YCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample ID994255005Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-013-SLClient PO#Printed Date/TimeCollected Date / TimeReceived Date/Time91309/09/99 16 :2808/14/99 11 :4008/18/99 16 :35MatrixSoil/SolidTechnical Director : Stephen C . EdeOrdered ByPWSIDParameterAldrinHeptachlor epoxideEndosulfan 14,4'-DDEDieLdrin' ndrin. ndosulfan II4,4'-DDDEndrin aldehyde4,4'-DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxapheneResults0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .000329 U0 .0329 UAllowableLimitsPrepDateAnalysisDateInitPOLUnitsMethod0 .0003290 .0003290 .000329.0 .0003290 .0003290 .000329mg/Kgmg / Kgmg /Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081A08/20/99 08/ 25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/ 25/99 LZ08/20/99 08/ 25/99 LZ08/20/99 08/ 25/99 LZmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846 - 8081ASW846-8081ASW846-8081ASW846-8081ASW846 - 8081ASW846 - 8081A08/20/ 99 08/25/99 LZ08/20 / 99 08 / 25/99 LZ08/20/ 99 08 / 25/99 LZ08/20/ 99 08 / 25/99 LZ08/20 / 99 08 / 25/99 LZ08/20 / 99 08/25/99 LZmg/Kgmg/KgSW846 - 8081ASW846-8081A%%SW846- 8081ASW846- 8081A0 .0003290 .0003290 .0003290 .0003290 .0003290 .0003290 .0003290 .032908/20 / 99 08/25/99 LZ08/20/99 08 / 25/99 LZ08/20/ 99 08 / 25/99 LZSurrogatesDecachlorobiphenyl < Surr>Tetrachloro- m-xylene 72 .462 .6( 46-154)(25-120)08/20 / 99 08/25/9908/20/ 99 08/25/99CT&E Environmental Services Inc .G4LCCT&E Ref .#994255006ClientPO#91309/10/99 09 :34Oil Spill ConsultantsPrinted Date/TimeClient NameProject Name /# Gambell DACA85-97-D-0010 DO 4 Collected Date/Time 08/14/99 14 :40Received Date /Time08/18/99 16 :35Client Sample ID 99-GAM-014-SLTechnical Director :_*pJieWC . EdeSoil/SolidMatrixOrdered ByPWSIDReleased BySample Remarks :SW7421 GF Metal - MS/MSD recoveries for Pb were outside acceptance criteria ; post digestio'spike was successful .SW7761 GF Metal - MS/MSD recoveries for Ag were outside acceptance criteria ; post digestion spike was successful .8270 - LCS/LCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .8260 - BFB field surrogate recovery (at 65 % vs . 71 %) is biased low . This may be due to matrix interference (biogenicsin the sample) .8270 - Internal standard phenanthrene-d12 is biased low . The samples are non-detect . The results are not affected .GRO/BTEX - Field surrogate recovery is biased low, run twice for confirmation, results may be biased low .SW7041 GF Metal - MS/MSD recoveries for Sb were outside acceptance criteria ; post digestion spike was successful .8081-Detection limit raised 15X due to presence of PCB .)RO/RRO - Pattern consistent with lube oil .DRO - Heavier hydrocarbons contributing to diesel range quantitation .RRO - Surrogate does not meet QC goals due to lube oil pattern . Results not affected .SW7740 GF Metal - MS/MSD recovery for Se was outside acceptance criteria ; bench spike also recovered outside controllimits . Sample concentration was confirmed by the method of standard additions .8270 - Presence of non target analytes requires analysis at a large dilution .AllowableParameterTotal solidsResultsPGL88 .6PrepDateAnalysisDateInitUnitsMethod Limits%SM18 2540G08/24/99 BJSmg/KgSW846 7060SW846 60108SW846 -7131SW846 -719108/24/99 08/30/99 JMO08/26/99 08/31/99 WTA08/24/99 08/25/99 KGF08/24/99 08/25/99 KGFSW846 -7421SW846 -7471SW846 -774008/24/99 08/25/99 KGF08/25/99 08/25/99 RMV08/ 24/99 08/27/99 GCPRCRA MetalsArsenicBariumCadmiumChromiumLeadMercury by Cold Vaporselenium1 .7557 .30 .65913 .22120 .1010 .439 U0 .2204 .420 .2202 .2043 .90 .01710 .439mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg'ILG4CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID913Client PO#09/10/99 09 :34Printed Date/TimeCollected Date/Time 08/14/99 14 :40Received Date/Time 08/18/99 16 :35Technical Director : Stephen C . Ede994255006Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-014-SLSoil/SolidParameterSilverGasoline Range OrganicsResultsPQLUnitsMethodAllowableLimitsPrep AnalysisDate DateInit1 .620 .439mg/Kgsw846 - 776108/ 24/99 08/25/99 KGF2 .99 U2 .99mg/ KgAK101 GR008/14 / 99 08/ 24/99 DARXXAK101 GR0AK101 GROmg/Kgmg /Kgmg/Kgmg /Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 8260sw846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260Surrogates4-Bromofluorobenzene !1,4-Difluorobenzene < Surr>37 .291 .7( 50-150)(50-150)08/14/99 08/24/9908/14/99 08/24/99VOA by GC/MS Method SW8260DichlorodifluoromethaneChloromethaneVinyl chlorideBromomethaneChloroethaneTrichtorofluoromethane1,1-DichloroetheneCarbon disulfideMethytene chloridetrans-1,2 - Dichloroethene1,1-DichLoroethane2-Butanone ( MEK)2,2-Dichloropropanecis-1,2 - DichloroetheneBromochloromethaneChloroform1,1,1-Trichloroethanec arbon tetrachlorideI,1-Dichloropropene0 .030 U0 .030 U0 .030 U0 .30 U0 .30 U0 .030 U0 .030 U0 .30 U0 .15 U0 .030 U0 .030 U0 .30 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .0300 .0300 .0300 .300 .300 .0300 .0300 .300 .150 .0300 .0300 .300 .0300 .0300 .0300 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg / KgSW846 - 8260SW846-8260SW846- 8260SW846- 826008/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08/ 14/99 08/ 22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/ 14/99 08/ 22/99 DRS08 / 14/99 08/ 22/99 ORS08 / 14/99 08 / 22/99 DRS08 / 14/99 08 / 22/99 DRS08 / 14/99 08/22/99 DRS1LCT&E Environmental Services Inc .ACT&E Ref .#994255006Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-014-SLMatrixOrdered ByPWSIDSoil/Solid913Client PO#TimePrinted Date /09/10/99 09 :34Collected Date/Time 08/14/99 14 :40Received Date /Time 08/18/99 16 :35Technical Director : Stephen C . EdeAllowableParameterResultsBenzene1,2-DichloroethaneTrichloroethene1,2-DichloropropaneDibromomethaneiromodichloromethane2-ChtoroethyL Vinyl Ethercis-1,3 - Dichloropropene4-Methyl - 2-pentanone ( MIBK)0 .030 U0 .030 U0 .030 U0 .030 UToluenetrans-1,3 - Dichloropropene1,1,2-TrichloroethaneTetrachloroethene1,3-Dichloropropane2-HexanoneDibromochloromethane1,2-DibromoethaneChlorobenzene1,1,1,2-TetrachtoroethaneEthylbenzeneP & M -Xyleneo-XyleneStyreneBromoformIsopropylbenzene ( Cumene )Bromobenzene1,1,2,2-Tetrachtoroethane0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .30 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U1,2,3-Trichloropropanen-Propylbenzene2-Chtorotoluene4-Chtorotoluene1,3,5-Trimethylbenzene0 .030 U0 .030 U0 .030 U0 .30 U0 .030 U0 .30 U0 .030 U0 .030 U0 .030 U0 .030 UPQLUnitsMethod0 .0300 .030mg/Kgmg/Kg0 .030mg/Kg0 .0300 .0300 .030mg/Kgmg/KgSW846-8260SW846 - 8260SW846 - 8260SW846 - 8260mg/Kg0 .30mg/Kg0 .030mg/Kg0 .30mg/Kg0 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kgmg/Kg0 .030mg/Kg0 .30mg/Kg0 .030mg/Kg0 .030mg/Kg0 .030mg/Kg0 .030mg/Kg0 .0300 .030mg/Kgmg/Kg0 .030mg/Kg0 .030mg/Kg0 .030mg/Kg0 .030mg/Kgmg/Kg0 .0300 .0300 .0300 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846-8260SW846- 8260SW846-8260SW846- 8260SW846-8260SW846- 8260SW846- 8260SW846- 8260SW846-8260SW846- 8260SW846- 8260SW846-8260SW846-8260SW846- 8260SW846- 8260SW846- 8260SW846-8260SW846 - 8260SW846 - 8260SW846- 8260SW846- 8260SW846 - 8260SW846- 8260SW846- 8260SW846-8260SW846- 8260SW846-8260LimitsPrepAnalysisDateDate Init08/14/99 08 / 22/99 DRS08 /14/99 08/22/99 DRS08 /14/99 08/22/99 DRS08 /14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08 / 22/99 DRS08/14/99 08 / 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRSL'zCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample ID994255006Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-014-SLClient PO#913Printed Date/Time09/10/99 09 :34Collected Date/Time08 /14/99 14 :40Received Date/Time08/18/99 16 :35MatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParametertert-ButyLbenzene1,2,4-Trimethylbenzenesec-Butylbenzene1,3-Dichlorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butylbenzene1,2-Dibromo-3-chloropropane1,2,4-TrichlorobenzeneHexachlorobutadieneNaphthalene1,2,3-TrichlorobenzenePalResults0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .30 U0 .030 U0 .030 U0 .030 U0 .030 UUnitsMethod0 .030mg/Kg0 .030mg/Kg0 .0300 .0300 .0300 .0300 .0300 .0300 .300 .030mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-82600 .0300 .0300 .030mg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260XXXXSW846-8260SW846-8260SW846-8260SW846-8260mg/Kgmg/KgAK102/103AK102/103XXAK102/103AllowablePrep AnalysisLimitsDate Date Init08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRSSurrogates1,2-Dichloroethane-D4 Dibromofluoromethane Toluene-d8 4-Bromofluorobenzene !1049796 .764 .6(74-123)(80-118)(79-130)(71-141)08/14/99 08/22/9908/14/99 08/22/9908/14/99 08/22/9908/14/99 08/22/99DR0/RRO CombinationDiesel Range Organics84 .0Residual Range Organics GC59210 .717 .708/24/99 08/28/99 MMP08/24/99 08/28/99 MMPSurrogates5a Androstane d-Triacontane !118217AK102/103(50-150)(50-150)08/24/99 08/28/9908/24/99 08/28/99~~ICT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample ID994255006Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-014-SLClient PO#Printed Date/TimeCollected Date / TimeReceived Date /Time91309/10/99 09 :3408/14/99 14 :4008/18/99 16 :35MatrixSoil/SolidTechnical Director : Stephen C . EdeOrdered ByPWSIDAllowableParameterResultsPQLUnitsMethod Limits9 .19 .19 .19 .19 .19 .19 .1mg /Kgmg/Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /KgSW846-8270SW846 - 8270SW846 - 82709 .19 .19 .19 .19 .19 .19 .19 .19 .19 .19 .19 .1469 .19 .19 .118mg /Kgmg /Kgmg/Kgmg /Kgmg /Kgmg /Kgmg/Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg/Kg9 .1189 .19 .19 .1mg /Kgmg/Kgmg /Kgmg /Kgmg/KgPrepDateAnalysisDate InitSemivolatiles by GC/MSN-NitrosodimethylaminePyridine%nilinePhenolBis(2-Chtoroethyl ) ether2-Chlorophenol1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1,2-Dichlorobenzene2-Methylphenol ( o-Cresol )bis(2-chLoroisopropyL)ether3&4-Methylphenol ( p&m-Cresol )N-Nitroso-di - n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-DimethylphenolBenzoic acidBis(2-Chloroethoxy ) methane1,2,4 .-TrichlorobenzeneNaphthalene4-ChLoroanitineHexachlorobutadiene4-Chloro-3 - methylphenol2,4-Dichlorophenol2-MethylnaphthaleneAexachlorocyclopentadiene9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U46 U9 .1 U9 .1 U9 .1 U18 U9 .1 U18 U9 .1 U9 .1 U9 .1 U08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/ 99 08/24/99 LZ08/ 22/99 08/ 24/99 LZ08/ 22/99 08/ 24/99 LZ08/ 22/99 08/ 24/99 LZSW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 827008/22/99 08/ 24/99 LZ08/22/99 08/ 24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08 / 24/99 LZ08/ 22/99 08 / 24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08 / 24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZSW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846-827008/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/ 24/99 LZ08/22/99 08/ 24/99 LZSW846-8270SW846-8270sw846 - 827008/22/99 08/ 24/99 LZ08/22/99 08/ 24/99 LZ08/ 22/99 08/ 24/99 LZLTA ., CT&E Environmental Services Inc .91309/10/99 09 :3408 /14/99 14 :4008/18/99 16 :35CT&E Ref.#Client NameProject Name/#Client Sample ID994255006Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-014-SLClient PO#Printed Date /TimeCollected Date / TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeAllowableParameter2,4,6-Trichlorophenol2,4,5-Trichtorophenol2-Chloronaphthalene2-NitroanilineDimethytphthaLatecenaphthylene2,6-DinitrotoLuene3-NitroaniLineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-DinitrotoLueneDiethylphthalate4-Chlorophenyt - phenyletherFLuorene4-NitroaniLine2-Methyl-4,6 - dinitrophenotN-Nitrosodiphenylamine4-Bromophenyl - phenyletherHexachLorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-butylphthalateFluoranthenePyreneAzobenzeneButylbenzylphthalate3,3-Dichlorobenzidinelenzo ( a)Anthracene,;hryseneResults9 .1 U9 .1 U9 .1 U46 U9 .1 U9 .1 U9 .1 U46 U9 .1 U46 U46 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U46 U9 .1 U9 .1 U9 .1 U46 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U18 U9 .1 U9 .1 UUnitsMethod9 .19 .19 .1469 .19 .19 .146mg/ Kgmg/ Kgmg/Kgmg/ Kgmg/ Kgmg/ Kgmg/ Kgmg/KgSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82709 .146469 .19 .19 .19 .1mg/ Kgmg/Kgmg/ Kgmg/ Kgmg/ Kgmg/ Kgmg /Kgmg/ Kgmg/Kgmg /Kgmg /Kgmg/Kgmg /Kgmg/Kgmg /Kgmg /Kgmg /Kgmg/KgPQL9 .19 .1469 .19 .19 .1469 .19 .19 .19 .19 .19 .19 .1189 .1mg/Kgmg /Kgmg /Kgmg /Kgmg /Kg9 .1mg /KgSW846 - 82705W846-8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270LimitsPrepAnalysisDateDateInit08 / 22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08 /22/99 08 / 24/99 LZ08/22 /99 08 /24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZAMN-ft.,CT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOrdered ByPWSIDCT&E Environmental Services Inc .994255006Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-014-SLSoil/SolidParameterbis(2-Ethylhexyt ) phthatatedi-n-OctylphthatateBenzo[b]FluorantheneBenzo[k]fluorantheneBenzo[a ] pyrene'ndeno[1,2,3 - c,d] pyreneDibenzo[a , hlanthraceneBenzo[g,h,i ] peryleneClient PO#Printed Date / TimeCollected Date/TimeReceived Date /TimeTechnical Director : Stephen C . EdePQLResults91309/10/99 09 :3508 /14/99 14 :4008 /18/99 16 :35UnitsMethodSW846-8270su846 - 8270SW846-8270SW846-8270SW846 - 82709 .1 U9 .1 U9 .1 U9 .1mg/Kg9 .1mg/Kg9 .1mg/Kg9 .1 U9 .1 U9 .1 U9 .1 U9 .1 U9 .1mg/Kg9 .1mg/Kg9 .1mg/Kg9 .1mg/Kg9 .1mg/KgAllowableLimitsPrepDateAnalysisDate Init08/22 /99 08 /24/99 LZ08 / 22/99 08 / 24/99 LZ08 / 22/99 08 / 24/99 LZ08/22 /99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZSW846 - 8270SW846 - 8270SW846 - 827008/22/99 08/24/99 LZSurrogates2,4,6-Tribromophenol < Surr>Phenol-d6 Terphenyl - d14 2-Fluorobiphenyl < Surr>2-Fluorophenol < Surr>Nitrobenzene - d5 46 .346 .611455 .939 .541 .7XXXXXXSW846 - 8270SW846 - 8270SW846-8270mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846-8270SW846 - 8270SW846 - 8270(18-122)( 24-88 )( 21-142)( 30-103)( 18-83)( 18-109)08 / 22/99 08/24/9908/22 /99 08/24/9908/22/99 08/24/9908/22 /99 08/24/9908/22/99 08/24/9908/22/99 08/24/99PCB's by GC ECDArocLor-1016ArocLor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor - 1254Aroclor-12600 .00338 U0 .00338 U0 .00338 U0 .00338 U0 .00338 U0 .00338 U0 .03170 .003380 .003380 .003380 .003380 .003380 .003380 .00338mg/KgSW846 8082SW846 8082SW846 8082XSW846 808208/20/ 99 08/ 22/99 WAA08/20/ 99 08/ 22/99 WAA08/20/99 08/ 22/99 WAA08/20/ 99 08/ 22/99 WAA08/20/99 08/ 22/99 WAA08/20/99 08/ 22/99 WAA08/20/99 08/ 22/99 WAASurrogatesoecachlorobiphenyl 95 .5( 53 .3-125 ) 08/20/ 99 08/22/99,ALL t CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#994255006Oil Spill ConsultantsGanibell DACA85-97-D-0010 DO 4Client Sample ID99-GAM-014-SLClient PO#Printed Date/TimeCollected Date /TimeReceived Date / TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterResultsUnitsMethod0 .005070 .00507mg/Kgmg/KgSW846-8081Amg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgPQL91309/10/99 09 :3508/14/99 14 :4008/18/99 16 :35AllowableLimitsPrepDateAnalysisDate InitPesticidesalpha-BHCbeta-BHCgamma-Chlordane0 .00507 U0 .00507 U0 .00507 Uatpha-Chlordanegamma -BHC (Lindane)deLta-BHCHeptachlorAldrinHeptachlor epoxideEndosuLfan I4,41-DDE0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .005070 .005070 .005070 .005070 .005070 .005070 .005070 .005070 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .00507 U0 .507 U0 .005070 .005070 .005070 .005070 .005070 .005070 .005070 .005070 .005070 .005070 .507DieldrinEndrinEndosulfan II4,4'-DDDEndrin aldehyde4,4'-DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxaphene08/20/99 08/26/99 LZ08/20/99 08/26/99 LZSW846-8081ASW846-8081A08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081Amg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081AXSW846-8081A(46-154)XSW846-8081A(25-120)08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZSurrogatesDecachlorobiphenyL Tetrachloro-m-xytene 707608/20/99 08/26/9908/20/99 08/26/99~1 ~. CT&E Environmental Services Inc .CT&E Ref .#994255007ClientPO#913Client NameOil Spill ConsultantsPrinted Date/Time 09/10/99 09 :35Project Name/# Gambell DACA85-97-D-0010 DO 4 Collected Date/Time 08/14/99 14 :40Client Sample ID 99-GAM-015-SL Received Date/Time 08/18/99 16 :35MatrixSoil/SolidTechnical DirectoprStJepb4h C . EdeOrdered ByPWSIDReleased BySample Remarks :8270 - Internal standard phenanthrene-d12 is biased low . The samples are non-detect . The resifits are not affected .8270 - LCS/LCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .8260 - BFB field surrogate recovery (at 60% vs. 71 %) is biased low . This may be due to matrix interference (biogenicsin the sample) .GRO/BTEX - Field surrogate recovery is biased low, run twice for confirmation, results may be biased low .DRO/RRO - Possible lube oil pattern.DRO - Heavier hydrocarbons contributing to diesel range quantitation .8270 Presence of non target analytes requires analysis at a large dilution .ParameterTotal SolidsResultsPQL88 .0UnitsAllowableMethod LimitsPrepDate%SM18 2540G08/24/99 BJSAnalysisDate InitRCRA MetalsArsenicBariumCadmiumChromiumLeadMercury by Cold VaporSeleniumSilver1 .6066 .71 .5723 .93110 .1150 .4020 .1690 .2104 .590 .083821 .021 .00 .01750 .2100 .0419mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 7060SW846 60108SW846- 7131SW846 -7191SW846 -7421SW846 -7471SW846 -7740SW846 -776108/24/99 08/30/99 JMO08/26/99 08/31/99 WTA08/24/99 08/25/99 KGF08/24/99 08/25/99 KGF08/24/99 08/25/99 KGF08/25/99 08/25/99 RMV08/24/99 08/27/99 GCP08/24/99 08/25/99 KGFGasoline Range Organics2 .95 U2 .95mg/ KgAK101 GRO08/14/99 08/24/99 DARL1,. - CT&E Environmental Services Inc .CT&E Ref .#994255007Client NameOil Spill ConsultantsProject Name /#Client Sample IDMatrixOrdered ByPWSIDGambell DACA85-97-D-0010 DO 499-GAM-015-SLSoil/SolidParameterResultsClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/10/99 09 :3508/14/99 14 :4008/18/99 16 :35Technical Director: Stephen C . EdePQLAllowableLimitsPrepDate( 50-150)( 50-150 )08/14/99 08/24/9908/14/99 08/24/99AnalysisDateInitUnitsMethodXXAK101 GR0SW846-826008/14/99 08/22/99 DRSSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14 / 99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/ 99 08 / 22/99 ORSSurrogates4-Bromofluorobenzene !1,4-Difluorobenzene 27 .394AK101 GR0VOA by GC/ MS Method SW8260DichlorodifluoromethaneChloromethaneVinyl chlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichtoroetheneCarbon disulfideMethylene chloridetrans-1,2 - Dichloroethene1,1-Dichloroethane2-Butanone ( MEK)2,2-Dichloropropanecis-1,2-DichloroetheneBromochloromethaneChloroform1,1,1-TrichloroethaneCarbon tetrachloride1,1-DichloropropeneBenzene1,2-DichloroethaneTrichloroethene',2-Dichloropropane. ibromomethane0 .030 U0 .030 U0 .030 U0 .0300 .0300 .030mg/Kgmg/Kgmg/Kg0 .30 U0 .30 U0 .030 U0 .030 U0 .30 U0 .15 U0 .030 U0 .030 U0 .30mg/Kg0 .30mg/Kg0 .0300 .0300 .300 .150 .0300 .0300 .300 .0300 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .30 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 Umg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0300 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0300 .030mg/Kgmg/KgSW846-8260sW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRSAllrok ~CT&E Environmental Services Inc .CT&E Ref .#994255007Client NameOil Spill ConsultantsProject Name /#Client Sample IDMatrixOrdered ByPWSIDGambell DACA85-97-D-0010 DO 499-GAM-015-SLSoil/SolidClient PO#913Printed Date/Time09/10/99 09 :35Collected Date/Time 08/14/99 14 :40Received Date/Time 08/18/99 16 :35Technical Director : Stephen C . EdeAllowableParameterBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropene4-Methyl-2-pentanone (MIBK)Toluene'raps-1,3-Dichloropropenei,1,2-TrichloroethaneTetrachloroethene1,3-Dichloropropene2-HexanoneDibromochloromethane1,2-DibromoethaneChtorobenzene1,1,1,2-TetrachlaroethaneEthylbenzeneP & t -Xyleneo-XyleneStyreneBromoformIsopropylbenzene (Cumene)Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene2-Chlorototuene4-Chlorotoluene1,3,5-Trimethylbenzenetert-Butylbenzene1,2,4-Trimethylbenzenesec-Butytbenzene1,3-Dichtorobenzene•isopropyltolueneResults0 .030 U0 .30 U0 .030 U0 .30 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 UPQL0 .0300 .300 .0300 .300 .0300 .0300 .0300 .0300 .0300 .300 .0300 .0300 .030UnitsMethodmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .30 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .030 U0 .0300 .0300 .0300 .0300 .0300 .0300 .0300 .0300 .0300 .0300 .030mg/Kg0 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kg0 .030 U0 .030 U0 .030 U0 .030 U0 .0300 .0300 .0300 .030mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846- 8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846- 8260SW846-8260SW846- 8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260LimitsPrepAnalysisDateDate Init08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 /14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 /14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRSL1,.CT&E Environmental Services Inc .CT&E Ref.#994255007Client NameOil Spill ConsultantsProject Name /#Client Sample IDMatrixOrdered ByPWSIDGambell DACA85-97-D-0010 DO 499-GAM-015-SLSoil/SolidParameter1,4-Dichlorobenzene1,2-Dichlorobenzenen-ButyLbenzene1,2-Dibromo - 3-chloropropane1,2,4-TrichlorobenzenelexachlorobutadieneNaphthalene1,2,3-TrichlorobenzeneResults0 .030 U0 .030 U0 .030 U91309/10/99 09 :35Collected Date/Time08/14/99 14 :40Received Date/Time 08/18 /99 16 :35Technical Director : Stephen C . EdePQL0 .030 U0 .030 U0 .030 U0 .30 U0 .030 UClient PO#Printed Date/Time0 .0300 .0300 .0300 .300 .0300 .0300 .0300 .030UnitsMethodmg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 8260SW846- 8260SW846 - 8260mg/Kgmg/Kgmg/Kgmg/Kgmg/KgAllowableLimitsPrep AnalysisDate DateInit08/ 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/ 22/99 DRS08 / 14/99 08/ 22/99 DRS08 / 14/99 08/22/99 DRSSW846-8260SW846-8260SW846 - 8260SW846 - 826008 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRSSurrogates1,2-Dichloroethane - D4 Dibromofluoromethane < surr>Toluene-d8 4-Bromofluorobenzene !10498 .496 .860XXXXSW846 - 8260SW846 - 8260SW846 - 8260SW846-8260(74-123)( 80-118 )( 79-130 )(71-141 )08/14/ 99 08/22/99mg/Kgmg/KgAK102 / 103AK102/103XXAK102/103AK102/ 103SW846-8270SW846- 827008 /22/99 08/24/99 LZ08/22/99 08/24/99 LZSW846- 8270SW846 - 827008/22/99 08/24/99 LZ08/22 / 99 08/24/99 LZ08/14/99 08/22/9908/14 /99 08/22/9908/14 /99 08/22/99DRO/RRO CombinationDiesel Range Organics68 .8Residual Range Organics GC3039 .9116 .408/ 24/99 08/28/99 MMP08/ 24/99 08/28/99 MMPSurrogates5a Androstane d-Triacontane < Surr>109143(50 - 150)(50-150 )08/24/99 08/28/9908/24/99 08/28/99Semivolatites by GC/MSt-N-NitrosodimethylaminePyridine9 .0 U9 .0 U9 .0mg/Kg9 .0mg/KgniLine•,henol9 .0 U9 .0mg/Kg9 .0 U9 .0mg/KgA&. CT&E Environmental Services Inc .CT&E Ref .#994255007Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-015-SLClient PO#Printed Date/TimeCollected Date /TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterBis(2 -Chtoroethyl)ether2-Chtorophenot1,3-Dichlorobenzene1,4-DichtorobenzeneBenzyl alcohol1,2-Dichtorobenzene2-Methylphenot (o-Cresol)bis(2-chloroisopropyt)ether3&4-Methytphenot (p&m-Cresol)N-Nitroso -di-n-propytamineHexachtoroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-DimethylphenolBenzoic acidBis(2 -Chloroethoxy)methane1,2,4-TrichtorobenzeneNaphthalene4-ChtoroanitineHexachtorobutadiene4-Chloro-3-methytphenol2,4-Dichtorophenol2-MethylnaphthateneHexachlorocyctopentadiene2,4,6-Trichtorophenot2,4,5-Trichlorophenol2-Chtoronaphthalene2-NitroaniLineDimethylphthalateacenaphthylene.,6-DinitrototueneResultsPQL9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U46 U9 .0 U9 .0 U9 .0 U18 U9 .0 U18 U9 .0 U9 .0 U9 .0 U9 .0 U91309 /10/99 09 :3508/14/99 14 :4008/18/99 16 :35AllowablePrepAnalysisLimitsDateDateUnitsMethod9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg9 .0mg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ9 .0mg/Kg9 .0mg/Kg9 .0mg/KgSW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 /99 08/24/99 LZ08/22/99 08/24/99 LZ9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg9 .0mg/Kg46mg/Kg9 .0mg/Kg9 .09 .0mg/Kgmg/Kg18mg/Kg9 .0mg/Kg18mg/Kg9 .09 .0mg/Kgmg/Kg9 .0mg/Kg9 .0mg/Kg9 .0 U9 .0 U46 U9 .0 U9 .09 .0mg/Kg469 .0mg/Kgmg/Kgmg/Kg9 .0 U9 .0 U9 .0mg/Kg9 .0mg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270Init08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ:.'AdCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample ID994255007Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-015-SLClient PO#Printed Date / TimeCollected Date/ TimeReceived Date / TimeMatrixSoil/SolidTechnical Director: Stephen C . Ede91309/10/99 09 :3508/14/99 14 :4008 /18/99 16 :35Ordered ByPWSIDParameter3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran1,4-DinitrototueneDiethylphthalate4-Chlorophenyl - phenyletherFluorene4-Nitroanitine2-Methyl - 4,6-dinitrophenolN-Nitrosodiphenylamine4-Bromophenyl - phenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-butylphthalateFluoranthenePyreneAzobenzeneButylbenzylphthalate3,3-DichlorobenzidineBenzo ( a)AnthraceneChrysenebis(2 - Ethylhexyl ) phthalatedi-n-OctylphthatateBenzo[b] FluorantheneBenzo[k ] fluorantheneBenzo[alpyrene' ndeno[1,2,3-c,d] pyrene, ibenzo[a , hlanthracener-ResultsPQL46 U9 .0 U46 U46 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U46 U9 .0 U9 .0 U9 .0 U46 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U18 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U9 .0 U469 .04646UnitsMethodmg/ Kgmg/Kgmg/ KgSW846-8270SW846 - 82709 .09 .09 .09 .09 .0mg / Kgmg /Kgmg/Kgmg /Kgmg /Kgmg /Kg9 .0469 .09 .09 .0mg/Kgmg/Kgmg/ Kgmg/Kgmg/ Kg469 .09 .09 .09 .09 .09 .09 .0189 .09 .09 .0mg / Kgmg / Kgmg/Kgmg/Kgmg/Kgmg/ Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/ Kgmg/Kg9 .09 .09 .09 .09 .0mg /Kgmg /Kgmg / Kgmg / Kgmg/Kg9 .0mg/ KgSW846 - 8270SW846- 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846-8270SW846- 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270 SW846-8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846-8270AllowablePrepAnalysisLimitsDateDateInit08/22/99 08 / 24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/ 24/99 LZ08 /22/99 08/24/99 LZ08 / 22/99 08/ 24/99 LZ08 / 22/99 08/ 24/99 LZ08 / 22/99 08/24/99 L208/ 22/99 08 /24/99 LZ08/ 22/99 08 /24/99 LZ08/ 22/99 08 / 24/99 LZ08/ 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/ 99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22 /99 08 / 24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08 / 24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/ 24/99 LZcCT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994255007Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-015-SLSoil/SolidClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/10/99 09 :3508/14/99 14 :4008/18 /99 16 :35Technical Director : Stephen C . EdeAllowableParameterBenzo[g ,h,i]peryleneResultsPaL9 .0 U9 .0UnitsMethodmg/KgSW846-8270XXXXXX54846-8270mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 8082SW846 808254846 8082SW846 8082SW846 8082X54846 8082S4846-8081ASW846-8081ALimitsPrepDateAnalysisDate Init08/22/99 08/24/99 LZSurrogates2,4,6-TribromophenoL °henol-d6 rerphenyl-d14 2-Fluorobiphenyl 2-Fluorophenot Nitrobenzene-d5 23 .234 .367 .242 .23132SW846-827054846-8270SW846-8270SW846-827054846-8270(18-122)(24-88)(21-142)(30-103)08/22/99 08/24/9908/22/99 08/24/9908/22/99 08/24/9908/22/99 08/24/99(18-83)(18-109)08/22/99 08/24/9908/22/99 08/24/99PCB's by GC ECDAroctor-1016ArocLor-1221Aroclor-1232Aroclor-1242Aroctor-1248Aroclor-1254Aroclor-12600 .00353 U0 .00353 U0 .00353 U0 .00353 U0 .00353 U0 .00353 U0 .01110 .003530 .003530 .003530 .003530 .003530 .003530 .0035308/20/99 08/22/99 WAA08/20/99 08/22/99 WAA08/20/99 08/22/99 4AA08/20/99 08/22/99 WAA08/20/99 08/22/99 WAA08/20/99 08/22/99 WAA08/20/99 08/22/99 WAASurrogatesDecachlorobiphenyl 74 .2(53 .3-125) 08/20/99 08/22/99Pesticidesalpha-BHC0 .00177 U0 .00177mg/Kgbeta-BHCgamma -Chlordanealpha -Chlordanearoma -BHC (Lindane)0 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .001770 .001770 .001770 .00177mg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081A08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZLTL. . CT&E Environmental Services Inc .CT&E Ref .#994255007Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-015-SLSoil/SolidMatrixOrdered ByPWSIDParameterdelta - BHCHeptachlorAldrinHeptachlor epoxideEndosulfan I4,4 1 -DDEJieldrinEndrinEndosulfan II4,4'-DDDEndrin aldehyde4,4 1 -DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxapheneResultsClient PO#Printed Date/TimeCollected Date /TimeReceived Date/Time91309 /10/99 09 :3508 /14/99 14 :4008/18/99 16 :35Technical Director : Stephen C . EdePQL0 .00177 U0 .00177 U0 .00177 U0 .001770 .001770 .001770 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .001770 .001770 .001770 .001770 .001770 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .00177 U0 .001770 .001770 .001770 .001770 .001770 .001770 .001770 .177 U0 .177AllowablePrepAnalysisLimitsDateDateUnitsMethodmg/KgSW846-8081A08/20 /99 08/26/99 LZmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081A08/20 /99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08 /26/99 LZ08/20 / 99 08 /26/99 LZmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20 / 99 08 /26/99 LZ08/20 / 99 08 / 26/99 LZ08/20 / 99 08/26/99 LZ08/20/ 99 08/ 26/99 LZ08/20/99 08/ 26/99 LZ08/20/99 08/ 26/99 LZ08/20 /99 08/ 26/99 LZSW846-8081ASW846-8081ASW846-8081A'SW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20 /99 08/26/99 LZ08/20 /99 08/ 26/99 LZ08/20 / 99 08 / 26/99 LZSW846-8081ASW846-8081ASurrogatesDecachlorobiphenyl < Surr>Tetrachloro - m-xytene 66 .572XXSW846-8081ASW846-8081AInit( 46-154)( 25-120 )08/20/ 99 08/26/9908/20/99 08/26/99Quanterra Environmental Services , Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 1Project Name : Gambell HTW/DebrisProject No : 99-092Analysis : Gasoline Range Organics . Alaska Dept . ofMethod : AK101Prep Meth : AK101 PRField ID : 99-GAM-016-SLDescr/Location : 99-GSample Date : 08/14/99Sample Time : 1420Matrix : SoilBasis : Dry WeightLab Samp 10 : 0640960003SARecd Date : 08/14/99Prep Date : 08/25/99Analysis Date : 08125/99QC Batch : S990825NNotes:AnalyteDet LimitRep LimitNoteGasoline Range Or anics1 .75 .4 PQLSURROGATE AND INTERNAL STANDARD RECOVERIES :4-Bromofluorobenzene50-150 SLSA GNTrifluorotoluene50-150 SLSAGN : Surrogate recovery is outside of control limitsApproved by.Date :Result Units Pvc DiiND MG/KG 1 .040%!92%1 .01,pQuanterra Environmental Services, Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 2Project Name :Project No :Gambell HTW/Debris99-092Diesel Range Organics . Alaska Dept. ofAnalysis :Method : AK102Prep Meth : SW3541Field ID :Descr/Location :Sample Date :Sample Time :Matrix :Basis :99-GAM-016-SL99-G08/14/991420SoilDry WeightLab Samp ID : 0640960001SA08/18/99Rec'd Date :Prep Date : 08124/99Analysis Date: 08/28/99QC Batch : S9908241Notes :AnalyteDet LimitRep LimitDiesel Range Or anics1 .84 .6 PQLSURROGATE AND INTERNAL STANDARD RECOVERIES :o-Terphenyi5 0-150Approved by.Note Result Units Pvc Dil72 MG/KG 1 .0SLSADate :103%1Quanterra Environmental Services, Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 3P rojec t N ame :Gam b ell HTW/D e b ri sProject No :99-092S tate of Al ask a R es id ual R ange HydrocarbonsAnalysis :Method : AK103Prep Meth : SW3541Field ID :Descr/Location :Sample Date :Sample Time:Matrix :Basis :99-GAM-016-SL99-G08/14/991420SoilDry WeightLab Samp ID : 0640960001SARec'd Date :08/18/99Prep Date : 08/24/99Analysis Date : 08/28/99QC Batch : S9908241Notes :AnalyteDet LimitRep LimitNote Result Units Pvc DilResidual Range Or anics1 .911 . PQL27Q MG/KG 1 .0SURROGATE AND INTERNAL STANDARD RECOVERIES :Tricontane50-150 SLSA AZ160%!AZ: Surr . recovery outside of acceptance limits due to matrix interf .Approved by.Date :1 .lQuanterra Environmental Services . Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 4Project Name : Gambell HTW/DebrisProject No : 99 -092Analysis : Organochlonne Pesticides & PCBs as Aroclors bySW8081Method:Prep Meth : SW3541Field 10 : 99-GAM-016-SLDescr/Location : 99-GSample Date : 08/14/99Sample Time: 1420Matrix: SoilBasis : Dry WeightLab Samp ID : 0640960001 SARec' d Date : 08/18/99Prep Date: 08125/99Analysis Date : 09/07/99CC Batch : S9906251Notes:AnaiyteDet LimitRep LimitNoteAldnn0.202.0 POLalpha-BHC0.202.0 POLbeta-BHC0.472.0 POLgamma-BHC (Lindane)0.202 .0 POLdelta-BHC0.202 .0 POL4,4'-DDD0.24.0 POL24,4'-DDE0.202.0 POL4,4'-DDT0.442.0 POL_ Dieldrin0.202.0 POLEndosutfan 10.202.0 POLEndosutfan II0.442 .0 POLEndosulfan sulfate0.212 .0 POLEndrin0.202 .0 POLEndrin aldehyde0.212.0 POLEndrin ketone0.212 .0 PQLHeptachlor0.232.0 POLHeptachlor epoxide0.202 .0 PQLMethoxychlor0.763 .8 POLToxaphene3.077. POLChlordane1 .120 . POLSURROGATE AND INTERNAL STANDARD RECOVERIES :Decachlorobiphenyt10-181 SLSATetrachlorometaxyleneApproved by.23-149 SLSADate :ResultUnitsNDNDNDNDNDNDNDNDNDNO'NDNDNDNDNDNDNDNDNDNDUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUGIKGUG/KGPvc Oil1 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .01 .032%164%1Ouanterra Environmental Services . Anchorage . AKLab Report No . : 064096 Date : 10/04/99Page : 5Project Name :Gambell HTW/DebrisProject No : 99-092Polychlorinated Biphenyls ( PCBs) by GasAnalysis :SW8082Method :Prep Meth : SW3550Field ID :99-GAM -0 16-SL/Location:Descr99-GSample Date :08/14 / 99Sample Time : 1420Matrix :SoilBasis : Dry WeightLab Samp ID : 0640960001 SARec 'd Date :08/18/99Prep Date: 08/25/99Analysis Date : 09/07/99S9908251QC Batch :Notes :AnalyteDet LimitNoteRep LimitPCB-1016 ( Aroclor 1016)0 .00330 .038 POLPCB-1221 ( Aroclor 1221 )0 .00370 .038 POLPCB-1232 ( Aroclor 1232)0 .00800 .038 POLAroclor1242)PCB-1242 (0 .0130 .038 POLPCB-1248 (Aroclor 1248 )0 .00890 .038 POLPCB-1254 ( Aroclor 1254 )0 .00380 .038 POLPCB-1260 ( Aroclor 1260 )0 .00200 .038 POLSURROGATE AND INTERNAL STANDARD RECOVERIES :Decachlorobiphenyi10-181 SLSATetrachlorometaxylene23-149 SLSAApproved by.Date :ResultUnits Pvc OilNDNDNDNDNDNDNDMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KG32%64%1 .01 .01 .01 .01 .01 .01 .0Quanterra Environmental Services . Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 6P roject Name :G ambe ll HTW /DebrisProject No : 99-092Analysis :Volatile Organic Compounds by GC/MSMethod :SW 8260Prep Meth : SW5030Field ID :99-GAM -016-SLDescr/Location : 99-GSample Date :08/14 / 99Sample Time: 1420SoilMatrix :Basis :Dry WeightLab Samp ID :Recd Date :Prep Date :Analysis Date :QC Batch :Notes :AnalyteBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethanen-Butyibenzenesec-Butylbenzene_ tert-ButylbenzeneCarbon tetrachlorideChlorobenzeneDibromochlorom ethaneChloroethaneChloroformChloromethane2-Chlorotoluene4-Chlorotoluene1,2-Dibromo- 3-chloropropane1,2-DibromoethaneDibromomethane1,2-Dichlorobenzene1 .3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluorom ethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2 - Dichloroethenetrans- 1,2-Dichloroethene1 .2-DichloropropaneApproved by.Det LimitRep Limit18.21 .30.25.24 .160.29.21 .18.20.15.21 .87 .15.160 .15.17 .67 .29 .19 .15.15.15 .75 .21 .45.24.18.25.20.150.POL.POL150150. PQLPQL150.150. PQLPQL300..PQL150150. POLPOL150.150. PQL150.PQL150. POL300.PQLPQL150.300.PQLPQL150.150.PQL300. POL. PQL150150. POL150.PQL150. POL150 .PQL300. POL150.PQL150.PQL150. POL75. POL75.PQL150.POL0640960003SA08/14/9908/1419908/26/99S9908261NoteDate :ResultUnitsNDNDNDNDNDNDNDNDNDN13NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDUG/ KGUG/KGUG/KGUG/KGUG/KGUG/KGUG / KGUG / KGUG/ KGUG/KGUG/KGUG/KGUG/KGUG /KGUG/KGUG/KGUG /KGUG/ KGUG / KGUG/KGUG /KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGPvc Dil0 .550 .550.550.550 .550 .550.550.550 .550 .550 .550 .550 .550 .550.550.550 .550 .550 .550.550.550 .550 .550 .550 .550 .550 .550 .550 .550 .55Quanterra Environmental Services , Anchorage, AKLab Report No . : 064096 Date: 10/04/99Page : 7Project ect Name:Project No :Gam belt HTW / Debris99-092Volatile Organic Compounds by GC, M,)Method :SW 8260Prep Meth : SW 5030ID :Descr/Location :Sample Date:Sample Time :Matrix :Basis :99-GAM - 016-SL99-G08/14 /991420SoilDry WeightLab Samp ID : 0640960003SARec' d Date : 08114/9908/14/99Prep Date:Analysis Date: 08/26/99S9908261OC Batch ::NotesAnalyte1,3-Dichloropropane2 .2-Dichloropropane1,1-DichloropropeneEthylbenzeneHexachlorobutadieneIsopropylbenzene4-IsopropyitolueneMethylene chloride_ Naphthalenen-PropylbenzeneStyrene1,1,1,2-Tetrachloroethane1,1,2,2 - TetrachloroethaneTetrachloroetheneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3 .5-TrimethyibenzeneVinyl chlorideo-XyieneAcetoneCarbon disulfide2-Chloroethyl vinyl ether1-ChlorohexaneApproved by.Analysis:Det Limit23 .27.15 .15 .77.15 .20.31 .47.22.16.15 .68.16.15 .52.44.17.15 .15.160.17.18.22.130.15 .130 .22.56 .15 .Rep Limit150 .600 .150 .150 .150 .150 .150.150.150.150.150.150 .150 .150 .150 .150 .150 .150 .150.150.300.150 .150.150.300.NotePOLPOLPQLPQLPQLPOLPOLPOLPOLPQLPQLPQLPQLPQLPQLPQLPQLPOLPOLPQLPQLPOLPQLPQLPQL75 . POL600 . PQL150 . POL600 . PQLPOL150.Date :ResultNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDUnits Pvc DiiUG/KG0 .55UGIKG0 .55UG/KGo.55UG/KG0 .55UG/KGo.55UG/KG0 .55UG/KG0 .55UG/KG0 .55UG/KG0 .55UG/KG0 .55UG/KG0.55UG/KG0.55UG / KG0.55UG/KG0.55UG/KG0 .55UGIKG0 .55UG/KG0 .55UG/KG0 .55UG/KG0 .55UG/KG0 .55UGIKG0 .55UG/KG0 .55UG/KG0 .55UG/KG0.55UG/KG0.55UG/KG0 .55UG/KG0 .55UG/KG0 .55UG/KG0 .55UG/KG0 .55Quanterra Environmental Services . Anchorage . AKLab Report No . : 064096 Date : 10/04/99Page : 8Project Name : Gambell HTW/DebrisAnalysis : Volatile Organic Compounds by GC/MSProject No : 99-092Method : SW8260Prep Meth : SW5030Field 10 : 99-GAM-016-SLDescr/Location : 99-GSample Date: 08/14/99Sample Time : 1420Matrix: SoilBasis : Dry WeightLab Samp ID : 0640960003SARec'd Date : 08/14/99Prep Date: 08/14/99Analysis Date : 08/26/99QC Batch : S9908261Notes :AnalyteDet LimitRep LimitNotecis-1 .3-Dichloropropene15.150 . POLtrans-1,3-Dichloropropene16.150 . POL1,1,2-Trichloro-1,2,2-trifluoroethane15.150 . POL2-Hexanone110.600 . POL2-Butanone150 .600 . POL4-Methyl-2-pentanone95.600 . POLVinyl acetate31 .300 . POLXylenes22.150 . POLm,p-Xylene (Sum of Isomers )30.75 . POLSURROGATE AND INTERNAL STANDARD RECOVERIES :4-Bromofluorobenzene70-130 SLSA GNToluene-d870-130 SLSAResultUnits Pvc DilNDNDNDNDNDNDNDNDNDUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG0.0.0.0.Dibromofiuoromethane70-130SLSA1,2-Dichloroethane-d470-130SLSA106%Approved by :Date :UG/KG144%!101%101%GN : Surrogate recovery is outside of control limitsUG/KG0 .550 .550 .550 .550 .550 .550 .550 .550 .55Quanterra Environmental Services, Anchorage, AKLab Report No . : 064096 Date : 10/04/99Project Name :Project No :Page: 9Gambell HTW/Debris99-092Semivolatile OrganicOrganic CompoundsCompounds by GC/MSGC/MSAnal isis :: SernivolatileMethod : SW8270Prep Meth : SW3541Field ID : 99-GAM-016-SLDescr/Location : 99-GSample Date: 08/14/99Sample Time : 1420Matrix : SoilBasis : Dry WeightAnaiyteAcenaphtheneAcenaphthyieneAnilineAnthraceneBenzoic acidBenzo (a)anthraceneBenzo (b)fluoranteneBenzo (k)fluorantheneBenzo (g,h,i)peryieneBenzo (a)pyreneBenzyl alcoholbis-(2-chloroethoxy)methanebis-(2-Chloroethyi) etherbis(2-Chloroisopropyi)etherbis-(2-ethyihexyi)phthalate4-Bromophenyi phenyl etherBenzyi butyl phthalate4-Chioroaniline1-Chloronaphthalene2-Chloronaphthalene4-Chloro-3-methyiphenol2-Chlorophenol4-Chlorophenyl phenyl etherChryseneDibenzo(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,3-Dichlorobenzene1,4-Dichlorobenzene1 .2-DichlorobenzeneApproved by:Lab Samp ID :Recd Date :Prep Date :Analysis Date :QC Batch :Notes :Det Limit610 .710 .700 .580.1200.590.610.620.570.550.920.720.680.790.780.780.850.790.590.520.940.650.540.540.570.560.610.660.580.500.Rep Limit0640960001SA08/18/9908/25/9909/09/99S990825ENote3800. POL3800. POL3800. PQL3800. PQLPQL3800 . POL3800 . POL3800 . POL3800 . PQL3800 . PQL3800 . PQL3800 . PQL3800 . PQL3800 . PQL3800 . PQL3800 . POL3800 . PQL3800. PQL3800. PQL3800. PQL3800. PQL3800. PQL3800. PQL3800. POL3800. PQL3800. PQL3800. PQL3800. PQL3800. PQL3800 . POLDate:ResultUnits Pvc OilNDNDNDNDNDNDNDNONDNDNDNDNDNDNDNDNDNDNDNONDNDNDNDNDNDNDNDNDNDUG/KGUG/KGUG/KGUG/KGUG/KGUGIKGUG/KGUG/KGUGIKGUG/KGUG/KGUG/KGUGIKGUG/KGUG/KGUGIKGUG/KGUGIKGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG101010101010101010101010101010101010101010101010101010101010Quanterra Environmental Services, Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 10Project Name : Gambell HTW/DebrisProject No :99-092Analysis : Semivolatile Organic Compounds by GC/MSMethod : SW 8270Prep Meth : SW3541Feld ID : 99-GAM-016-SLDescr/Location : 99-GSample Date: 08/14/99Sample Time : 1420Matrix : SoilBasis : Dry WeightLab Samp 10 : 0640960001SARecd Date:08/18/9908/25/99Prep Date:Date:09/09/99AnalysisQC Batch : S990825ENotes:Analyte3,3'-Dichlorobenzidine2 .4-DichlorophenolDiethyl phthalate2.4-DimethyiphenolDimethyi phthalate2-Methyl-4,6-dinitrophenol2.4-Dinitrophenol2,4-Dinitrotoluene_ 2,6-DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneindeno(1,2,3-cd)pyreneIsophorone2-Methyinaphthalene2-Methylphenol (o-Cresol)4-Me" phenol (p-Cresol)Naphthalene2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenoln-Nitrosodimethylaminen-NitrosodiphenylamineApproved by.Det Limit8600.960.460.590.540.650.570.690.910.540.520.470.450.1700.540.850.520.680.660.990.1900.620.650 .770.720.590.900.570.1200.920. 'Rep Limit----. PQL3800. PQL3800. PQL3800. POL3800. POLPQL---- . POL3800. POL3800. POL3800. POL3800. POL3800. PQL3800. PQL3800 . PQL---- . POL3800 . PQL3800. POL3800 . POL3800 . POL3800 . POL3800. POL3800 . PQL""'. PQL---- . PQL---- . PQL3800 . POL3800 . POLPQL3800 . PQL3800 . PQLNoteDate :ResultUnitsNDNONDNDNONDNDNDNDNDNDNDNDNDNONDNDNDNDNDNDNONDNDNDNDNDNONDNDUG/KGUG/KGUG/KGUG/KGUGJKGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUGIKGUG/KGUG/KGUG/KGUG/KGPvc oil101010101010101010101010101010101010101010101010101010101010Quanterra Environmental Services . Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 11Project Name :Gambell HTW/DebrisProject No : 99 -0 92Semivolatile Organic Compounds by GC/MSAnalysis :Method :SW8270Prep Meth : SW3541Field ID : 99-GAM-016-SLDescr/Location : 99-GSample Date :08/14/99Sample Time : 1420SoilMatrix :Basis : Dry WeightLab Samp ID : 0640960001SA08/18/99Rec'd Date :08/25/99Prep Date :Analysis Date : 09/09/99OC Batch :S990825ENotes :AnalyteDet LimitRep LimitNoten-Nitrosodi-n-propylamine750 .3800. POLPentachlorophenol800.---- . POLPhenanthrene370.3800 . POL3800 . POLPhenol620.Pyrene760.3800 . POLPOL1,2,4-Trichlorobenzene680.3800 ..POL2,4,5-Trichlorophenol800 .38002,4,6-Trichlorophenol740.3800. POLPOL690.3800._ AzobenzenePOLCarbazole290 .3800.7600. POLPyridine890 .SURROGATE AND INTERNAL STANDARD RECOVERIES:25-159 SLSA AXNitrobenzene -d525-178 SLSA AX2,4,6-TribromophenolResultUnitsNDNDNDNDNDNDNDNDNDNDNDUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG0 .0%!0 .0%!2-Fluorophenol25-132 SLSA AXPhenol-d525-144 SLSA AX0 .0%!0 .0%!2-Fluorobiphenyl25-158 SLSA AX0 .0%!Terpheny!-d1425-166 SLSA AX0 .0%!AX : Sample too dilute to quantify surrogateApproved by.Date:Pvc Oil1010101010101010101010Quanterra Environmental Servica , Anchorage, AKLab Report No . : 064096 Date : 10/04/99Page : 12Project Name :Gambell HTW/Debris RemovaProject No : 99-092Field ID :Descr/Location :99-GAM- 016-SL99-GSample Date: 08/14/99Sample Time : 1420Lab Samp ID : 0640960001 SAAnalyteMercuryApproved by:Detection ReportingLimit Limit0 .02 0.10 POLNote Result0 .12Date :Units DiiMG/KG dw 1 .0PrepMethodMETHODAnalysisMethodSW7471Basis : DryMatrix : SoilAnalysisDate08/24 /990CBatchS990823HBQuanterra Environmental Service‚ , Anchorage, AKPage: 13Lab Report No. : 064096 Date : 10/04/99Project Name :Gambell HTW/Debris RemovaProject No : 99-092Field ID :Descr/Location :99-GAM- 016-SL99-GSample Date : 08/14/99Sample Time : 1420Basis : DryMatrix : SoilLab Samp ID : E9H210161002AnalyteArsenicBariumCadmiumChromiumDetection ReportingLimit Limit0 .92 2 .3 PQL0 .23 4 .6 PQL0.12 1 .2 POL0 .23 2 .3 PQLLead0.46 1 .2 POLSeleniumSilver0 .92 1 .2 PQL0 .23 2 .3 POLApproved by:Units DilMG/KG dw 2.0MG/KG dw 2 .0MG/KG dw 2 .0MG/KG dw 2 .0PrepMethodSW3050BSW3050BSW3050BSW3050BAnalysisMethodSW6010BSW6010BSW6010BSW6010BAnalysisDate08/25/9908/25/9908/25/9908/25 /99197 .MG/KG dw 2 .0SW3050BSW6010B08/25/99 S99082311 .3NDMG/KG dw 2 .0MG/KG dw 2 .0SW3050BSW3050BSW6010BSW6010B08/ 25/9908/25/99Note Result8 .357 .0ND24 .7-Date:QCBatchS9908231S9908231S9908231S9908231S9908231S9908231Quanterra Environmental Service, Anchorage, AKPage: 15Lab Report No. : 064096 Date : 10/04/99Project Name :Gambell HTW/Debris RemovaProject No : 99-092Field ID :Descr/Location :99-GAM- 016-SL99-GSample Date: 08/14/99Sample Time : 1420Lab Samp ID : 0640960001 SAAnalytePercent MoistureApproved by :Detection ReportingLimit LimitNANANote Result13 .Date :Basis : Not FilteredMatrix : SoilUnits DilPrepMethodAnalysisMethodAnalysisDateOCBatchPERCE 1 .0NONED221608/25/99S990824H20Quanterra Environmental Service, Anchorage, AKPage : 16Lab Report No . : 064096 Date : 10/04/99Project Name :Gambell HTW/Debris RemovaProject No : 99-092Field ID :Descr/Location :99-GAM- 016-SL99-GSample Date: 08 / 14/99Sample Time : 1420Lab Samp ID : 0640960003SAAnalytePerce nt MoistureApproved by:Detection ReportingLimit LimitNA NANote Result8.Date :Units DilPERCE 1 .0PrepMethodNONEAnalysisMethodD2216Basis : Not FilteredMatrix: SoilAnalysis QCBatchDate08/25/99 S990824H20L ƒG CT&E Environmental Services Inc .ACT&E Ref.# 994255008Client NameClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeTechnical Director ;,Oil Spill ConsultantsProject Name/# Gambell DACA85-97-D-0010 DO 4Client Sample ID 99-GAM-017-SLMatrix Soil/SolidOrdered ByPWSID91309/09/99 16 :2808/14/99 15 :1508/18/99 16 :35p n . EdeReleased BySample Remarks :8270 - LCS/LCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results f6r these compounds areestimated .8270 - Internal standard phenanthrene-d12 is biased low . The samples are non-detect . The results are not affected .ParameterTotal SolidsUnitsAllowableMethod LimitsXSM18 2540G08/24/99 BJSmg/Kgmg/Kg0 .06990 .2004 .190 .02005 .526 .430 .00873 U0 .200 U0 .0400 U2 .002 .000 .008730 .2000 .0400mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 7060SW846 60108SW846-7131SW846-7191SW846-7421SW846-7471SW846-7740SW846-776108/24/ 99 08 / 30/99 JMO08/26/99 08 / 31/99 WTA08/24/99 08 / 25/99 KGF08/24/99 08 / 25/99 KGF08/24/99 08/ 25/99 KGF08/25 /99 08/ 25/99 RMV08/24 /99 08/ 27/99 GCP08/24 / 99 08/25/99 KGF1 .88 U1 .88mg/KgAK101 GRO08/14/99 08/24/99 DARXXAK101 GRO (50-150 )AK101 GRO (50-150 )08/14/99 08/24/9908/14/99 08/24/99ResultsPpL96 .1PrepAnalysisDateDate InitRCRA MetalsArsenicBariumCadmiumChromiumLeadMercury by Cold VaporSeleniumSilverGasoline Range Organics3 .1310 .0mg/KgSurrogates4-Bromofluorobenzene 1,4-Difluorobenzene 6895 .3,A111FML ICT&E Environmental Services Inc .CT&E Ref.#994255008Client NameOil Spill ConsultantsProject Name/#Gambell DACA85-97-D-0010 DO 4Client Sample IDMatrixOrdered ByPWSID99-GAM-017-SLSoil/SolidParameterResultsClient PO#Printed Date /TimeCollected Date/TimeReceived Date /Time91309/09/99 16 :2808/14/99 15 :1508/18/99 16 :35Technical Director : Stephen C . EdeAllowableMethod LimitsPrepDatemg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-826008/14/ 99 08 / 22/99 DRS08/14/99 08 / 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS0 .0940 .0190 .0190 .190 .0190 .0190 .0190 .0190 .019mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .019mg/Kg0 .019mg/Kg0 .019mg/Kg0 .019mg/Kg0 .0190 .0190 .0190 .019mg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08 /22/99 DRS08/14/99 08/22/99 DRS08/14/99 08 / 22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14 /99 08/ 22/99 DRS08/14 /99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/14 /99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08 / 22/99 DRS08/14/99 08/22/99 DRSSW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/ 99 08/ 22/99 DRS08/14/99 08/22/99 DRSSW846-8260SW846-826008/14/99 08/ 22/99 DRSPOLUnitsAnalysisDateInitVOA by GC/MS Method SW8260DichlorodifluoromethaneChloromethane'inyt chlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneCarbon disulfideMethylene chloridetrans-l,2 - Dichloroethene1,1-Dichloroethane2-Butanone (MEK)2,2-Dichloropropanecis-1,2 - DichloroetheneBromochLoromethaneChloroform1,1,1-TrichloroethaneCarbon tetrachloride1,1-DichtoropropeneBenzene1,2-DichloroethaneTrichloroethene1,2-DichloropropaneDibromomethaneBromodichtoromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropene-Methyl-2- pentanone ( MIBK).,luene0 .019 U0 .019 U0 .0190 .0190 .019 U0 .19 U0 .19 U0 .019 U0 .019 U0 .19 U0 .094 U0 .019 U0 .019 U0 .0190 .190 .190 .0190 .0190 .190 .19 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .19 U0 .019 U0 .19 U0 .019 U0 .190 .0190 .190 .019mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRSILME Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample ID994255008Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-017-SLClient PO#Printed Date/TimeCollected Date /TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParametertrans - 1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroethene1,3-Dichloropropane2-Hexanonelibromochtoromethane1,2-DibromoethaneChlorobenzene1,1,1,2-TetrachloroethaneEthylbenzeneP & M -Xyleneo-XyleneStyreneBromoformIsopropylbenzene ( Cumene )Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene2-Chtorotoluene4-Chtorotoluene1,3,5-Trimethylbenzenetert-Butylbenzene1,2,4-Trimethylbenzenesec-Butytbenzene1,3-Dichlorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-DichLorobenzenen-Butytbenzene1,2-Dibromo - 3-chloropropane,2,4-TrichlorobenzeneResultsPOLUnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 8260SW846- 8260SW846- 8260SW846-8260SW846- 8260SW846 - 82600 .019 U0 .019 U0 .019 U0 .019 U0 .19 U0 .019 U0 .019 U0 .019 U0 .0190 .0190 .0190 .0190 .190 .0190 .0190 .0190 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .0190 .0190 .0190 .019mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0190 .019mg/Kgmg/Kg0 .019mg/Kg0 .019 U0 .019 U0 .019 U0 .0190 .019mg/Kgmg/Kg0 .019mg/Kg0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .019 U0 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .0190 .019mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846-8260SU846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 82600 .0190 .0190 .190 .019mg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 8260SW846 - 8260SW846 - 82600 .019 U0 .019 U0 .019 U0 .019 U0 .19 U0 .019 USW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 826091309 /09/99 16 :2808 /14/99 15 :1508 /18/99 16 :35AllowableLimitsPrepDateAnalysisDate Init08/ 14/99 08/ 22/99 DRS08/14/99 08 / 22/99 DRS08 / 14/99 08/ 22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08 / 14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/ 22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08 / 14/99 08/22/99 DRS08 / 14/99 08/ 22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/ 22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08 / 22/99 DRS08/14/99 08 / 22/99 DRS08/14/99 08/ 22/99 DRS,ALCT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name/#Client Sample IDMatrixOrdered ByPWSID994255008Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-017-SLSoil/SolidParameterHexachlorobutadieneNaphthalene1,2,3-TrichlorobenzeneResultsClient PO#Printed Date / TimeCollected Date / TimeReceived Date /TimeTechnical Director : Stephen C . EdePOL0 .019 U0 .019 U0 .019 U91309/09/99 16 :2808/14/99 15 :1508/18/99 16 :350 .0190 .0190 .019UnitsMethodmg/KgSW846-8260SW846-8260mg/Kgmg/KgAllowablePrep AnalysisLimitsDate DateInit08/14/99 08 / 22/99 DRS08/14/99 08 / 22/99 DRS08/14 / 99 08 / 22/99 DRSSW846-8260Surrogates1,2-Dichloroethane - D4 DibromofLuoromethane < surr>Toluene - d8 4-Bromofluorobenzene 105101XXSW846-8260SW846 - 826010197XXSW846- 8260SW846- 8260mg/Kgmg/KgAK102 / 103AK102 / 103XXAK102/103AK102/103mg/Kgmg/Kgmg/KgSW846- 8270SW846-8270SW846 - 8270mg/Kgmg/Kgmg/KgSW846-8270SW846 - 8270SW846 - 8270SW846 - 8270(74-123)(80-118)( 79-130 )(71-141)08/14/99 08/22/9908/14/99 08/22/9908/14/99 08/22/9908 / 14/99 08/22/99DRO/RRO CombinationDiesel Range OrganicsResidual Range Organics GC15 .347 .79 .8816 .308 / 24/99 08/28/99 MMP08 / 24/99 08/28/99 MMPSurrogates5a Androstane d-Triacontane < Surr>95 .7113( 50-150)( 50-150)08/24/99 08/28/9908/24 /99 08/28/99Semivolatiles by GC/MSN-NitrosodimethytaminePyridineAnilinePhenolBis(2-Chloroethyl ) ether2-Chtorophenot1,3-DichLorobenzene', 4-Dichlorobenzene., enzyl alcohol0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .340 .340 .340 .340 .340 .340 .340 .340 .34mg/Kgmg/Kgmg/KgSW846 - 8270SW846 - 827008 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08/24/99 LZAILCT&E Environmental Services Inc .CT&E Ref .#994255008Client NameOil Spill ConsultantsProject Namel#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-017-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . Ede91309 /09/99 16 :2808 /14/99 15 :1508/18 /99 16 :35AllowableParameter1,2-D.ichlorobenzene2-Methylphenol ( o-Cresol)bis(2-chloroisopropyl ) ether3&4-Methylphenol ( p&m-Cresol)N-Nitroso - di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-DimethytphenolBenzoic acidBis(2 - Chloroethoxy ) methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanitineHexachLorobutadiene4-Chloro-3- methylphenol2,4-Dichlorophenol2-MethylnaphthaleneHexachlorocyctopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthyLene2,6-Dinitrototuene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-Nitrophenol+ibenzofuranRe su lt sPOLUnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82700 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .340 .340 .340 .340 .340 .340 .34 U0 .34 U0 .34 U0 .34 U1 .7 U0 .34 U0 .34 U0 .34 U0 .340 .34mg/Kgmg/Kgmg/Kg0 .34mg/Kg0 .34mg/Kg1 .7mg/Kg0 .34mg/Kg0 .340 .340 .69mg/Kgmg/Kgmg/Kg0 .34 U0 .34mg/Kg0 .69 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U1 .7 U0 .34 U0 .690 .34mg/Kgmg/Kg0 .34mg/Kg0 .340 .340 .34mg/Kgmg/Kgmg/Kg0 .34mg/Kg1 .70 .340 .340 .341 .7mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .34mg/Kg1 .71 .70 .34mg/Kgmg/Kg0 .69 U0 .34 U0 .34 U1 .7 U0 .34 U1 .7 U1 .7 U0 .34 Umg/KgSW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846- 8270SW846- 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270LimitsPrepAnalysisDateDateInit08/ 22/99 08/24/99 LZ08/22/ 99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08 / 24/99 LZ08/22/99 08 / 24/99 LZ08 /22/99 08/ 24/99 LZ08 / 22/99 08/ 24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 / 99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08 /24/99 LZ08/ 22/99 08 / 24/99 LZ08/22/ 99 08 / 24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 /99 08/ 24/99 LZ08/22 /99 08/ 24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZA&fCT&E Environmental Services Inc .CT&E Ref .#994255008Client PO#913Client NameProject Name/#Client Sample IDOil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-017- SLPrinted Date/TimeCollected Date/TimeReceived Date/Time09/09/99 16 :2808 /14/99 15 :1508 /18/99 16 :35MatrixSoil /SolidTechnical Director: Stephen C . EdeOrdered ByPWSIDParameter2,4-DinitrototueneDiethylphthalate4-Chlorophenyl - phenyletherFluorene4-Nitroaniline2-Methyl - 4,6-dinitrophenotN-Nitrosodiphenylamine4-Bromophenyl - phenyletherHexachtorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-butylphthalateFluoranthenePyreneAzobenzeneButylbenzytphthalate3,3-DichlorobenzidineBenzo ( a)AnthraceneChrysenebis(2-Ethylhexyl ) phthalatedi-n-OctytphthalateBenzo[b]FluorantheneBenzo[k]fluorantheneBenzo[a ] pyreneIndeno[1,2,3 - c,d] pyreneDibenzo[a , hlanthraceneBenzo[g , h,ilperyleneResultsUnitsMethod0 .340 .340 .340 .340 .341 .70 .34mg /Kgmg /Kgmg /Kgmg/Kgmg /Kgmg / Kgmg/Kg0 .340 .341 .70 .340 .340 .34mg / Kgmg / Kgmg / Kgmg / Kgmg / Kgmg/ KgSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82700 .34 U0 .34 U0 .34 U0 .34 U0 .69 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .34 U0 .340 .340 .340 .340 .690 .340 .340 .340 .340 .340 .340 .34mg/ Kgmg/Kgmg/ Kgmg/Kgmg/Kgmg/ Kgmg/ Kg0 .34 U0 .34 U0 .34 U0 .340 .340 .340 .34 U0 .34 U0 .34 U0 .34 U0 .34 U1 .7 U0 .34 U0 .34 U0 .34 U1 .7 U0 .34 U0 .34 U0 .34 UPOLmg/Kgmg/ Kgmg/ Kgmg / Kgmg /Kgmg /Kgmg /Kgmg /KgAllowablePrepAnalysisLimitsDateDate08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/ 99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/ 24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZSW846 - 8270SW846- 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SurrogatesL,4,6-Tribromophenot < Surr>61 .3%sW846-8270Init( 18-122 )08/22 / 99 08/24/99'AILL ~CT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample ID994255008Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-017-SLClient PO#Printed Date/ TimeCollected Date / TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterPQLResultsUnitsMethodXXXXXSW846-8270SW846-8270mg/Kgmg/Kgmg/Kgmg/KgSW846 8082SW846 808291309/09/99 16 :2808/14/99 15 :1508/18 /99 16 :35AllowableLimitsPrepDateAnalysis(24-88)(21-142)(30-103)(18-83)(18-109)08/22/99 08/24/9908/22/99 08/24/9908/22/99 08/24/9908/22/99 08/24/9908/22/99 08/24/99Date InitSurrogatesPhenol-d6 56 .2Terphenyl-d14 ?-FLuorobiphenyl 2-Fluorophenol Nitrobenzene-d5 92 .760 .349 .656 .3SW846-8270SW846-8270SW846-8270PCB's by GC ECDArocLor-1016Aroclor-1221Aroclor-1232ArocLor-1242Aroclor-1248ArocLor-1254Aroclor-12600 .00325 U0 .00325 U0 .00325 U0 .00325 U0 .00325 U0 .00325 U0 .00325 U0 .003250 .003250 .003250 .003250 .003250 .003250 .00325mg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846 8082XSW846 8082mg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAASurrogatesDecachlorobiphenyl 102(53 .3-125) 08/20/99 08/23/99Pesticidesalpha-BHCbeta-BHCgamma -Chlordanealpha-Chlordanegamma-BHC (Lindane)delta-BHCieptachlor0 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .0003250 .0003250 .0003250 .0003250 .000325mg/Kgmg/Kgmg/Kgmg/Kg0 .0003250 .000325mg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081A08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZCT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994255008Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-017- SLClient PO#Printed Date/TimeCollected Date/ TimeReceived Date/TimeMatrixSoil/SolidTechnical Director: Stephen C . Ede91309 /09/99 16 :2908 /14/99 15 :1508 /18/99 16 :35Ordered ByPWSIDParameterAldrinHeptachlor epoxideEndosulfan 14,4'-DDEDieldrin-ndrinEndosulfan II4,4'-DDDEndrin atdehyde4,4'-DDTEndosulfan sulfateEndrin ketoneMethoxychtorToxapheneResultsPOL0 .000325 U0 .000325 U0 .0003250 .0003250 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .000325 U0 .0003250 .0003250 .0003250 .0003250 .0003250 .000325 U0 .0003580 .000325 U0 .000325 U0 .000325 U0 .0325 U0 .0003250 .0003250 .0003250 .0003250 .0003250 .0003250 .0325UnitsMethodmg/KgSW846-8081ASW846 - 8081Amg/ Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg /Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/ Kgmg/KgAllowablePrepAnalysisLimitsDateDate Init08/20 / 99 08/25/99 LZ08/20 / 99 08 / 25/99 LZ08/20 / 99 08/25/99 LZ08/20/99 08/ 25/99 LZ08/20/ 99 08/ 25/99 LZSW846-8081ASW846-8081ASW846-8081ASW846 - 8081ASW846-8081A08/20/99 08/ 25/99 LZ08/20/99 08/ 25/99 LZ08/20/99 08/ 25/99 LZ08 / 20/99 08/25/99 LZSW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081ASW846- 8081A08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20 /99 08/ 25/99 LZ08/20 /99 08/25/99 LZ08/20/99 08/25/99 L2SW846 - 8081ASW846- 8081ASurrogatesDecachlorobiphenyl < Surr>Tetrachloro -m-xylene < Surr>70 .468%%SW846- 8081ASW846 - 8081A( 46-154 )( 25-120 )08/20/ 99 08/25/9908/20/ 99 08/25/99AL.CT&E Environmental Services Inc .CT&E ReI .IClient NameProject Name/IClient Sample IDMatrixOrdered ByPWSID913Client POI09 /10/99 09 :35Printed Date/TimeCollected Date/Time 08 /14/99 15 :30Received Date/Time 08/18/99 16 :35Technical Dlrectorr8fe)he 9` Ede994255009Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-0 18-SLSoil/SolidReleased BySample Remarks:8270 - LCSILCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results fof these compounds areestimated.8270 - Internal standards phenanthrene -d 12 are biased low . The result of benzo[b]fluoranthene may bias high .8082- Detection limit raised 10X due to matrix interference .8081 /8082 - Surrogate recovery does not meet QC goals due to matrix interference .8081 -Detection limit raised 200X due to matrix interference .DRO - Pattern consistent with highly weathered middle distillate .DRO - Heavier hydrocarbons contributing to diesel range quantitation.nRO/RRO - Surrogate recoveries outside controls due to matrix interference .'0 - Presence of non target analytes requires analysis at a large dilution .ParameterTotal SolidsResultsPCL93 .5AllowableLimitsPrepDateAnalysisDateInitUnitsMethod%SM18 2540G08/24/99 BJSme/Kgmg/K9mg/K9me/KeSWO46 7060511846 60106SY846-7131mp/Kgmg/K0mg/Kgmg/KgSV846-7421SY846-7671SY846-774008/24 /99 08 /30/99 JMO08/26/99 08/31/99 WTA08/24/99 08/ 25/99 KGF08/24/99 08/25/99 KGF08/24/99 08/25/99 KGFRCRA MetalsArsenicBariumCadmiumChromiumLeadMercury by Cold VaporSeleniumSilver3 .0118 .60 .2900 .2223 .790 .022242222 .244 .30 .04450 .4880 .44022 .20 .01340 .2220 .0443SW846-7191S11846-776108/25 /99 08/25/99 RMV08/24/99 08/27/99 GCP08/24/99 08/ 25/99 KGFq1CT&E Envirc :imental Services Inc .CT&E Rd.IClient NameProject Name / #Client Sample IDMatrixOrdered ByPWSIDClient PO/913Printed DaterTlme09/10/99 09 :35Collected Daterrlme 08/14/99 15 :30Received Date/TIme 08/18 199 16 :35Technical Director. Stephen C . Ede994255009Oil Spill ConsultantsGatnbell DACA85-97-D-0010 DO 499-GAM-018-SLSoil/SolidParameter;asoline Range organicsResults2 .66 UPQL2 .66UnitsMethodmg/KgAK101 GROxAK101 GROAK101 GROAllowableLimitsProp AnalysisDate Date Init08/14/99 08/24/99 DARSurrogates4-Bromofluorobenzene < Surr>1,4-Difluorobenzene < Surr>60 .593 .1X( 50-150)( 50-150 )08/14/99 08/24/9908/14/99 08/24/99VOA by GC /MS Method Sv8260Dichlorodiftuoromethane0 .027 U0 .027 me/Kg54846 - 8260ChloromethaneVinyl chloride0 .0270 .02754846 - 826054846 - 8260Methylene chloride0 .027 U0 .027 U0 .27 U0 .27 U0 .027 U0 .027 U0 .27 U0 .13 Utrans - 1,2-Dichloroethene0 .027 U1,1-Dichloroethane0 .027 U2-Butanone ( MEK)2,2-Dichloropropane0 .27 U0 .027 U0 .027 UBromomethaneChtoroethaneTrichloroftuoromethane1,1-DichloroetheneCarbon disulfidecis-1,2-DichLoroetheneBromochloromethane0 .027 UChloroform0 .027 U1,1,1-Trichloroethane0 .027 UCarbon tetrachloride1,1-DichloropropeneBenzene0 .027 U0 .027 U0 .027 U0 .27mg/Kgmg/Kgmg/Kgmg/Kg08/14/99 08/22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 ORSS4846 - 826008/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/14/99 08/ 22/99 DRS08/ 14/99 08 / 22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08/22/99 DRSmg/Kg54846 - 8260S4846- 82600 .027me/Kg54846- 82600 .270 .130 .0270 .027mg/Kgmg/Kgmg/Kgmg/KgS4846-8260S4846 - 82600 .27 mg/Kg0 .027 mg/Kg54846 - 826051846 - 826054846 - 826008/14/99 08/22/99 ORS08/14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/ 14/99 08/22/99 DRS08/14 /99 08/22/99 DRS54846-826008/14 / 99 08/ 22/99 DRSSH846 - 826054846- 8260S4846- 826054846- 826054846- 826008/14 /99 08/22/99 DRS08/14 /99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS0 .270 .0270 .0270 .027mg/Kgmg/Kg0 .0270 .0270 .0270 .027mg/Kgmg/Kgmg/Kgmg/Kg0 .027mg/Kg54846 - 8260SW846 - 826092CT&E Environmental Services Inc .CT&E Ret./Client NameProject Name/#Client Sample IDMatri xOrdered ByPWSIDClient P00913Printed DateiIime09/10/99 09:35Collected Date/Time 08/14199 15 :30Received Date/I7me 08/18/99 16 :35Technical Director: Stephen C . Ede994255009Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-018-SLSoil/SolidAllocablePer a.e ter1,2-DichloroethaneTrichtoroethene1,2-Dichtoropropeneibraso.ethane.rosodichloramethaneResults0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U2-chloroethyl Vinyl Ether0 .27 Ucis-1,3 - Dichloropropene4-Methyl - 2-pentanone ( MIBK)Toluenetrans - 1,3-Dichtoropropene0 .027 U0 .27 U0 .027 U0 .027 U0 .027 U1,1,2-TrichloroetheneTetrachloroethene1,3-Dichloropropane2-NexanoneDibromochloromethane1,2-DibroawethaneChtorobenzene1,1,1,2-TetrachtoroethaneEthytbenzeneP & M -Xyleneo-XyteneStyreneBranafor.Isopropyl benzene ( Cu.ene )Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichtoropropenen-Propylbenzene?-Chlorototuene-Chlorototuene1,3,5-Trimethylbenzenetert - Butylbenzene0 .027 U0 .027 U0 .27 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 UUnitsPOL0 .027 .e/KS0 .0270 .0270 .0270 .0270 .270 .0270 .270 .0270 .0270 .0270 .0270 .0270 .270 .0270 .0270 .0270 .0270 .0270 .0270 .0270 .0270 .027 U0 .0270 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .0270 .027 U0 .027 U0 .027 U0 .0270 .0270 .027.e/Ka.e/KgmeAsme/Kgmg/Keme/Kgmp/Kgme/Kgme/Keme/Ksme/Kgme/Kg•e/Keme/Kg. e/Kgme/Kgmg/Kgma/K9me/Kgme/Kgme/Kgme/Kgmg/Keme/K9me/Kgme/Kg0 .027 me/Kg0 .0270 .0270 .0270 .027me/Kgme/K9.e/Kgme/K9MethodLimitsPrepDateAnalysisDateInitSWO46- d2b0SY846-826008/14/99 08/22/99 DRSSY846 - 8260SY846 - 8260SW646 - 6260Si846 - 826008/14 /99 08/22/99 DRSSv846 - 8260S1d846-826OSY846-8260SY846- 8260SY846 - 8260S11846 - 8260SW646 - 8260SW846 - 8260Sti846 - 8260SWO46 - 8260SWO46- 8260SS846- 8260SW646- 8260SW646 - 8260S1d846-8260S%846 - 826008/14/99 08/22/99 DRS08/14/99 08/22/99 ORS08/14/99 08 / 22/99 ORS08/14/99 08/22/99 DRS08/14/99 08/22/99 ORS08/14/99 08/22/99 DRS08 / 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/ 22/99 ORS08/14/99 08/22/99 DRS08/14/99 08 / 22/99 DRS08/ 14/99 08/22/99 DRS08/14/99 08/22/99 DRS08/14 /99 08 / 22/99 DRS08/14/99 08/22/99 DRS08/ 14/99 08/22/99 ORS08/14/99 08/ 22/99 DRS08/14/99 08/22/99 DRS08/14/99 08/22/99 ORSSi. 46 - 826O08/14/99 08/22/99 ORSS4846-8260SW846-8260SW846 - 826008/14/99 08/22/99 ORS08/14/99 08/ 22/99 ORS08/ 14/99 08/ 22/99 DRS08/ 14/99 08/ 22/99 ORSS'846 - 8260SW546-826OSY846- 8260Sta846- 826OSS1846 - 8260SY846 - 826008/14/99 08/22/99 ORS08/14 / 99 08 / 22/99 DRS08/14/99 08/22/99 ORS08/14/99 08/22/99 DRS08/14/99 08/22/99 DRSQ2CT&E Environmental Services Inc .CT&E Ref .JiClient NameProject Name/SClient Sample IDMatri xOrdered ByPWSID913Client POO09/10/99 09 :35Printed Date/TimeCollected Dateffime 08/14/99 15 :30Received Date/IYme 08/18/99 16 :35Technical Director: Stephen C . Ede994255009Oil Spill ConsultantsGambeU DACA85-97-D-0010 DO 499-GAM-018-SLSoil/SolidResultsParameterPOL0 .027 q-1,2,4-Trimethylbenzenesac-RutytbenzeneI,3-Dichtorobenzene-Isopropyltotuenei,4-Dichlorobenzene0 . 027 U0 .027 U0 .03960 .027 U0 .027 U0 .027 U0 .27 U1, 2-Oichlorobenzenen-Butylbenzene1,2-Dibromo - 3-chtoropropene0 .027 U0 .027 U1 .200 .027 U1,2,4-TrichlorobenzeneNexachlorobutadieneNaphthalene1,2,3-Trichlorobenzens0 .0270 .0270 .0270 .0270 .0270 .0270 .0270 .270 .0270 .0270 .0270 .027AllowableLimitsProp AnalysisDate Date InitUni tsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg514846-8260SW846- 8260SL1846- 8260SY846- 8260SV846- 826008/14/99 08/22/99 DRSmg/Kgmg/Kgmg/Kgmg/Kg514846- 8260514846- 8260514846- 8260514846 - 826008/14/99 08/22/99 DRS08/14/99 08/22/99 DRSmg/Kgmg/Kgmg/Kg514846 - 826008 / 14/99 08/22/99 ORS514846-826051846 - 826008/14/99 08/22/99 DRS08/14/99 08 / 22/99 DRSSW846- 8260SY846- 8260514846- 8260514846 - 826008/14/99 08/22/99 DRS08/14/ 99 08/22/99 DRS08/14 / 99 08/22/99 DR$08/14 /99 08 / 22/99 ORS08/14/99 08/22/99 DRS08/14 /99 08 / 22/99 DRSSurrogates1,2-Dichloroethane - D4 Dibromofluoromethane 105X99 .1xToluene - d8 4-Bromoftuorobenzene 98 .992 .8XX(74-123)( 80-118 )( 79-130 )(71-141)08/14/99 08/22/9908/14/99 08/22/9908/14/99 08/22/9908/14 /99 08/22/99DRO/RRO Canbination1310930Diesel Range OrganicsResidual Range Organics GC49 .782 .1mg/Kgmg/KgAK102/103XXAK102/ 103AK102 /10308/24 /99 09/ 01/99 MMP08/24 /99 09/ 01/99 MMPAK102/103Surrogates5a Androstane d-Triacontane II317312(50 - 150)(50 - 150)08/24/99 09/01/9908/24/99 09/01/9994CT&E Environmental Services Inc .CT&E Rd .rClient NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994255009Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-018-SLSoil/SolidClient Por913Printed DatefTlme09/10/99 09 :35Collected DatelTime 08/14/99 15 :30Received Date/Time 08/18199 16 :35Technical Director: Stepben C . EdeAllowableParaaKterResultsPOLUnitsMethod Limits181818.p/K8mommm/Kg511846 -82701818181818mm/KgrJKOme/Kgm8/Kg"/Kgmg/KgPrepDateAnetysisDateInitSemivotatitee by GC/MS1-NitrosodimethylaminePyridineAnilinePhenolBis(2 -Chloroethyl)ether2-Chlorophenot1,3-Dichtorobenzene1,4-DichtorobenzeneBenzyl alcohol1,2-Dichtorobenzene18 U18 u18 u18 u18 U18 U18 U18 U18 U18 U2-Methytphenol (o-Cresol)18 ubis(2-chtoroisopropyt)ether3i4-Methylphenot (pim-Cresot)N-Nitroso-di-n-propylamineNexachloroetheneMitrobenzeneIsophorone2-Nitrophenol2,4-DimethytphenolBenzoic acidBis(2 -Chtoroethoxy)methane18 U18 U18 U18 U18 u18 U18 U18 u89 U18 U1,2,4-TrichtorobenzeneNaphthatene4-ChtoroanilineNexachtorobutediene4-Chtoro-3-methytphenot18 U18 U36 U18 U2,4-Dichlorophenot2-MethytnaphtheLeneHexachtorocyclopentediene36 u18 U18 U18 USN846-827008/22/99 08/24/99 L208/22/99 08/24/99 L2511846-827008/22/99 08/24/99 L2511846-8270SW546-827008/22/99 08/24/99 L208/22/99 08/24/99 L1SV846-827008/22/99 08/24/99 LZ511846-827008/22199 08/24/99 L2511846-8270Sv846-827008/22/99 08/24/99 L208/22/99 08/24/99 L2m8/Kpma/Kg511846-827008/22/99 08/24/99 LZS'846-827008/22/99 08/24/99 LZWe/KgwJKSmp/Kgmg/Kgmp/Kgmp/KSma/Kgmg/KBSti+846-8270511846-8270551846-827008/22/ 99 08/24/99 L208/22/ 99 08/24/99 LZ08/22/99 08/24/99 L2Si1846-827008/22/99 08/24/99 L2SW646-827008/22 /99 08/24/99 L208/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 LZmm/Kgme/KBma/K9"/KgSW546-8270511846-8270S1r846-8270ma/KgS'846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 L208/22/99 08/24/99 LZ08/22/99 08/24/99 LZSH846-827008/22/99 08/24/99 L21818ft/Kgft/Kgft/KgHp/Kg511846-8270511846-827008/22/99 08/24/99 L208/22/99 08/24/99 LZ511846-827008/22/99 08/24/99 LZ18mp/KgSW846-827008/22/99 08/24/99 LZ181818181818181818181889181818361836511846-8270S1846-8270SW646-8270SH846-827095CT&E Environmental Services Inc .CT&E Ref;rClient NameProject Name /#Client Sample 1DmatrixOrdered ByPWSID994255009Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-018-SLSoU/SoHdParameter2,4,6-Trichloropherwl2,4,5-Trichtorophenol2-Chloronaphthatene2-Nitroanitine.iaathylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran2,4-DinitrototueneDiethylphthslate4-ChIorophenyt-phenylotherFtuorene4-Nitroaniline2-Methyl-4,6-dinitrophenolN-Nitrosodiphenylamine4-Brorphenyt-phenytetherHexachlorobenzenePentachtorophenotPhenanthreneAnthraceneDi-n-butylphthatateFluorantheneResultsClient PO#913Printed DatelTlme09/10/99 09 :35Collected DatetTlme 08/14/99 15 :30Received Datenline 08/18/99 16 :35Technical Director : Stephen C . EdePCL18 U18 u18 U89 U18 U18 U18 U89 U18 u89 U89 U18 u18 u18 u18 U18 U18 u89 U18 U18 U18 U89 u18 U18 U18 U17 .4Pyrene25 .2AzobenzeneButytbenzylphthalate3,3-Dichlorobenzidine18 U18 U36 uBenzo (a)AnthraceneChrysene18 U18 uUnitsAllowableMethod LimitsPrepDate54846-8270SY846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 u08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 Lz181818WWKgme/KIDMR/KO8918181889mp/KpSS846-8270511846-8270mg/Ksag/Ka54046-827054846-8270Mg/KBmg/Kgng/Kp54846-827054846-827054846-8270mg/Kgmg/Kg54846-8270S4846-8270ma/Kgsu846-8270ag/Ksme/Kg54846-8270S4846-827054846-8270S4046-827054846-627054846-827054846-827054846-827054846-8270Sv846-8270i88989181818181818ag/KBa4/Kgme/KB89mg/Kg1818w4/Kgmg/KB18W4/KgW4/Kgmp/Kga4/KBn4/KBmg/Kg891s181818AnalysisDateInit08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 LZ54846-827008/22/99 08/24/99 LZ54846-827054846-8270ag/Kp54646-827054846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ18mg/Kgmg/Kgag/Kgme/KB54646-827054846-827054646-827054646-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ18Mg/Kg54846-827008/22/99 08/24/99 LZ18181836QcAL.CT&E Environmental Services Inc .CT&E Rd.IClient NameProject Name /IClient Sample 1MatrixOrdered ByPWSID994255009Oil Spill ConsultaaqGambell DACA85-97-D-0010 DO 499-GAM-018-SLSoil/SolidResul tsParameterbis(2-Ethylhexyl)phthalatedi-n-Octytphthatate8enzo [b]FLuorantheneBenzo (k)ftuorentheneBenzo (alpyrene18 UAllowableLimitsPrepDateAnalysisDateInitUnitsMethodSW646-827008/22/99 08/24/99 LZS11846-827008/22/99 08/24/99 L208/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 L218Me/KgWWKgme/Kgme/Kgnq/Kgmg/Kg1818mg/Kgmg/Kg511846-8270SW846-8270(18-122)(24-88)(21-142)(30-103)PQL18 U18 U21 .418 U18 U18 U18 UIndeno(1,2,3-c,d] pyreneDibenzo[a,hlanthraceneBenzo[g ,h,i]peryteneClient POO913Printed DatelTime09/10/99 09 :35Collected DatetTlme 08/14/99 15 :30Received Date/ Ttme 08 /18/99 16 :35Technical Director- Stephen C . Ede1818181818SW846-827051846-8270SW646-8270SW646-827008/22/99 08/24/99 L208/22/99 08/24/99 LZ08/22/99 08/24/99 L2Surrogates2,4,6-Tribromophenol 49 .7Phenol-d6 61 .7XXTerphenyl-d14 104XSW646-8270SW846-8270S6846-82702-Ftuorobiphenyt 2-Ftuorophenol Tetrechtoro - m-xylene < Surr>II700200XX511846 - 8081A511846 - 8081A(46-154)( 25-120 )08/20/99 08/26/9908/20/99 08/26/9998A ILCT&E Environmental Services Inc .CT&E Ref.# 994255010Client PO#Client NameOil Spill ConsultantsPrinted Date/Time/#GambellDACA85-97-D-0010DO4CollectedDate/TimeProject NameID99-GAM-019-SLReceivedDate/TimeClient SampleMatrixS011/SolidOr d ered ByPWSID91309/10/99 09 :3508/14/99 15 :4508/18 /99 16 :35e. EdeTechnical Director~,ReleasedS amp l e Remarks :ByA'98270 - Internal standard phenanthrene-d12 is biased low . The samples are non-detect . The results are not affected .8270 - LCS/LCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .8082- Detection limit raised lox due to matrix interference .8081-Detection limit raised 70X due to matrix interference .DRO/RRO - Pattern consistent with lube oil .DRO/RRO - Pattern consistent with weathered middle distillate .DRO/RRO - Surrogate recoveries outside controls due to matrix interference .8270 - Presence of non target analytes requires analysis at a large dilution .AllowableParameterTotal SolidsResultsPQL91 .2LimitsPrepAnalysisDateDate InitUnitsMethod%SM18 2540G08/24/99 BJSRCRA Metals0 .2144 .230 .21421 .421 .40 .01610 .2140 .0428mg/ Kgmg/Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 7060SW846 60108Silver4 .2216 .81 .9131135 .10 .01730 .6680 .0767SW846- 7740SW846- 776108/ 24/99 08/30/99 JMO08/26/ 99 08/31/99 WTA08/ 24/99 08/25/99 KGF08/ 24/99 08/25/99 KGF08/ 24/99 08/25/99 KGF08/ 25/99 08/25/99 RMV08/24/99 08 / 27/99 GCP08/ 24/99 08 / 25/99 KGFGasoline Range Organics2 .85 U2 .85mg/ KgAK101 GRO08/14/99 08/24/99 DARArsenicBariumCadmiumChromiumLeadMercury by Cold VaporseleniumSW846- 7131SW846- 7191SW846- 7421SW846-7471'ILCT&E Environmental Services Inc .91309/10/99 09 :3508/14/99 15 :4508/18/99 16 :35CT&E Ref .#Client NameProject Name /#Client Sample ID994255010Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-019- SLClient PO#Printed Date/TimeCollected Date/ TimeReceived Date / TimeMatrixSoil/SolidTechnical Director : Stephen C . EdeOrdered ByPWSIDParameterResultsPOLAllowablePrepAnalysisDateUnitsMethodLimitsDate%AK101 GROAK101 GRO(50-150)08/14/99 08/24/99(50-150)08/14/99 08/24/99InitSurrogates4-Bromofluorobenzene 1,4-Difluorobenzene 61 .393 .3%VOA by GC/MS Method SW8260DichiorodifluoromethaneChloromethaneVinyl chlorideBromomethaneChloroethaneTrichtorofluoromethane1,1-DichtoroetheneCarbon disulfideMethytene chloridetrans-1,2-DichLoroethene1,1-Dichloroethane2-Butanone (MEK)2,2-Dichloropropanecis-1,2-DichloroetheneBromochLoromethaneChloroform1,1,1-TrichloroethaneCarbon tetrachloride1,1-DichloropropeneBenzene1,2-DichloroethaneTrichLoroethene1,2-DichLoropropaneJibromomethane0 .029 U0 .029 U0 .029 U0 .29 U0 .29 U0 .029 U0 .029 U0 .29 U0 .14 U0 .029 U0 .029 U0 .29 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .0290 .0290 .0290 .29mg/Kgmg/Kgmg/Kgmg/Kg0 .290 .0290 .0290 .290 .140 .0290 .0290 .290 .029mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0290 .0290 .0290 .0290 .0290 .0290 .0290 .0290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260sw846-8260SW846-8260SW846-8260SW846-826008/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 ORS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRSAMk~CT&E Environmental Services Inc .91309/10/99 09 :3508/14/99 15 :4508 /18/99 16 :35CT&E Ref.#Client NameProject Name /#Client Sample ID994255010Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-019-SLClient PO#Printed Date /TimeCollected Date /TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeAllowableParameterBromodichloromethane2-ChloroethyL Vinyl Ethercis-1,3 - DichLoropropene4-Methyl - 2-pentanone ( MISK)Toluenetrans-1,3 - Dichloropropene1,1,2-TrichloroethaneTetrachloroethene1,3-Dichloropropane2-HexanoneDibromochloromethane1,2-DibromoethaneChlorobenzene1,1,1,2-TetrachloroethaneEthylbenzeneP & M -Xyleneo-XyleneStyreneBromoformIsopropylbenzene ( Cumene )Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propytbenzene2-Chlorotoluene4-Chlorotoluene1,3,5-Trimethylbenzenetert-Butylbenzene1,2,4-Trimethylbenzenesec-Butytbenzene1,3-Dichlorobenzene-IsopropyltolueneResults0 .029 U0 .29 U0 .029 U0 .29 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .29 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 U0 .029 UPOLUnitsMethod0 .0290 .290 .0290 .290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-82600 .0290 .0290 .290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0290 .0290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .029mg/Kg0 .0290 .0290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/Kg0 .0290 .0290 .0290 .029mg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260LimitsPrepAnalysisDateDate Init08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/ 25/99 DRS08/14 /99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/ 25/99 DRS08/14 /99 08/ 25/99 DRS08/14 /99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/ 25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/ 25/99 DRSJAIL ~CT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994255010Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-019-SLSoil/SolidParameterResults1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butytbenzene1,2-Dibromo -3-chloropropane1,2,4-Trichlorobenzene' 1exachlorobutadiene0 .029 U0 .029 U0 .029 U0 .29 U0 .029 U0 .029 U0 .029 U0 .029 U4aphthatene1,2,3-TrichlorobenzeneClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/10/99 09 :3508/14/99 15 :4508/18/99 16 :35Technical Director: Stephen C . EdePQL0 .0290 .0290 .0290 .290 .0290 .0290 .0290 .029UnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846- 8260SW846- 8260SW846- 8260SW846 - 8260SW846- 8260mg/Kgmg/Kgmg/KgAllowablePrep AnalysisLimitsDate Date Init08/ 14/99 08/ 25/99 DRS08/14/99 08 / 25/99 DRS08/14/99 08 /25/99 DRS08 /14/99 08/25/99 DRS08 / 14/99 08/ 25/99 DRS08 / 14/99 08/ 25/99 DRS08 / 14/99 08/25/99 DRS08 / 14/99 08/25/99 DRSSW846 - 8260SW846 - 8260Surrogates1,2-Dichloroethane- D4 Dibromofluoromethane 106107Toluene - d8 4-Bromofluorobenzene < Surr>10089 .3XXXXSW846 - 8260mg/Kgmg/KgAK102 / 103AK102 / 103XXAK102/103AK102/ 1038 .4mg/Kg8 .48 .48 .4mg/Kgmg/ Kgmg/ KgSW846 - 8270SW846- 8270SW846 - 8270SW846-8270SW846 - 8260SW846 - 8260SW846-8260(74-123)( 80-118)( 79-130 )( 71-141)08/14 /99 08/25/9908 / 14/99 08/25/9908/14/99 08/25/9908/14/99 08/25/99DRO/RRO CombinationDiesel. Range Organics77810 .5Residual Range Organics GC45017 .308/ 24/99 08/28/99 MMP08/ 24/99 08/28/99 MMPSurrogates5a Androstane !176d-Triacontane !189(50-150 )(50-150 )08/24 /99 08/28/9908/24 /99 08/28/99Semivotatites by GC/MSN-NitrosodimethylaminePyridine8 .4 U8 .4 UAnilinehenol8 .4 U8 .4 U08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZA0-'CT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample ID994255010Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-019-SLClient PO#Printed Date/TimeCollected Date /TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterBis(2 -Chloroethyl)ether2-Chlorophenol1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1,2-Dichlorobenzene2-Methylphenol (o-Cresol)bis(2-chloroisopropyl)ether3&4-Methylphenol (p&m-Cresol)N-Nitroso-di -n-propylamineHexachioroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-DimethylphenotBenzoic acidBis(2 -Chtoroethoxy) methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2,4-Dichlorophenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene,6-Dinitrotoluener_Re s ultsPQLDate08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZmg/Kg8 .4mg/Kg8 .4mg/Kg8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .48 .48 .48 .4mg/Kgmg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4438 .4mg/Kgmg/Kgmg/Kg8 .4mg/Kg8 .4mg/Kg17mg/Kg8 .4 UAnalysisDateSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270mg/Kg8 .48 .4 U43 U8 .4 U8 .4 UPrepLimitsMethod8 .443 U8 .4 U8 .4 U8 .4 U17 U8 .4 U17 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 UAllowableUnits8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U91309 /10/99 09 :3508 /14/99 15 :4508/18/99 16 :35mg/Kgmg/Kg8 .4mg/Kg17mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .48 .48 .443mg/Kgmg/Kgmg/Kgmg/Kg8 .4mg/Kg8 .48 .4mg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270Init08/22/99 08/24/99 LZ08/22 /99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/ 99 08 /24/99 LZ08/22/99 08 /24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 /24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 L208/22/99 08/24/99 LZ08/22/99 08/24/99 LZti.CT&E Environmental Services Inc .CT&E Ref .#994255010Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-019-SLClient PO#Printed Date /TimeCollected Date /TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . Ede91309/10/99 09 :3608/14/99 15 :4508/18/99 16 :35AllowableParameter3-NitroanitineAcenaphthene2,4-DinitrophenoL4-NitrophenolDibenzofuran2,4-DinitrotoLueneiiethylphthatate4-Chtorophenyt - phenytetherFtuorene4-Nitroanitine2-Methyl-4,6 - dinitrophenotN-Nitrosodiphenytamine4-Bromophenyt - phenytetherResultsPOLUnitsMethodSW846 - 8270SW846 - 8270SW846-8270SW846- 8270SW846- 8270SW846-827043 U43mg/Kg8 .4 U43 U43 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4mg/Kg43mg/Kg43mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg43mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg43mg/Kg8 .48 .4mg/Kgmg/KgHexachLorobenzenePentachlorophenolPhenanthrene8 .4 U43 U8 .4 U8 .4 U8 .4 U43 U8 .4 UAnthracene8 .4 UDi-n-butyLphthatateFluoranthenePyreneAzobenzeneButylbenzytphthatate3,3-DichtorobenzidineBenzo ( a)Anthracene8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U17 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .417mg/Kgmg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4mg/Kg8 .4 U8 .4 U8 .4 U8 .4 U8 .4 U8 .4mg/Kg8 .48 .48 .4mg/Kgmg/Kgmg/Kg8 .4mg/KgChrysenebis(2 - Ethythexyl ) phthatatedi-n-OctytphthalateBenzo[b]FtuorantheneBenzo[k ] ftuorantheneBenzo[a ] pyreneIndeno[1,2 , 3-c,d] pyrenebenzo[a , h]anthraceneSW846-8270SW846-8270SW846- 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW646 - 8270SW846 - 8270sw846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270LimitsPrepAnalysisDateDateInit08 /22/99 08/ 24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 / 99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08 /24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08/ 22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 /22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22 / 99 08/24/99 LZ08 /22/99 08/24/99 LZ08/22 / 99 08/24/99 LZ08/22 / 99 08/24/99 LZ08/ 22/99 08/24/99 LZIL!A -CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name/#Client Sample ID994255010Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-019-SLClient PO#Printed Date / TimeCollected Date /TimeReceived Date / TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterBenzo[g , h,i]peryleneResultsPQLUnitsMethodmg/KgSW846-827053 .259 .1XXSW846-8270SW846- 827011571 .248 .7XXXXSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82708 .4 U8 .491309/10/99 09 :3608/14/99 15 :4508/18/99 16 :35AllowableLimitsPrepDateAnalysisDate In it08/22/99 08/ 24/99 LZSurrogates2,4,6-TribromophenoL < Surr>Phenol-d6 erphenyl-d14 < Surr>2-Fluorobiphenyl 2-FLuorophenot < Surr>Nitrobenzene - d5 53 .7( 18-122 )( 24-88 )( 21-142 )(30-103 )(18-83)(18-109 )08/22 / 99 08/24/9908/22/99 08/24/9908/22/ 99 08/24/9908/22/99 08/24/9908/22/99 08/24/9908/22/99 08/24/99PCB's by GC ECDAroclor-1016Aroclor - 1221Aroctor-12320 .0314 U0 .0314 U0 .0314 U0 .03140 .03140 .0314mg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 808208/20/99 08/23/99 WAA08/20/99 08/ 23/99 WAA08/20/99 08/23/99 WAAAroclor-12420 .0314'U0 .0314mg/KgSW846 808208/20 /99 08/23/99 WAAAroclor - 1248Aroctor-1254Aroclor-12600 .0314 U0 .0314 U0 .0314 U0 .03140 .03140 .0314mg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 808208/20 /99 08/23/99 WAAXSW846 8082mg/Kgmg/KgSW846-8081A08/20/ 99 08 / 26/99 LZSW846-8081ASW846-8081ASW846-8081A08/20/99 08/26/99 LZ08/20/99 08/ 26/99 LZ08/20/99 08/ 26/99 LZSW846-8081A08/20/99 08/ 26/99 LZ08/20 /99 08/ 23/99 WAA08/20 /99 08/23/99 WAASurrogatesDecachlorobiphenyl 106(53 .3-125 ) 08/20/ 99 08/23/99Pesticidesalpha-BHCbeta - BHC0 .0110 U0 .0110 Ugamma - Chlordanealpha-Chlordane3mma - BHC (Lindane )0 .0110 U0 .0110 U0 .0110 U0 .01100 .01100 .01100 .01100 .0110mg/Kgmg/Kgmg/KgLTA ., CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name/#Client Sample ID994255010Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-019-SLClient PO#Printed Date/ TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterResultsdelta - BHCHeptachlor0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 UAldrinHeptachlor epoxideEndosuLfan 14,4 1 -DDEiieldrinEndrinEndosulfan II4,4'-DDDEndrin atdehyde4,4'-DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxaphene0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 U0 .0110 U1 .10 UPOLUnitsMethod0 .01100 .01100 .01100 .01100 .01100 .01100 .0110mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081AsW846-8081AsW846-8081A0 .01100 .01100 .01100 .01100 .01100 .0110mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg91309/10/99 09 :3608/14/99 15 :4508/18/99 16 :35AllowableLimits0 .01100 .0110mg/Kgmg/Kgmg/Kg1 .10mg/KgXXSW846 - 8081ASW846- 8081AAnalysisDate Init08/20 /99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20 /99 08/ 26/99 LZ08/20 /99 08/ 26/99 LZ08/20 / 99 08/26/99 LZSU846-8081AsW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A5W846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081APrepDate08/20 /99 08/ 26/99 LZ08/20/99 08/26/99 LZ08/20 /99 08/ 26/99 LZ08/20 / 99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/ 26/99 LZ08/20 / 99 08/26/99 LZ08/20 /99 08/ 26/99 LZ08/20 / 99 08 /26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08 / 26/99 LZSurrogatesDecachtorobiphenyl Tetrachloro - m-xytene 6963(46-154 )( 25-120 )08/20 / 99 08/26/9908/20/ 99 08/26/99CT&E Environmental Services Inc .994282001CT&E Ref .#Client NameOil Spill ConsultantsProject Name/#Gambell DACA85-97-0010 DO 4Client Sample ID99-GAM-020-SLSoil/SolidMatrixOrdered ByPWSIDReleasedClient PO#913Printed Date/Time09 /01/99 15 :10Collected Date/Time 08 /14/99 16 :30Received Date/Time 08 /18/99 16 :35Technical Directoc:.Staphen C . EdeBySample Remarks :8082- Detection limit raised lox due to matrix interference .8270 - CCV recovery for 2,4-dinitrophenol is biased low . The results for this compound are estimated .8270 - LCS/LCSD recovery for pyridine and 3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .8270- Surrogate recovery for nitrobenzene-d5 is biased high possibly due to matrix or/and dilution .8081-Detection limit raised 30X due to matrix interference .GRO/BTEX - Surrogate recovery is biased high due to matrix interference . Results not affected .DRO - Pattern consistent with weathered middle distillate .DRO/RRO - Surrogate recoveries outside controls due to matrix interference .ParameterResultsTotal Solids83 .2Gasoline Range Organics34 .9PQL3 .75AllowableLimitsPrep AnalysisDate Date InitUnitsMethod%SM18 2540G08/24/99 MPAmg/KgAK101 GRO08/14/99 08/27/99 DAR%%AK101 GROAK101 GROmg/KgSW846 - 8260SW846 - 8260SW846 - 826008 / 14/99 08/26/99 DRS08/14/99 08/26/99 DRS08 / 14/99 08/ 26/99 DRSSW846-8260SW846 - 826008/14/99 08 / 26/99 DRS08/14/99 08/26/99 DRSSurrogates4-Bromofluorobenzene !1,4-Difluorobenzene < Surr>16892(50-150 )( 50-150 )08/14/99 08/27/9908/14/99 08/27/99VOA by GC / MS Method SW8260DichtorodifluoromethaneChtoromethaneVinyl chlorideRromomethanehloroethane0 .038 U0 .038 U0 .038 U0 .38 U0 .38 U0 .0380 .0380 .0380 .380 .38mg/Kgmg/Kgmg/Kgmg/Kg'A L CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994282001Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-020-SLSoil/SolidClient PO#Printed Date/TimeCollected Date / TimeReceived Date / Time91309/01/99 15 :1008/14/99 16 :3008/18/99 16 :35Technical Director : Stephen C . EdeAllowableParameterTrichlorafluoromethane1,1-DichloroetheneCarbon disulfideMethytene chloridetrans-1,2-Dichloroethene1,1-DichloroethaneResults0 .038 U0 .038 U0 .38 U0 .19 U0 .038 U0 .038 U2-Butanone (MEK)0 .38 U2,2-Dichloropropane0 .038 Ucis-1,2-DichtoroetheneBromochloromethaneChloroform1,1,1-TrichloroethaneCarbon tetrachloride0 .038 U0 .038 U0 .038 U0 .038 U0 .04960 .038 U0 .038 U1,1-DichloropropeneBenzene1,2-DichloroethaneTrichtoroethene1,2-DichloropropaneDibromomethaneBromodichtoromethane2-chloroethylvinyl ethercis-1,3 - Dichloropropene4-Methyt-2 - pentanone ( MIBK)Toluenetraps - 1,3-Dichloropropene1,1,2-TrichtoroethaneTetrachloroethene1,3-Dichloropropane2-HexanoneDibromochtoromethane2-Dibromoethanelorobenzene0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .38 U0 .038 U0 .38 U0 .038 U0 .038 U0 .038 U0 .038 UPQLUnitsMethod0 .0380 .0380 .38mg/Kgmg/Kgmg/Kg0 .190 .0380 .0380 .380 .0380 .038mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-82600 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .380 .038mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .38mg/Kg0 .0380 .038mg/Kgmg/Kgmg/Kg0 .038 U0 .38 U0 .038 U0 .038 U0 .0380 .0380 .0380 .380 .0380 .0380 .038 U0 .038mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260LimitsPrepAnalysisDateDate Init08/14 / 99 08/ 26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/ 99 08 /26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14 / 99 08 / 26/99 DRS08/14/ 99 08 / 26/99 DRS08/14/99 08/26/99 DRS08/14/ 99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/26/99 DRS~M : CT&E Environmental Services Inc .CT&E Ref.#994282001Client NameOil Spill ConsultantsProject Name /#Client Sample IDMatrixOrdered ByPWSIDGambell DACA85-97-0010 DO 499-GAM-020-SLSoil/SolidParameter1,1,1,2-TetrachloroethaneEthytbenzeneP & M -Xyteneo-XyleneStyreneSromoformIsopropylbenzene ( Cumene )Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene2-Chlorotoluene4-Chlorotoluene1,3,5-Trimethylbenzenetert-Butylbenzene1,2,4-Trimethylbenzenesec-Butylbenzene1,3-Dichlorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butylbenzene1,2-Dibromo-3-chtoropropane1,2,4-TrichlorobenzeneHexachlorobutadieneNaphthalene1,2,3-TrichlorobenzeneResults0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .038 U0 .04810 .04050 .038 U0 .038 U0 .038 U0 .09610 .038 U0 .038 U0 .038 U0 .38 U0 .038 U0 .038 U0 .3820 .038 UClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/01/99 15 :1008 /14/99 16 :3008/18/99 16 :35Technical Director : Stephen C . EdeUnitsMethod0 .0380 .0380 .038mg/Kgmg/Kgmg/Kg0 .0380 .0380 .0380 .038mg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846-8260SW846-82600 .038mg/Kg0 .0380 .0380 .038mg/Kgmg/KgPQL0 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .0380 .038mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .038mg/Kg0 .38mg/Kg0 .0380 .0380 .0380 .038mg/Kgmg/Kgmg/KgAllowableLimitsPrepDateAnalysisDate Init08 /14/99 08/26/99 DRS08/14/99 08 /26/99 DRS08 / 14/99 08 /26/99 DRS08/14/99 08/26/99 DRS08/14/99 08 / 26/99 DRS08 / 14/99 08 /26/99 DRS08/14 / 99 08 / 26/99 DRS08/14 / 99 08 /26/99 DRS08 / 14/99 08/26/99 DRSSW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 826008/ 14/99 08 / 26/99 DRS08 / 14/99 08 /26/99 DRS08/14/99 08 / 26/99 DRS08/ 14/99 08/26/99 DRS08/ 14/99 08/ 26/99 DRSSW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 826008/ 14/99 08/26/99 DRS08/ 14/99 08/26/99 DRS08/14/99 08/26/99 DRS08/14/99 08/ 26/99 DRS08/ 14/99 08/ 26/99 DRS08/ 14/99 08/26/99 DRS08/ 14/99 08/26/99 DRS08/ 14/99 08/26/99 DRS08/ 14/99 08/ 26/99 DRS08/ 14/99 08/ 26/99 DRSmg/KgSW846 - 82605W846 - 8260SW846 - 826008/14/99 08/26/99 DRS08/ 14/99 08/ 26/99 DRS08/14/99 08/ 26/99 DRSXXSW846-8260SW846 - 8260Surrogates', 2-Dichloroethane - D4 ibromofluoromethane < surr>88 .8103(74-123)( 80-118)08/14/99 08/26/9908/14/99 08/26/99IL ACT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample ID994282001Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-020-SLClient PO#Printed Date/TimeCollected Date /TimeReceived Date/Time91309 /01/99 15 :1008/14/99 16 :3008/18/99 16 :35MatrixSoil /SolidTechnical Director: Stephen C . EdeOrdered ByPWSIDParameterResultsAllowablePrep AnalysisUnitsMethodLimitsDate Date%%SW846 - 8260SW846 - 8260( 79-130 )( 71-141)08/14/99 08/26/9908/ 14/99 08/26/99mg/Kgmg /KgAK102/ 103AK102 / 103%%AK102 / 103AK102 / 1039 .49 .49 .49 .49 .49 .49 .49 .4mg/ Kgmg / Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/ Kgmg/ Kg9 .49 .49 .49 .49 .4mg /Kgmg/Kgmg /Kgmg/KgSW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SU846 - 8270SW846-8270SW846 - 82705W846 - 8270POLInitSurrogatesToluene - d8 10877 .84-Bromoftuorobenzene < Surr>DRO/RRO CombinationDiesel Range OrganicsResidual Range Organics GC1390090522937808/24/99 09/ 01/99 MMP08 /24/99 09/01/99 MMPSurrogates5a Androstane d-Triacontane < Surr>!!771357(50-150)(50-150 )08/24 / 99 09/01/9908/24 /99 09/01/99Semivolatiles by GC/MSN-NitrosodimethylaminePyridineAnilinePhenolBis(2-Chloroethyl ) ether2-Chlorophenot1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1,2-Dichtorobenzene9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 Ubis(2-chtoroisopropyl ) ether9 .4 U9 .4 U9 .4 Uz&4-Methylphenol ( p&m-Cresol )-Nitroso-di - n-propylamine9 .4 U9 .4 U2-Methylphenot ( o-Cresol )9 .4mg/Kgmg/KgSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 827008/ 22/99 08/25/99 LZ08/22/ 99 08/ 25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08 / 25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08 / 25/99 LZOR.. y CT&E Environmental Services Inc .CT&E Ref .#994282001Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-020-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . Ede91309/01/99 15 :1008/14/99 16 :3008/18/99 16 :35AllowableParameterHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenotlenzoic acidSis(2-Chloroethoxy ) methane1,2,4-TrichlorobenzeneNaphthalene4-ChtoroanilineHexachlorobutadiene4-Chloro-3 - methylphenol2,4-Dichlorophenol2-MethylnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol2-Chloronaphthalene2-NitroanitineDimethylphthalateAcenaphthylene2,6-Dinitrototuene3-NitroanitineAcenaphthene2,4-Dinitrophenot4-NitrophenolDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chtorophenyl - phenytether7tuorene‚NitroanitineResultsPQLDateSU846 - 8270SW846-8270SW846-8270SW846-827008 / 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22 / 99 08/ 25/99 LZSW846-8270SW846-8270SW846 - 8270SW846-8270SW846 - 827008/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .448mg/Kgmg/Kg9 .4 U9 .4 U9 .4 U19 U9 .4 U9 .4mg/Kg9 .49 .4mg/Kgmg/Kg48 U9 .4 U48 U48 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 UAnalysisDateInitMethod Limits9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U48 U19 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U48 U9 .4 U9 .4 U9 .4 UPrepUnits19mg/Kg9 .4mg/Kg19mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg48mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg48mg/Kg9 .4mg/Kg48mg/Kg489 .49 .49 .4mg/Kgmg/Kgmg/Kgmg/Kg9 .49 .4mg/Kgmg/Kg9 .4mg/KgSW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846- 8270SW846-8270SW846- 8270SW846- 8270SW846- 8270SW846-8270SW846 - 8270SU846- 8270SW846-8270SW846 - 8270SW846-8270SW846 - 8270. SU846 - 8270SW846-8270SW846-8270SW846 - 8270SW846 - 827008/22/99 08/ 25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/ 25/99 LZ08 /22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08 /22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 /22/99 08/25/99 LZCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994282001Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-020-SLSoil/SolidParameter2-Methyl - 4,6-dinitrophenolN-Nitrosodiphenylamine4-Bromophenyl - phenyletherHexachlorobenzenePentachlorophenol'henanthreneAnthraceneDi-n-butylphthalateFluoranthenePyreneAzobenzeneButylbenzylphthalate3,3-DichlorobenzidineBenzo ( a)AnthraceneChrysenebis(2-Ethylhexyl ) phthalatedi-n-OctylphthalateBenzo[b]FluorantheneBenzo[k] fluorantheneBenzo[alpyreneIndeno(1,2 , 3-c,d] pyreneDibenzo[a,hlanthraceneBenzo[g , h,ilperyleneResultsClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/01/99 15 :1008/14/99 16 :3008/18/99 16 :35Technical Director: Stephen C . EdePOLPrepAnalysisLimitsDateDate InitUnitsSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-827008 / 22/99 08/ 25/99 LZSW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 827008 / 22/99 08 /25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZSW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846-8270SW846-8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 827008/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22 / 99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ48 U48mg/Kg9 .4 U9 .4 U9 .4 U48 U9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg48mg/Kg9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4mg/Kg9 .4mg/Kgmg/Kg9 .4mg/Kg9 .4 U19 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4 U9 .4mg/Kg9 .4AllowableMethod9 .4mg/Kg9 .4mg/Kg19mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .49 .49 .4mg/Kgmg/Kgmg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg9 .4mg/Kg08 / 22/99 08 / 25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/ 25/99 LZSurrogates2,4,6-Tribromophenol Phenol - d6 Terphenyt-d14 2-Fluorobiphenyl < Surr>I-Fluorophenol itrobenzene - d5 !55 .359 .796 .778 .947 .1146XXXXXXSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270( 18-122)(24-88 )( 21-142)( 30-103 )SW846 - 8270SW846-8270( 18-83)( 18-109)08 /22/99 08/25/9908/22 /99 08/25/9908 /22/99 08/25/9908/22 /99 08/25/9908/22/99 08/25/9908 / 22/99 08/25/99LTI ƒ CT& E Environmental Services Inc .CT&E Ref .#994282001Client NameOil Spill ConsultantsProject Name/#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-020-SLClient PO#Printed Date/TimeCollected Date/ TimeReceived Date/ TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsPQLUnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 808291309/01/99 15 :1008/14/99 16 :3008/18 /99 16 :35AllowablePrepAnalysisLimitsDateDateInitPCB's by GC ECOAroclor-10160 .0390 UAroclor-1221oroclor-1232Aroctor-1242Aroclor-1248Aroclor-1254Aroclor-12600 .0390 U0 .0390 U0 .0390 U0 .0390 U0 .0390 U0 .0390 U0 .03900 .03900 .03900 .03900 .03900 .03900 .0390mg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846 8082SW846 8082%SW846 80820 .01170 .01170 .01170 .01170 .01170 .01170 .01170 .0117mg/Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846- 8081ASW846- 8081ASW846- 8081ASW846- 8081ASW846- 8081ASW846 - 8081ASW846-8081ASW846- 8081A0 .01170 .01170 .01170 .01170 .0117mg/Kgmg/Kgmg/Kgmg/Kgmg/ Kg0 .01170 .0117mg/KgSW846 - 8081ASW846- 8081ASW846- 8081ASW846 -8081ASW846 - 8081ASW846-8081Amg/KgSW846 - 8081A08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08 /20/99 08/23/99 WAA08 /20/99 08/23/99 WAASurrogatesDecachlorobiphenyl 112(53 .3-125) 08/20/99 08/23/99Pesticidesalpha-BHCbeta-BHCgamma -Chlordanealpha -Chlordanegamma - BHC (Lindane)delta-BHCHeptachlorAldrinHeptachlor epoxideEndosulfan I0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U4,41-DOEDieldrinEndrinEndosulfan II0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U,,4'-DDD0 .0117 U08/20/ 99 08 /26/99 LZ08/20/99 08 /26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/ 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20 / 99 08 /26/99 LZ08 / 20/99 08 /26/99 LZA& ; . CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSIDClient PO#Printed Date/TimeCollected Date/TimeReceived Date /Time994282001Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-020-SLSoil/SolidParameterEndrin aldehyde4,4 1 -DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxapheneResults0 .0117 U0 .0117 U0 .0117 U0 .0117 U0 .0117 U1 .17 U91309 /01/99 15 :1008 /14/99 16 :3008 /18/99 16 :35Technical Director : Stephen C . EdeUnitsMethod0 .0117mg/Kg0 .0117mg/Kg0 .01170 .01170 .01171 .17mg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846 - 8081ASW846-8081ASW846 - 8081ASW846 - 8081APQLAllowableLimitsPrepDateAnalysisDate Init08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZSW846 - 8081ASurrogatesDecachlorobiphenyl < Surr>Tetrachloro - m-xylene < Surr>12259XXSW846 - 8081ASW846- 8081A(46-154).robenzene - d5 l74 .450 .2133XXX77 .335 .7XXX130SW846-8270SW846-8270SW846 - 8270SW846-8270( 18-122)SW846 - 8270SW846-8270(18-83)( 18-109)( 24-88 )( 21-142)( 30-103 )08/ 22/99 08/25/9908/22/ 99 08/25/9908/ 22/99 08/25/9908/22 / 99 08/25/9908 /22/99 08/25/9908 /22/99 08/25/99LILCT&E Environmental Services Inc .CT&E Ref .#994282002Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-021-SLMatrixOrdered ByPWSIDSoil/SolidParameterResultsClient PO#913Printed Date/ Time09/01/99 15 :11Collected Date / Time 08/14/99 16 :30Received Date / Time08/18/99 16 :35Technical Director : Stephen C . EdePQLUnitsMethod0 .03860 .03860 .03860 .03860 .03860 .0386mg/KgSW846 8082SW846 8082sW846 8082SW846 80820 .0386mg/KgSW846 8082SW846 8082SW846 8082XSW846 80820 .0116 U0 .0116 U0 .01160 .01160 .01160 .01160 .01160 .01160 .0116mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0116 U0 .0116 U0 .0116 U0 .0116 U0 .0116 U0 .01160 .01160 .01160 .01160 .0116mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A0 .0116 U0 .0116 U0 .0116 U0 .01160 .01160 .0116mg/Kgmg/Kgmg/KgAllowablePrepAnalysisLimitsDateDate InitPCB's by GC ECDAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-12600 .0386 U0 .0386 U0 .0386 U0 .0386 U0 .0386 U0 .0386 U0 .0386 Umg/Kgmg/Kgmg/Kgmg/Kgmg/Kg08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAASurrogatesDecachtorobiphenyt 61 .6(53 .3-125) 08/20/99 08/23/99Pesticidesalpha-BHCbeta-BHCgamma-Chtordaneatpha-Chlordanegamma -BHC (Lindane)delta-BHCHeptachlorAldrinHeptachlor epoxideEndosulfan I4,4'-DDEDieldrinEndrin-ndosulfan II:'-DDD0 .0116 U0 .0116 U0 .0116 U0 .0116 U0 .0116 USW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZA1,. VCT&E Environmental Services Inc .CT&E Ref .#994282002Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-021-SLSoil/SolidMatrixOrdered ByPWSIDParameterEndrin aldehyde4,4'-DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxapheneResults0 .0116 U0 .0116 U0 .0116 U0 .0116 U0 .0116 U1 .16 UClient PO#913Printed Date/Time09/01/99 15 :11Collected Date/Time 08 /14/99 16 :30Received Date/Time 08/18/99 16 :35Technical Director : Stephen C . EdePOL0 .01160 .01160 .01160 .01160 .01161 .16UnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg541846 - 8081ASW846-8081A541846 - 8081ASW846 - 8081ASW846 - 8081A541846 - 8081AXXSW846 - 8081ASW846 - 8081AAllowablePrepAnalysisLimitsDateDate Init08/20 /99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/ 26/99 LZ08/20 / 99 08/ 26/99 LZ08/20 / 99 08/ 26/99 LZSurrogatesDecachtorobiphenyl Tetrachloro - m-xylene 10759( 46-154)( 25-120 )08/20/ 99 08/26/9908/20/ 99 08/26/990". . CT&E Environmental Services Inc .CT&E Ref.# 994255012Client NameOil Spill ConsultantsProject Name/# Gambell DACA85-97-D-0010 DO 4Client Sample ID 99-GAM-021-SLMatrix Soil/SolidOrdered ByPWSIDClient PO# 913Printed Date/Time 09/09/99 16 :29Collected Date/Time 08/14/99 16 :30Received Date/Time 08/18/99 16 :35Technical Director. tepheiit . EdeSample Remarks :Sample analyzed for Dioxins (SW8290) by Triangle Laboratories of Durham, NC .ParameterResultsPQLUnitsAllowableMethod LimitsPrep AnalysisDate Date Initmg / KgSW846 6010809/02 /99 09/ 03/99 WTA%SM18 2540G08/24/99 BJSMetals by ICPCopper33 .2Total Solids83 .14 .37Metals by Graphite FurnaceAntimony0 .206 U0 .206mg /KgSW846 - 704108/ 24/99 08/27/99 KGF0 .6420 .206mg/KgSW846 706008/ 24/99 08/30/99 JMO0 .09270 .0206mg/KgSW846 - 713108/ 24/99 08/25/99 KGF22 .22 .06mg/KgSW846 - 742108/ 24/99 08/25/99 KGFMetals by Graphite FurnaceArsenicMetals by Graphite FurnaceCadmiumMetals by Graphite FurnaceLeadTLI Project : 49337 Method 8290 PCDDIPCDF Analysis (b)Client Sample : 99 .42 -55-1.2 Client Sample ID : 99-GAM -021-SL Analysis File : U316704Client Project :Sample Matrix :TLI ID :Gambell, AXSOIL244-42-2Date Received : 0812111999Spike File :SPMrr=SDate Extracted : 08/2911999Date Analyzed: 09/11/1999ICal:ConCal :UF58319U993166Sample Size :11.800 g9.9128DB-5Dilution Factor. n/aU315501Blank File:SWAnalyst:% Moisture :% Lipid:% Solids :16.0n/a84.0Dry Weight :GC Column :Azagytm2-3 .7 .X-T('DDI .2.3 .7 .;t-PeCDD1 .2.3 .4.7 .8-HxCDDI .2_ . 3 .6 .7 .8-Hx('DD1 .2 .3 .7,8 .9-HxCDDt ._.3 .4.6 .7 .8-HpCDD1 .2.3 .4.o .7 .8.9-OCDD11 .71 .3-TCDF1 .2 .3 .7 .,`t-PeC:DF2 .3 .4.7,4-PeCDF1 .2 .? .4.7 .8-HxCDFI .2 .3 .6.7 .8-HxC DF1 .4.6.7 .8-HxCDF1 .2A7 .8 .9-HxCDF1 .2 .3 .4 .6.7 .8-HpCDFI .2 .', .4 .7 .8 .)-HpCDF1 '? .4 .6.7 .8 .9-OCDFTotal T('DDTotal Pe('DDTot-,d Hx('DDTot .d HpCDDCot :d T('DFrot :d l\K('DFTotal I Ix('DFTo al IIpCDFCam 8FbWND2 .23 .08 .98 .21518000 .61 .441 .111 .271221 .030 .8434 :2337 :2040:540 .8025 :55B_J_1 .371 .341 .291 .1730:3333:1933:2433 :53JJ1J74 .14 .81 .061 .0837 :494360.9041 :064 .1E.iPC1 .74 .61 .8NDJ_34:050.972.91 .519 .167 .130:5234 :000.536 :181-2.5263177226 .7729 .912.8614.559 .47362420 .3tPage I of 2MM--MR 1 04 . L,AM 6 15Triangl e Laboratories, Inca801 Capitola Drive ‚ Durham , North Carolina 27713ot, - . ra, C~ ce t .c7w ‚ Cix 19191 544- "O!Printed: 03 :50 09/1411999TL[ Project :Client Samp l e :493379 9.4255-12Method 8290 PCDD/PCDF Analysis (b)Analysis File : U316704Client Sample iD : 99-GAM-021-SLb t TW StandardsCOW."C, :-2.3 .7 .8-TCDF11C' :2.? .7 .8-TCDD"C, :-1 .? 3 .7.8-PeCDF"C,--- 1 .? 3 .7.9-PeCDD"C, :-1 .? 3 .6.7,8-HpCDF' C, :-1 .2.3 .6 .7.9-HxC.'DD1 .2 .3 .4 .6.7,8-HpCDF"C, . 1 .'_,3 .4 .6.7 .8-HpCDD161180187180204228294"C, ‚- 1 .? 3 .4.6 .7.8.9-OCDD473"C, :-2.3 .4 .7 .8-PeCDF"C, :- ( . :.3 .4.7 .8-HpCDF"C,, 1 ' .3 .4 .7.9-HxCDD"C . :-1 .2 .3 .4 .7 .9 .9-HpCDF187187,215liro OWyOC i( tft"I m.79.840%-130%0.7389 .192.889 .410110711314611740%-130%0.821 .481 .470 .311 .2225 :5226 :3529:4930:5240%-130%40%-130%40%-130%40%-130%25%-130%25%-130%25%-130%40%-130%23092 .592.9105114'CL-2.3 .7 .9-TODD15 .878 .140%-130%t ' 3 .7 . .&9-HpCDF''C', :-? 2 .4 .6.7 .9-HAMF217Ltd11040%-130%40%-130%2122211 .2.3 .4-T1'OD. :-1 .2.' .7 .9 .9-HxCDDData ReviewerVC/Page 2 Of 240%-130%40%-130%25%-130%0 .441 .180.841 .480.511 .260 .4333:2434 :0436 :1737 :1940 :5330:3133:1834:0037 :4926 :360.510.5134 :3933 :530 .851 .1926 :2434 :2309/1411999Wi. - PSR . , a. i.usa : : 70Triangle Laboratories, inc . .801 Capitola Drive ‚ Durham, North Carolina 27713Phone . (919) 544-5729 ‚ Fax: (919) 544-5491Printed : 03 :50 09/14, 19 c 9TLI Project :Client Sample :Client Project :Sample Matrix :TT-I ID :Sample Size :Dry Weight:GC Column :4933799.4255-12Gambell, AKSOIL244-42-21L800 g9.912 gDB-2252.3 .7 .8-TCDFMethod 8290 TCDD/TCDF Analysis (DB-225)Client Sample ID : 99-GAM -021 -S L Analysis File : P993261Date Received: 08x21/1999Date Extrxted : 08129/1999Date Analyzed: 09/14/1999Spike File :ICal :ConCal :SPCZNFZPF27079Dilution Facra- n/a% Moisture :% Lipid:% Solids :16.0n/a84.0Blank File :P993270AnalystSS0 .92cc17CI :-2.3 .7.8-TCDF253125P9930.7423 :010.7823:00Q_0.8821 :50Q-t„40%-130%M13C, -1 .x .4-TODDDara Reviewer. -KPage 10( 109/17/1999C 2W-M rips L.ARS 616-00Triangle Laboratori es, Inc..801 Capitols Drive ‚ Durham, North Carolina 27713Phone : (919) 544-5729 ‚ Fax: (919 ) 544-5491Printed : 17 :59 09/17/1999Quanterra Environmental Services , Anchorage, AKPage : 14Lab Report No . : 064096 Date : 10/04/99Project Name:Gambell HTW /Debris RemovaProject No : 99-092Field ID :Descr/Location :99-GAM-022-SL99-GSample Date : 08/14/99Sample Time : 1630Basis : DryMatrix : SoilLab Samp ID : E9H21016 1001AnalyteDetection ReportingLimitLimitNoteAntimony0.507 .5POLArsenicCadmiumCopperLead1 .00 .131 .00 .501 .30 .633 .10 .63POLPOLPOLPQLResultNDJ1 .1ND65 .736 .5J: EPA Flag - Estimated valueApproved by :Date:PrepMethodAnalysisMethodAnalysisDateOCBatchMG/KG dw 1 .0SW3050BSW6010B08/25/99S9908231MG/KG dwMG/KG dwMG/KG dwMG/KG dwSW3050BSW3050BSW3050BSW3050BSW6010BSW6010BSW6010BSW6010B08/25/9908/25/9908/25/9908/25/99S9908231S9908231S9908231S9908231UnitsDil1 .01 .01 .01 .0Quanterra Environmental Servicets, Anchorage, AKPage : 17Lab Report No . : 064096 Date : 10/04/99Project Name :Gambell HTW/Debris RemovaProject No : 99-092Field ID :99-GAM - 022-SLSample Date : 08/ 14/99Basis : Not FilteredDescr/Location :99-GSample Time : 1630Lab Samp I D : 0640960002SAMatrix : SoilAnalytePercent MoistureApproved by:Detection ReportingLimit LimitNA NANoteResult20 .Date :Units DilPERCE 1 .0PrepMethodNONEAnalysisMethodD2216AnalysisDate08/25/99OCBatchS990824H20Quanterra Environmental Servicet , Anchorage, AKPage: 18Lab Report No . : 064096 Date : 10/04/99Project Name :Gambell HTW/Debris RemovaProject No : 99-092Field ID :99-GAM - 022-SLSample Date: 08 / 14/99Basis : WetDescr/Location :99-GSample Time : 1630Matrix : SoilLab Samp ID : G9H210185001AnalytePercent MoistureApproved by:Detection ReportingLimit LimitNA NANoteResult17 .1Date:Units DilPERCE ww 1PrepMethodMETHODAnalysisMethodD2216Analysis QCDateBatch09/14/99 9237207Quanterra Environmental Services , Anchorage, AKPage : 19Lab Report No . : 064096 Date: 10/04/99Project Name : Gambell HTW/DebrisAnalysis :PolychlorinatedProject No: 99-092Method :SW8290Prep Meth :METHODField ID : 99-GAM-022-SLLab Samp ID :G9H2101 85001Descr/Location : 99-GRec'd Date :08/21/99Sample Date : 08/14/99Prep Date:08/25/99Sample Time : 1630Matrix : SoilAnalysis Date :QC Batch :09/11/999237207Basis: Dry WeightNotes :AnalyteDet LimitRep Limit2,3,7,8-Tetrachlorodibenzo-p-dioxin0.151 .01,2,3,7,8-Pentachlorodibenzo-p-dioxin1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin0.300.420.612.25.05 .0PQL1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin0.41 .5.01,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin0.305.0Octachlorodibenzo-p-dioxin2,3,7,8-Tetrachlorodibenzofuran1,2,3,7,8-Pentachlorodibenzofuran2 .3,4,7,8-Pentachlorodibenzofuran1 .20.080.300.3710.01 .01 .61 .51,2,3,6,7,8-Hexachlorodibenzoturan1,2,3 .7,8,9-Hexachlorodibenzofuran0 .300.411,2,3,4,7,8-Hexachlorodibenzoturan2,3,4,6,7,8-Hexachlorodibenzoturan1 .2,3 .4,6.7,8-He tachlorodibenzofuranApproved by:NoteResultUnits Ratio FITPOL0.60PG/G0.1POLPOLND12.03.3PG/GPG/GPG/G0.0.0.111POL5.1PG/G0.1POL250.PG/G0.1POLPOLPQLPOL1100 .1 .2NDNDPG/GPG/GPG/GPG/G0.0.0.0.11112 .11 .6POLPOLNDNDPG/GPG/G0.0.110 .350 .422 .91 .8POLPOLNDNDPG/GPG/G0.0.110 .305.0POL96 .0PG/G0.1Date :Pvc DilQuanterra Environmental Services , Anchorage, AKPage : 20Lab Report No . : 064096 Date : 10/04/99Project Name : Gambell HTW/DebrisAnalysis :PolychlorinatedProject No :Method :SW8290Prep Meth:METHOD99 - 092Field ID :99-GAM-022-SLDescr/Location : 99-GSample Date:08/14/99Sample Time : 1630Lab Samp ID :Rec'd Date :Prep Date :Analysis Date:G9H2101 8500108/21/9908/25/9909/11/99Matrix:QC Batch :9237207SoilNotes :Basis : Dry WeightAnalyteDet Limit Rep Limit1,2,3,4,7, 8,9-HeptachlorodibenzofuranOctachlorodibenzofuranNoteResultUnitsRatio RT5.0570.PG/GPG/G0.0.Pvc Dil5.010.0POLPOL40-135SMSATotal He tachlorodibenzo- -dioxins2.501 ATE AND INTERNAL STANDA D RECOVERIES :5.0PQL430.PG/G0.1Total Heptachlorodibenzofurans (HpCDF)2.5r SURROGATE AND INTERNAL STANDARD RECOVERIES :5.0PQL470 .PG/G0.12.5Total Hexachlorodibenzo - dioxinsOI ATE AND INTERNAL STANDA D RECOVERIES :5.0POL68.0PG/G0.1Total Hexachiorodibenzofurans (HxCDF) 1 2.5SURROGATE AND INTERNAL STANDARD RECOVERIES :4 .5Total Pentachlorodibenzo - dioxinSATE AND INTERNAL STANDA D RECOVERIES :5 .0PQL61 .0PG/G0.14 .5POLNDPG/G0.1Total Pentachlorodibenzofurans (PeCDF) 1 2 .5SURROGATE AND INTERNAL STANDARD RECOVERIES :5 .0PQL11 .0PG/G0.10.310.6011SURROGATE AND INTERNAL STANDAR D RECOVERIES :1,2,3,4 , 7,8-Hexachlorodibenzofuran -C13Approved by :IN171%IDate :Quanterra Environmental Services , Anchorage, AKPage : 21Lab Report No . : 064096 Date: 10/04/99Project Name : Gambell HTW/DebrisAnalysis :PolychlorinatedProject No : 99-092Method :SW8290Prep Meth :METHODField ID : 99-GAM-022-SLLab Samp ID :G9H210185001Descr/Location : 99-GSample Date : 08/14/99Sample Time : 1630Matrix : SoilBasis : Dry WeightRec'd Date :Prep Date :Analysis Date :DC Batch :Notes :08/21/9908/25/9909/11/999237207AnalyteDet LimitRep Limit0 .501 .0Total Tetrachlorodibenzo-p-dioxins(TCDD)1 .0Total Tetrachlorodibenzofurans CDF0.50SURROGATE AND INTERNAL STANDARD RECOVERIES :40-135IN1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin-C131,2,3,6,7 .8-Hexachlorodibenzo-p-dioxin-C131,2,3,7 .8-Pentachlorodibenzo-p-dioxin-C13ResultUnits Ratio RT Pvc DilPDL7.6PG/G0.1POL47.0PG/G 0.1SMSA65%1NoteIN40-135SMSA72%1IN40-135SMSA69%1IN40-135SMSA65%140-135SMSA69%1Octachlorodibenzo-p-dioxin-C13ININ40-135SMSA72%12,3,7 .8-Tetrachlorodiibenzo-p-dioxin-C 13IN40-135SMSA70%12,3,7,8-Tetrachlorodibenzofuran-C 13IN40-135SMSA78%11,2,3,4,6 .7,8-Heptachlorodibenzofuran-C131 .2,3 .7,8-Pentachlorodibenzofuran-C 13Approved by :Date :~iuanterraQuanterra Inc - Anchorage AK LabClient Sample ID :Client Sample ID : 99-GAM - 022-SL99-GAM - 022-SLDioxinsMatrix . . . . . . . . . . SCLIDLot-Sample # . . . : G9H210185-001Work Order # . . . : D1M9N102Date Sampled . ._ : 08/14 /99 Date Received - . : 08/21/99Prep Date . . . . . . : 08/25 /99 Analysis Date . . : 09/11/99Prep Batch # . . . : 9237207Dilution Factor : 1DETECTIONLIMIT UNITSPARAMETERRESULT2,3,7,8 - TCDD0 .60 1TotalTCDD7 .61,2,3,7,8-PeCDD NDTotalPeCDDND1,2,3,4 , 7,8-HxCDD3 .3 J1,2,3,6 , 7,8-HxCDD125 .1 J1,2,3,7, 8,9-HxCDDTotalHxCDD1,2,3,4 , 6,7,8-HpCDD682502 .24 .5BTotalHpCDD430OCDD1100B2,3,7,8 - TCDF1 .2 CONTotalTCDF471,2,3,7,8-PeCDF ND2,3,4,7,8-PeCDF NDTotalPeCDF111,2,3,4,7,8-HxCDF ND2 .92 .11 .80 .181,2,3,6,7,8-HxCDF ND2,3,4,6,7,8-HxCDF ND1,2,3,7,8,9-HxCDF NDTotalHxCDF611, 2, 3, 4 , 6, 7, 8-Hp(DDF 961,2,3,4 , 7,8,9-HxCDF 5 .0 JTotalHpCDF470OIDF570INTERNAL STANDARDS13C-2,3,7,8-TODD13C-1,2,3,7,8-PeCDD13C-1,2,3,6,7,8-HxCDD13C-1,2,3,4,6,7,8-HpCDD13C-OCDDPERCENT RECOVERYRECOVERY LIMITS70(40135)69(40135)72(40135)65(40135)72(40135)13C-2,3,7,9-TCDF13C-1,2,3,7,8-PeCDF13C-1,2,3,4,7,8-HxCDF13C-1,2,3,4,6,7,8-HxCDF78697165(40(40(40(40-pg/gpg/gpg/gp9/ 9pg/gpg/gpg/gpg/gpg/gpg/gpg/gpg/gPg/gpg/gpg/gpg/gpg/gpg/gpg/gpg/gpg/gpg/gpg/gpg/gPg/gMETHODSW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846 8290SW846SW846SW846SW8468290829082908290( r ll G3135)135)135)135)NOTE(S) :Results and reporting limns have been adjusted for dry Weight.J E umated result. Result u less than the reporting limit .8 Method blank :ontarnutauun. The associated method bank contains the target analyte at a reportable level .COY Confirm anon analysts.JAIL ~CT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample IDMatrix994282003Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-023-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeSoil/SolidTechnical Directopr 5tephejYt . EdeOrdered ByPWSID91309/01/99 15 :1108 /14/99 16 :4508 /18/99 16 :35Released BySample Remarks :8270 - LCS/LCSD recovery for pyridine and 3,3-dichlorobenzidine is biased low . The resultIor these compounds areestimated .8270 - CCV recovery for 2,4-dinitrophenol is biased low . The results for this compound are estimated .DRO - Pattern consistent with highly weathered middle distillate .DRO/RRO - Surrogate recoveries outside controls due to matrix interference .ParameterTotal SolidsGasoline Range OrganicsResultsPaL89 .62 .68 U2 .68AllowableLimitsPrep AnalysisDate Date InitUnitsMethod%SM18 2540G08/24/99 MPAmg/KgAK101 GRO08/ 14/99 08 / 27/99 DAR%%AK101 GROAK101 GROmg/KgSW846- 8260mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846- 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 826008/ 14/99 08 / 27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRSSW846 - 8260SW846 - 8260SW846-826008/14/99 08/ 27/99 DRS08/ 14/99 08/27/99 DRS08/14/99 08/27/99 DRSSurrogates4-Bromoftuorobenzene 1,4-Difluorobenzene 56 .892 .2(50-150)(50-150 )08/14/99 08/27/9908/14/99 08/27/99VOA by GC/MS Method SW8260DichlorodifluoromethaneChloromethaneVinyl chlorideBromomethaneChloroethane0 .027 U0 .027 U0 .027 U0 .27 U0 .27 U0 .0270 .027TrichLoroftuoromethane1,1-Dichtoroethene^arbon disulfide!thylene chloride0 .027 U0 .027 U0 .27 U0 .1640 .0270 .0270 .270 .0270 .270 .270 .13mg/Kgmg/Kg08/14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRSLIE. 4 CT&E Environmental Services Inc .91309/01/99 15 :1108/14/99 16 :4508 /18/99 16 :35CT&E Ref.#Client NameProject Name/#Client Sample ID994282003Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-023-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/ TimeMatrixSoil/SolidTechnical Director : Stephen C . EdeOrdered ByPWSIDAllowableParametertrans - 1,2-Dichloroethene1,1-Dichloroethane2-Butanone ( MEK)2,2-Dichtoropropanecis-1,2-Dichtoroethene' romochloromethane.hloroform1,1,1-TrichloroethaneCarbon tetrachloride1,1-DichloropropeneBenzene1,2-DichloroethaneTrichloroethene1,2-DichloropropaneDibromomethaneBromodichloromethane2-chloroethylvinyl ethercis-1,3-Dichloropropene4-Methyl-2-pentanone (MIBK )Toluenetrans-1,3 - Dichloropropene1,1,2-TrichloroethaneTetrachloroethene1,3-DichLoropropane2-HexanoneDibromochloromethane1,2-DibromoethaneChlorobenzene1,1,1,2-TetrachloroethaneEthylbenzene& M -XyleneXyleneResults0 .027 U0 .027 U0 .27 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 UPQLUnitsMethod0 .0270 .0270 .27mg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 82600 .0270 .0270 .0270 .0270 .0270 .027mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0270 .0270 .0270 .027mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .027 U0 .027 U0 .027 U0 .27 U0 .027 U0 .27 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .27 U0 .027 U0 .027 U0 .027 U0 .0270 .0270 .0270 .270 .0270 .270 .0270 .0270 .0270 .0270 .027 U0 .027 U0 .027 U0 .0270 .0270 .0270 .0270 .027 U0 .0270 .270 .0270 .0270 .027mg/Kgmg/Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260LimitsPrepAnalysisDateDate Init08/ 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08 / 14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRSSW846 - 8260SW846 - 8260SW846-8260SW846- 8260SW846 - 8260SW846 - 8260SW846-8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 826008/ 14/99 08/ 27/99 DRS08 / 14/99 08/ 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRSSW846- 8260SW846 - 8260SW846 - 826008/ 14/99 08 / 27/99 DRS08 / 14/99 08/ 27/99 DRS08 / 14/99 08 / 27/99 DRSSW846 - 8260SW846 - 826008/ 14/99 08 / 27/99 DRS08 / 14/99 08/ 27/99 DRS08 / 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08 / 27/99 DRS08/14/99 08/27/99 DRS08 / 14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRSLt .. CT&E Environmental Services Inc .CT&E Ref .#994282003Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-023-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterStyreneBromoformIsopropylbenzene ( Cumene )Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene2-Chlorotoluene4-Chlorotoluene1,3,5-Trimethylbenzenetert - Butylbenzene1,2,4-Trimethytbenzenesec-Butylbenzene1,3-Dichlorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-DichLorobenzenen-ButyLbenzene1,2-Dibromo - 3-chloropropane1,2,4-TrichlorobenzeneHexachlorobutadieneNaphthalene1,2,3-TrichLorobenzeneResults0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .027 U0 .03270 .027 U0 .027 U0 .027 U0 .27 U0 .027 U0 .027 U0 .027 U0 .027 UPQLUnits0 .0270 .027mg/Kgmg/Kg0 .027mg/Kg0 .0270 .0270 .0270 .0270 .027mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0270 .0270 .0270 .0270 .027mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0270 .0270 .0270 .0270 .0270 .27mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0270 .0270 .0270 .027mg/Kgmg/Kgmg/KgMethod91309/01/99 15 :1108/14/99 16 :4508/18/99 16 :35AllowableLimitsSW846-8260PrepDateAnalysisDate Init08/14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRSSW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRSSW846-8260sW846-8260SW846-8260sw846-826008/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14 / 99 08/27/99 DRSSW846-8260sW846-8260Sw846-8260sW846-8260sW846-8260SW846-8260SW846-8260SW846-8260SW846-8260sw846-8260Sw846-8260Sw846-8260SW846-826008/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14 / 99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14 / 99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14 / 99 08/ 27/99 DRSSurrogatesDibromofluoromethane 90 .9106Toluene - d8 4-Bromofluorobenzene < Surr>107761,2-Dichloroethane - D4 %%%XSW846-8260SW846- 8260( 74-123 )(80-118)SW846- 8260SW846- 8260( 79-130 )( 71-141)08/14/99 08/27/9908 / 14/99 08/27/9908/14/99 08/27/9908/14/99 08/27/99CT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994282003Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-023-SLSoil/SolidParameterResultsClient PO#913Printed Date/Time09 /01/99 15 :11Collected Date/Time 08/14/99 16 :45Received Date/Time08/18 /99 16 :35Technical Director : Stephen C . EdePOLUnitsMethodAllowablePrep AnalysisLimitsDate DateInitDRO/RRO CombinationDiesel Range Organics6439 .98mg/KgResidual Range Organics GC18716 .5mg/KgAK102/ 103AK102/103XXAK102/ 103AK102 / 1030 .330 .330 .330 .330 .330 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 -82700 .33mg/Kg08/ 24/99 08/28/99 MMP08/24/99 08/28/99 MMPsurrogates5a Androstane !d-Triacontane !199216(50-150 )(50-150)08/24 /99 08/28/9908/24 / 99 08/28/99Semivolatiles by GC/MSN-NitrosodimethylaminePyridineAnilinePhenolBis(2 - Chloroethyl ) ether2-ChLorophenot1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1,2-DichLorobenzene2-Methylphenol (o-CresoL)bis(2-chloroisopropyl ) ether3&4-Methylphenot ( p&m-Cresol)N-Nitroso-di-n-propyLamineHexachtoroethaneNitrobenzene0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33mg/Kg0 .330 .330 .330 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/KgIsophorone2-Nitrophenol, 4-Dimethylphenol0 .33 U0 .33 U0 .33 U0 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/KgSW846 - 8270SW846-8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846- 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 827008/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08 / 25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 /22/99 08/ 25/99 LZ,z /G4CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name/#Client Sample . ID994282003Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-023-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterBenzoic acidBis(2-Chloroethoxy ) methane1,2,4-TrichlorobenzeneNaphthalene4-Chloroaniline! exachlorobutadiene4-Chtoro-3 - methylphenol2,4-Dichlorophenol2-MethylnaphthaleneHexachlorocyctopentadiene2,4,6-Trichlorophenol2,4,5-Trichtorophenol2-ChLoronaphthatene2-NitroaniLineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphthene2,4-DinitrophenoL4-NitrophenolDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyt - phenytetherFluorene4-Nitroaniline2-Methyl-4 , 6-dinitrophenolN-Nitrosodiphenylamine4-Bromophenyl - phenyletherexachlorobenzeneentachlorophenolResults1 .7 U0 .33 U0 .33 U0 .33 U0 .67 U0 .33 U0 .67 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U1 .7 U0 .33 U0 .33 U0 .33 U1 .7 U0 .33 U1 .7 U1 .7 U0 .33 U0 .33 U0 .33 U0 .33 UPQLUnits1 .7mg/Kg0 .330 .33mg/Kgmg/Kg0 .330 .670 .330 .670 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .330 .330 .330 .331 .70 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg1 .7mg/Kg0 .33mg/Kg1 .7mg/Kg1 .7mg/Kg0 .330 .330 .33mg/Kgmg/Kgmg/Kg0 .33mg/Kg0 .33 U0 .33 U1 .7 U0 .33 U0 .33mg/Kg0 .33mg/Kg1 .7mg/Kg0 .33mg/Kg0 .33 U0 .33 U1 .7 U0 .33mg/Kg0 .33mg/Kgmg/Kg1 .791309/01/99 15 :1108/14/99 16 :4508/18/99 16 :35AllowableMethod LimitsPrepDateSW846-8270SW846-8270SW846- 8270SW846-8270SW846- 8270SW846 - 8270SW846 - 827008 / 22/99 08/ 25/99 LZSW846- 8270SW846 - 8270SW846- 8270SW846- 8270SW846- 827008 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08 / 25/99 LZ08 / 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZSW846- 8270SW846 - 8270SW846- 8270SW846- 8270SW846- 8270SW846- 8270SW846- 8270SW846- 8270SW846 - 8270SW846- 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 827008/22/99 08/25/99 LZ08/ 22/99 08 / 25/99 LZ08/22/99 08/25/99 LZ08/22 / 99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22 / 99 08/25/99 LZ08/ 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270AnalysisDate Init08 /22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22 /99 08/25/99 LZ08 /22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ,A& LCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample ID994282003Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-023-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterPhenanthreneAnthraceneDi-n-butylphthalateFtuoranthenePyrene` zobenzenedutytbenzytphthatate3,3-DichlorobenzidineBenzo ( a)AnthraceneChrysenebis(2 -Ethythexyt) phthalatedi-n-OctylphthalateBenzo[b]FluorantheneBenzo[k]ftuorantheneBenzo[a] pyreneIndeno[1,2 , 3-c,d] pyreneDibenzo[a , h]anthraceneBenzo[g,h,i ] peryleneResultsPQL0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .67 U0 .33 U0 .33 U0 .3840 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 UUnitsMethod0 .33mg/Kg0 .33mg/Kg0 .330 .33mg/Kgmg/KgSW846 - 8270SW846- 8270SW846-8270SW846-82700 .330 .33mg/Kgmg/Kg0 .33mg/Kg0 .670 .330 .330 .33mg/Kgmg/Kgmg/Kg0 .33mg/Kg0 .33mg/KgXXXXXXSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82700 .330 .330 .330 .33mg/Kg0 .33mg/KgAllowableLimitsPrepDateAnalysisDateInit08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22 / 99 08/ 25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZSW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270mg/Kgmg/Kgmg/Kgmg/Kg91309 /01/99 15 :1108 /14/99 16 :4508 /18/99 16 :3508/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08 /22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZSurrogates2,4,6-Tribromophenot < Surr>Phenol - d6 Terphenyt - d14 2-Ftuorobiphenyt < Surr>2-FLuorophenot Nitrobenzene - d5 78 .856 .110869 .947 .459 .5( 18-122)( 24-88 )( 21-142)( 30-103 )( 18-83)( 18-109)08 / 22/99 08/25/9908/22 /99 08/25/9908/22/99 08/25/9908/22/99 08/25/9908/ 22/99 08/25/9908/ 22/99 08/25/99'AN11W& ~CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrixOrdered ByPWSID994282003Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-023-SLSoil/SolidParameterResultsClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/01/99 15 :1108/14/99 16 :4508/18/99 16 :35Technical Director: Stephen C . EdePOLAllowablePrepAnalysisLimitsDateDate InitUnitsMethod0 .003430 .003430 .003430 .00343mg/Kgmg/ Kgmg/Kgmg/KgSW846 808208/20/99 08/23/99 WAA0 .003430 .003430 .00343mg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846 808208/20 / 99 08 /23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/ 99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAAPCB's by GC ECDAroclor-12210 .00343 U0 .00343 U4roclor-1232,roclor-1242Aroclor-1248Aroclor-1254Aroclor-12600 .00343 U0 .00343 U0 .00343 U0 .00343 U0 .00343 UAroclor-1016SW846 8082SurrogatesDecachlorobiphenyl 120%SW846 8082(53 .3-125 ) 08/20 / 99 08/23/99mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8081ASW846 - 8081ASW846-8081ASW846 - 8081ASW846 - 8081ASW846- 8081ASW846- 8081ASW846 -8081A08/20/99 08/26/99 LZ08 /20/99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20/99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20 /99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 /99 08/26/99 LZSW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 -8081A08/20/99 08/26/99 LZ08/20/99 08/26/99 LZ08/20 /99 08 /26/99 LZPesticidesalpha-BHCbeta-BHCgamma -Chlordanealpha -Chlordanegamma - BHC (Lindane)delta-BHCHeptachlorAldrinHeptachlor epoxideEndosulfan I4,4'-DDEDieldrinEndrinEndosulfan II4'-DDD0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .001710 .001710 .00171 U0 .00171 U0 .00171 U0 .001710 .001710 .001710 .00171 U0 .001710 .001710 .001710 .001710 .001710 .001710 .001710 .001710 .001710 .00171mg/Kgmg/Kgmg/Kgmg/Kgmg/ KgSW846-8081ASW846 - 8081ASW846 - 8081A08/20/99 08/26/99 LZ08/20/ 99 08 /26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZAI ~ .CT&E Environmental Services Inc .CT&E Ref.#994282003Client NameOil Spill ConsultantsProject Name/#Client Sample IDMatrixOrdered ByPWSIDGambell DACA85-97-0010 DO 499-GAM-023-SLSoil/SolidParameterEndrin aldehyde4,4'-DDTEndosulfan sulfateEndrin ketoneMethoxychlor- oxapheneRes ul t sClient PO#Printed Date /TimeCollected Date/TimeReceived Date/TimeTechnical Director : Stephen C . EdePOL0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .00171 U0 .171 U91309/01/99 15 :1108/14/99 16 :4508/18/99 16 :35UnitsMethod0 .001710 .001710 .001710 .00171mg/Kgmg/Kgmg/Kgmg/Kg0 .00171mg/Kg0 .171mg/KgSW846- 8081ASW846-8081ASW846- 8081ASW846-8081ASW846 - 8081ASW846 - 8081AAllowablePrepAnalysisLimitsDateDate08/20 / 99 08 / 26/99 LZ08/20 / 99 08 / 26/99 LZ08/20/ 99 08 / 26/99 LZ08/20/99 08 / 26/99 LZ08/20/99 08 / 26/99 LZ08/20 /99 08/ 26/99 LZSurrogatesDecachlorobiphenyl < Surr>Tetrachloro - m-xylene < Surr>86X64XSW846 - 8081ASW846 - 8081AInit( 46-154 )(25-120 )08/20 / 99 08/26/9908/20 / 99 08/26/99'AHWEL ~CT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample ID994255013Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-023-SLMatrixOrdered ByPWSIDSoil/SolidClient PO#913Printed Date/Time09/09/99 16 :29Collected Date/Time 08/14/99 16 :45Received Date/Time 08/18/99 16 :35Technical DirectorrSteahan C . EdeReleased BySample Remarks :Sample analyzed for Dioxins (SW8290) by Triangle Laboratories of Durham, NC .AllowableParameterTotal SolidsResultsPQL89 .6LimitsPrep AnalysisUnitsMethodXSM18 2540G08/24/99 BJSDate DateInitMetals by ICPCopper694041 .2mg/KgSW846 6010809/02 / 99 09/03/99 WTA3 .340 .226mg/KgSW846 - 704108/24/99 08/27/99 KGF1 .570 .226mg/KgSW846 706008/24/99 08/30/99 JMO1 .800 .0904mg/KgSW846-713108 / 24/99 08/25/99 KGF39622 .6mg/KgSW846 - 742108/ 24/99 08/25/99 KGFMetals by Graphite FurnaceAntimonyMetals by Graphite FurnaceArsenicMetals by Graphite FurnaceCadmiumMetals by Graphite FurnaceLeadTL1 Project : 49337 Method 8290 PCDD/PCDF Analysis (b)- lient Sample : 99 .4255-13 Client Sample ID : 99-GAMAnalysis File : U316705-023-SLClient Profit u : Gambell, AKSample Matrix :SOIL Date Received: 08/21/1999 Spike File : SPMITTLI ID : 244-42-3Date Extracted : 08129/1999 ICai : UF58319Date Analyzed: 09111/1999ConCal :U993166Sample Size :Dry weight.GC Column :10.800 g Dilution Factor. rda % Moisture : 10.29.698 g Blank File :U315501 % Lipid:n/aDB-5 Analyst :SW % Solids : 89.8CoPUP42 .3 .7 . ;1= fCDD1 .2,3 .7 .3-PeCDD1 .2.3,4.7 .S-HxCDD1,'_.3 .6.7 .8-HxCDD1 .2.3 .7.X .9-HxCDD( .2.3 .4.6 .7 .8-HpCDD1 .2.3.4.6 .7 .8.9-OCDDND3 .32 .95 .83 .746 .31802.3.7.8-TCDF1 .2,3 .7 .8-PeCDF?.3 . 4.7 ..X -PeCDF. .2 .1 .4 .7 .8-Hx('DF1 . . 3 .6 .7 .$-HxCDF2 .3 .4.6.7 . :1-HxCDFI .' 3 .7 .8 .9-HxCDFI .2 .3 .4 .6 .7,8-Hp('DE1 .2 .3 .4 .7 .X .9-HpCDF1 .2 .' .4 .6 .7 .8 .9-0CDF44 .2EMPC6 .916.650.314.029 .1ND0 .883 .47 .958 .11 .01 .551 .261 .231 .141 .070 .8630 :5234 :0134 :0534:2337:1940:540 .79 25 :551 .441 .261 .231 .2330:3233 :1833 :2533 :531 .050 .960 .9336 :1837 :4941 :06TotskToalTCDDToad PiC'DDTotal I [xCDDTonal Hp('DD17 .145 .1731912Total "l'('DFTotal PXDFTotal Hx('DFTotal FIrC13F214166157141487219 .853 .01211t04219175159Page 1 of 2%Cr-- P= , I .olLAM a Is 00801 Capitola Onve ‚ Durham . North Carolina 27713Phone : (919) 544-5729 ‚ Fax : (919) 544-5491Printed : 03 :43 09/14/1999Triangle Laboratoris, IncaTLI Project : 49337 Method 8290 PCDD/PCDF Analysis (b)Client Sample : 99 .4255-13 Analysis File : U316705Client Sample ID : 99-GAM-023-SL"C, ‚-2 .3 .7 .8-TC'DF.8-TODD.7.3'1C,---2:-1 2 .3 .7 .8-PeCDF"C,-'C,,- 1 ._.3 .7 .8-PeC:DD"C, :- 1 .? 3 .6.7 .8-HxCDF"C, :-1 .2_.3 .6.7 .8-HxCDD"C, :-1 .2.3 .4.6,7 .8-HpCDF"C, :-1 . :.3 .4.6 .7 .8-HpCDD"C, :-1 .2.3 .4.6 .7 . 9-OCDD157182189183196228225309486Surrogaibs Sbrodwds Cry" ."C, :-2 .3 .4 .7 .8-PeCDF"C 1 .2 .3 .4 .7 .8-HxCDF"C, :-1 .' 1A7 .8-HxCDD"C, :-1 2 .3 .4.7 .8 .9-HpCDFI76 .188 .391 .588 .795 .111110915011840%-130%40%-130%40%-130%40%-130%40%-130%40%-130%25%-130%25%-130%25%-130%0 .760 .811 .451 .460.511 .220 .441 .250.8525 :5326:3629 :5030:51 _33 :24 _34:0536:1737:19 RO_40:5330:3133 :1937 :4941Caw ~>20318198 .587 .640%-130%22326510812840%-130%1 .470.521 .2825%-130%0.43Ot . StandardCare.'CL-2 .3 .7 .8-TCDD15 .3'-'C, .2_.3 .7 .8 .9-HxCDF:-1A', ‚-'_3 .4.6 .7 .8-HxCDF223231RT74 .440%-130%26:3710840%-130%40%-130%__112WPage 2 of 2Triangle Laboratori es, Inc.,801 Capitola Drive ‚ Durham, North Carolina 27713Phone (919) 544-5729 ‚ Fax : (919) 544-549134:00C lJanlts%"C,.4-TODD.3.2:-1'V . -- 1 . 2 .3 .7 .8 .9- HxCDDData Reviewer40%-130%0.5134 :390.5133:530.841 .2026 :2634:2309/14/1999%a .yM ., . a .LABSe,5 XPrinted: 03 :43 09/14/1999. ( ATLI Project : 49337 Method 8290 TCDD/TCDF Analysis (DB-225)Client Sample : 99 .4255-13 Client Sample ID : 99-GAM-023 -S L Analy sis File : P993249Client Project:Sample Matrix :TLI ID :1Gambell, AXSOIL244-42-3Date Received: 08/2111999Date Extracted : 08/29/1999Spike File :ICal :Date Analyzed: 09113/1999ConCal:Sample Size :10.300 gDilution Factorr n/a% Moisture :Dry Weight :9.698 gBlank File :P993270% Lipid :GC Column :DB-225Analyst:SW% Solids :ArAMM3,7,8-TCDFSPC2NF2SFF27079P99324510.2n/a89.3Cove.RW6 .1"C, :- 1 .2.34-TCDDData Reviewer _~tl23 :000 .8021 :48- 09/16/1999Page I of 1Triangle Laboratori e s, Inc .*801 Capitola Drive ‚ Durham, North Carolina 27713Phone (919) 544-5729 ‚ Fax : (919) 544-54910.72C4V Pgt .zo:L 56 :530Printed : 20 :08 09/16(1999'ACT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample IDMatrix994282004Client PO#913Printed Date/Time09/01/99 15 :11Collected Date/Time 08/14/99 17 :0008/18/99 16 :35Received Date/TimeTechnical Directote lih9QC . EdeOil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-024-SLSoil/SolidOrdered ByPWSIDSample Remarks :8270 - LCS/LCSD recovery for pyridine and 3 , 3-dichlorobenzidine is biased low . The results ?or these compounds areestimated .8270 - CCV recovery for 2, 4-dinitrophenol is biased low . The results for this compound are estimated .ParameterTotal SolidsGasoline Range OrganicsResultsPQLPrepAnalysisDate Date InitUnitsXSM18 2540G08/24/99 MPAmg/KgAK101 GR008/ 14/99 08/ 27/99 DARXXAK101 GR0AK101 GR00 .022mg/KgSW846 - 82600 .0220 .0220 .22mg/Kgmg/Kgmg/KgSW846 - 8260SW846 -8260SW846 -82600 .220 .0220 .022mg/Kgmg/Kgmg/KgSW846 -82600 .220 .110 .0220 .022mg/Kgmg/Kgmg/Kgmg/Kg94 .22 .17 UAllowableLimitsMethod2 .17Surrogates4-Bromofluorobenzene 1,4-Difluorobenzene 74 .994 .4(50-150 )( 50-150 )08/14 /99 08/27/9908/14/99 08/27/99VOA by GC/MS Method SU8260ChLoromethaneVinyl chloride0 .022 U0 .022 U0 .022 UBromomethaneChLoroethaneTrichtorofluoromethane1,1-Dichloroethene0 .22 U0 .22 U0 .022 U0 .022 UCarbon disulfideMethylene chloridetrans-1,2-Dichtoroethene,1-Dichloroethane0 .22 U0 .1410 .022 U0 .022 UDichlorodifluoromethaneSW846-8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SU846-826008 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08/14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08/14/99 08/27/99 DRSA 04CT&E Environmental Services Inc .91309 /01/99 15 :1108 /14/99 17 :0008 /18/99 16 :35CT&E Ref.#Client NameProject Name/#Client Sample ID994282004Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-024-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil /SolidTechnical Director : Stephen C . EdeAllowableParameter2-Butanone ( MEK)2,2-Dichloropropanecis-1,2-DichloroetheneBromochtoromethaneChloroform', 1,1-Trichloroethane. arbon tetrachloride1,1-DichLoropropeneBenzene1,2-DichloroethaneTrichLoroethene1,2-DichloropropaneDibromomethaneBromodichloromethane2-chloroethylvinyt ethercis-1,3 - Dichtoropropene4-Methyt - 2-pentanone ( MIBK )Toluenetrans-1,3 - Dichloropropene1,1,2-TrichtoroethaneTetrachloroethene1,3-Dichtoropropane2-HexanoneDibromochtoromethane1,2-DibromoethaneChlorobenzene1,1,1,2-TetrachloroethaneEthytbenzeneP & M -Xyleneo-Xylenet yrenexnoformResults0 .22 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .22 U0 .022 U0 .22 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .22 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 UUnitsMethod0 .220 .0220 .0220 .0220 .0220 .022mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 82600 .0220 .0220 .0220 .022mg/Kgmg/Kgmg/ Kgmg/Kg0 .0220 .0220 .0220 .0220 .220 .0220 .220 .0220 .0220 .0220 .0220 .0220 .220 .0220 .0220 .0220 .0220 .022mg/Kgmg/Kgmg/Kgmg/Kgmg/ Kgmg/Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg/ Kgmg/Kgmg/ Kgmg/Kgmg/Kgmg/Kgmg/KgPQL0 .0220 .0220 .0220 .022mg/Kgmg/ Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260LimitsPrepAnalysisDateDate Init08/ 14/99 08/ 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08 / 14/99 08 / 27/99 DRS08 / 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/14/99 08 / 27/99 DRS08/ 14/99 08 / 27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRS08 / 14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/ 27/99 DRSAIL 4 CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994282004Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-024-SLClient PO#Printed Date /TimeCollected Date/TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterIsopropytbenzene ( Cumene)Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene'-Chlorotoluene4-Chtorotoluene1,3,5-Trimethytbenzenetert - Butylbenzene1,2,4-Trimethylbenzenesec-Butylbenzene1,3-Dichlorobenzene4-Isopropyttotuene1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butytbenzene1,2-Dibromo - 3-chloropropane1,2,4-TrichlorobenzeneHexachLorobutadieneNaphthalene1,2,3-TrichlorobenzeneResultsUnitsMethod0 .022mg/KgSW846-82600 .0220 .0220 .0220 .022mg/Kgmg/KgSW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846-8260SW846 - 8260PQL0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .022 U0 .22 U0 .022 U0 .022 U0 .022 U0 .022 U0 .0220 .0220 .0220 .0220 .022mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .022mg/Kgmg/Kg0 .022mg/Kg0 .0220 .0220 .0220 .0220 .220 .0220 .0220 .0220 .022mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg91309/01/99 15 :1208/14/99 17 :0008 /18/99 16 :35AllowableLimitsPrepDateAnalysisDate Init08/14 / 99 08/27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08 / 27/99 DRS08/ 14/99 08/27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/14/99 08/27/99 DRSSW846 - 8260SW846 - 8260SW846-8260SW846 - 8260SW846 - 8260SW846 - 8260SW846 - 826008/ 14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/14/99 08/27/99 DRS08/ 14/99 08/ 27/99 DRS08/ 14/99 08/27/99 DRS08/14/99 08/ 27/99 DRSSW846-8260SW846 - 8260SW846 - 82605W846-8260SW846-8260SW846 - 8260SW846 - 8260Surrogatesy1,2-Dichloroethane-D4 91 .4XDibromoftuoromethane Toluene -d8 4-Bromofluorobenzene 10610896xXXSW846 - 8260SW846 - 8260SW846 - 8260SW846 - 8260(74-123 )(80-118)( 79-130 )( 71-141)08/14/99 08/27/9908/ 14/99 08/27/9908/14/99 08/27/9908/14/99 08/27/99CT&E Environmental Services Inc .91309/01/99 15 :1208 /14/99 17 :0008 /18/99 16 :35CT&E Ref .#Client NameProject Name /#Client Sample ID994282004Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-024-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixSoil /SolidTechnical Director : Stephen C . EdeOrdered ByPWSIDParameterResultsPQLUnitsMethodmg/Kgmg / KgAK102/103AK102/ 103%AK102/ 103AK102/ 103AllowablePrep AnalysisLimitsDate Date InitDRO/RRO CombinationDiesel Range OrganicsResidual Range Organics GC10 .2 U22 .010 .216 .908/24/99 08/28/99 MMP08/ 24/99 08/28/99 MMPSurrogates5a Androstane < surr>d-Triacontane < Surr>91 .6120%(50-150 )08/24 /99 08/28/99(50 - 150)08/24/99 08/28/99Semivolatiles by GC/MSN-NitrosodimethylaminePyridineAnilinePhenolBis(2-Chloroethyl ) ether2-Chtorophenol1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1,2-Dichlorobenzene2-Methylphenol ( o-Cresol )bis(2-chloroisopropyl ) ether3&4-Methylphenot ( p&m-Cresol )N-Nitroso - di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-Dimethylphenol0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .310 .31mg/ Kgmg/ Kg0 .310 .310 .310 .310 .310 .310 .310 .310 .31mg/ Kgmg/ Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/ Kgmg/ Kgmg/ Kgmg/ Kg0 .310 .310 .310 .310 .310 .310 .310 .31mg/ Kgmg/ Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/KgSW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 827008/ 22/99 08/25/99 LZ08/22/99 08 / 25/99 LZ08/22/99 08 / 25/99 LZ08/22 /99 08 / 25/99 LZ08/22/99 08/25/99 LZ08/22 /99 08 / 25/99 LZ08/22 /99 08/25/99 LZ08/22 /99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22 /99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZLt -CT&E Environmental Services Inc .CT&E Ref.#994282004Client NameOil Spill ConsultantsProject Name /#Gambell DACA85-97-0010 DO 4Client Sample ID99-GAM-024-SLClient PO#Printed Date / TimeCollected Date /TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterBenzoic acidBis(2-Chloroethoxy ) methane1,2,4-TrichlorobenzeneNaphthalene4-Chloroanilineiexachlorobutadiene4-Chloro - 3-methylphenot2,4-Dichtorophenol2-MethylnaphthateneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthatateAcenaphthytene2,6-Dinitrotoluene_3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenotDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl - phenyletherFluorene4-Nitroaniline2-Methyl-4,6 - dinitrophenolN-Nitrosodiphenylamine4-Bromophenyl - phenylether1 exachtorobenzene.' entachtorophenotResults1 .6 U0 .31 U0 .31 U0 .31 U0 .63 U0 .31 U0 .63 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U1 .6 U1 .6 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U0 .31 U0 .31 U1 .6 UPOLUnitsMethodSW846 - 8270SW846 - 8270SW846-8270SW846 - 82701 .6mg/Kg0 .31mg/Kg0 .31mg/Kg0 .310 .63mg/Kg0 .310 .630 .310 .31mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .31mg/Kg0 .310 .310 .31mg/Kgmg/Kgmg/Kg1 .6mg/Kg0 .310 .310 .31mg/Kgmg/Kgmg/Kg1 .6mg/Kg0 .311 .6mg/Kgmg/Kg1 .6mg/Kg0 .31mg/Kg0 .31mg/Kg0 .31mg/Kg0 .310 .310 .31mg/Kgmg/Kg1 .6mg/Kgmg/Kg0 .31mg/Kg0 .310 .31mg/Kg1 .6mg/Kgmg/KgSW846-8270SW846 - 8270SW846-8270SW846- 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846-8270SW846-8270SW846- 8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 827091309 /01/99 15 :1208 /14/99 17 :0008 /18/99 16 :35AllowablePrepAnalysisLimitsDateDateInit08 / 22/99 08 /25/99 LZ08/22/99 08 /25/99 LZ08/22/99 08/25/99 LZ08/22/99 08 / 25/99 LZ08/22/ 99 08 / 25/99 LZ08/ 22/99 08/ 25/99 LZ08/22/ 99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22 /99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22/99 08 / 25/99 LZ08/22/99 08 / 25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 /22/99 08/25/99 LZAUM-LCT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994282004Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-024-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsPQLUnitsMethodPhenanthreneAnthraceneDi-n-butytphthatateFluoranthenePyrene0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31mg/KgSW846 - 82700 .310 .310 .31mg/Kgmg/Kgmg/Kg0 .31mg/Kglzobenzeneautylbenzytphthalate3,3-DichtorobenzidineBenzo( a)AnthraceneChrysenebis(2-Ethylhexyl)phthalatedi-n-OctylphthalateBenzo[b]FluorantheneBenzo[k]fluoranthene0 .31 U0 .31 U0 .63 U0 .31 U0 .31 U0 .31 U0 .310 .310 .630 .310 .310 .31mg/Kgmg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82700 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .310 .310 .310 .310 .310 .31mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .31mg/KgSW846-8270XXXXXXSW846- 8270SW846 - 8270SW846- 8270SW846- 8270SW846-8270SW846-8270Benzo[alpyreneIndeno[1,2 , 3-c,d] pyreneDibenzo[a,hlanthraceneBenzo[g , h,i]perylenemg/Kgmg/Kg91309/01/99 15 :1208 /14/99 17 :0008 /18/99 16 :35AllowableLimitsPrepDateAnalysisDate Init08/ 22/99 08 / 25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/ 25/99 LZSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 82705W846 - 8270SW846 - 827008/22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/ 25/99 LZ08 / 22/99 08/ 25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/ 25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZSW846 - 8270SW846-8270SW846 - 8270Surrogates2,4,6-Tribromophenol Phenol - d6 Terphenyt - d14 2-Fluorobiphenyl < Surr>2-Fluorophenol Nitrobenzene - d5 7464 .910772 .55766(18-122 )( 24-88 )( 21-142 )(30-103 )( 18-83)( 18-109)08/22 / 99 08/25/9908/22 / 99 08/25/9908/22 / 99 08/25/9908/22/99 08/25/9908/22/99 08/25/9908/ 22/99 08/25/99ANWOLCT&E Environmental Services Inc .CT&E Ref .#994282004Client NameOil Spill ConsultantsProject Name/#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-024-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsPQLUnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 808291309/01/99 15 :1208/14/99 17 :0008/18/99 16 :35AllowableLimitsPrepDateAnalysisDate InitPCB's by GC ECDAroclor-12210 .00317 U0 .00317 U0 .003170 .00317roctor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-12600 .00317 U0 .00317 U0 .00317 U0 .00317 U0 .00317 U0 .003170 .003170 .003170 .003170 .00317Aroctor-1016SW846 808208/ 20/99 08/ 23/99 WAA08/ 20/99 08/23/99 WAAmg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846 808208/20/99 08/23/99 WAA08/20 / 99 08/ 23/99 WAA08/20 / 99 08/23/99 WAA08/20/99 08 / 23/99 WAA08/20/99 08 / 23/99 WAAXSW846 8082mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASurrogatesDecachlorobiphenyl < Surr>96 .6( 53 .3-125 ) 08/20 /99 08/23/99Pesticidesalpha-BHCbeta-BHCgamma - Chlordanealpha-Chlordanegamma - BHC (Lindane)delta-BHCHeptachlorAldrinHeptachlor epoxideEndosulfan I4,41-ODEDietdrinEndrin'dosulfan II.,4'-DDD0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .0003170 .0003170 .0003170 .0003170 .0003170 .0003170 .0003170 .0003170 .0003170 .0003170 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .0003170 .0003170 .000317mg/Kgmg/Kgmg/Kgmg/Kg0 .0003170 .000317mg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20 / 99 08/26/99 LZ08/20 / 99 08/ 26/99 LZ08/20 / 99 08/ 26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08 / 26/99 LZ08/20/ 99 08 / 26/99 LZ08/20/ 99 08 / 26/99 LZ08/20/ 99 08 / 26/99 LZ08/20/ 99 08 / 26/99 LZ08/20/99 08 / 26/99 LZ08/20/99 08 / 26/99 LZ08/20/99 08/26/99 LZ08/20/99 08/26/99 LZAl~kCT&E Environmental Services Inc .CT&E Ref .#994282004Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-024-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterEndrin aldehyde4,4 1 -DDTEndosulfan sulfateEndrin ketoneMethoxychlor.oxapheneResultsPQL0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .000317 U0 .0317 U0 .0003170 .0003170 .0003170 .0003170 .0003170 .0317UnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081ASW846 - 8081AXXSW846-8081ASW846-8081A91309/01/99 15 :1208/14/99 17 :0008 /18/99 16 :35AllowablePrepAnalysisLimitsDateDate Init08/20 / 99 08/26/99 LZ08/20 / 99 08 / 26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/ 26/99 LZ08/20 / 99 08/26/99 LZ08/20 / 99 08/ 26/99 LZSurrogatesDecachlorobiphenyl < Surr>Tetrachloro - m-xylene 78 .264 .8(46-154)( 25-120 )08/20/99 08/26/9908/20/99 08/26/99IL ACT&E Ref.#Client NameProject Name/#Client Sample IDMatrixCT&E Environmental Services Inc .994255014Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-024-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeSoil/SolidTechnical Director: SOrdered ByPWSID91309/09/99 16 :2908/14/99 17 :0008/18 /99 16 :35hen _C . WeReleased BySample Remarks :Sample analyzed for Dioxins (SW8290) by Triangle Laboratories of Durham, NC .ParameterTotal SolidsResultsPaL94 .2UnitsAllowableMethod LimitsXSM18 2540G08/24/99 BJSPrep AnalysisDate DateInitMetals by ICPCopper7 .324 .25mg/KgSW846 6010809/02 /99 09/03/99 WTA0 .211 U0 .211mg/KgSW846-704108/24/99 08 /27/99 KGF1 .090 .211mg/KgSW846 706008/24 / 99 08/30/99 JMO0 .03750 .0211mg/KgSW846-713108/24 / 99 08/ 25/99 KGF5 .642 .11mg/KgSW846 -742108/24/99 08/25/99 KGFMetals by Graphite FurnaceAntimonyMetals by Graphite FurnaceArsenicMetals by Graphite FurnaceCadmiumMetals by Graphite FurnaceLeadTLI Project : 49337 Method 8290 PCDD/PCDF Analysis (b)Client Sample : 99 .4255-14 Client Sample ID : 99-GAM -024-SL Analysis File : U316706Client Project : Gambell, AKSample Mtatrvc :SOIL Date Received : 08/21/1999 Spike File : SPMI'i72STL[ ID : 244-42-4 Date Extracted: 08/29/1999 ICal : UFS8319Date Analyzed : 09/1111999ConCal :U993166Sample Size :Dry Weight :GC Column :10 .500 g Dilution Factor. n/a % Moisture : 5.69.912 g Blank Fide : U313501 % Lipid : n/aDB-5 Analyst:SW % Solids : 94.41QUM2.3 .7.X-TCDD1 .2 .3 .7 .5-PeCDD1 .2.3,4.7 .8-HxCDD1 .2.3 .6.7 .X-HxCDD1 ._2.3.7.8 .9-HxCDD1 .2.3.1.6.7 .8-HpCDDI ,2.3.4,6.7 .8.94)CDDNDNDND1 .01 .41 .0090 .9ND9 .952 .41 .08 37:19 B_0.83 40:533 .4 .6.7 .8-HxCDF12.3 .7 .X .1)-HxCDFI .2 .3 .4 .6.7 .X-HpCDFI .2 .3 .4 .7 ., .9-HpCDFt .: .3 .4 .6.7 . ;t .94)CDF4 .8ND0 .9IDWC8 .62 .26 .7ND0 .917 .62 .115 .41'utal TC DDTotal PeCDDTotal Hx('DDTotal HpCDDNDND6 .621 .8Tot:d "I'('I)FTotal PeCDFTotal Hx('DFTotal 1(p('DF7S211 .1226 .062 .3 .7 .5-TCDF1 .2 .3 .7 .8-PeCDF2_.3 .4.7 .8-PeCDF12.3 .4 .7.8-HxCDFI .2.3 .6.7 .8-HxCDF32 .90 .78 25 :55 B2 .51 .22 33 :18 _1 .23 33 :25 J1-1933 :541 .010 .970 .8736 :18 _37 :48 J_41 :053217 .54Page 1 of 2WTr._M -106 . LA AS 6.15 XTriangl e Laboratori es, Inc.,,801 Capdola Drive • Durham , North Carolina 27713Ph-r (g191 544-5729 • Fax : (919) 544-5491• Printed : 03 :16 09/ 1411999. n CTLl Project : 49337Client Sample : 99 .4255-14Method 8290 PCDDI PCDF Analysis (b)Analysis File : U316706Client Sample ID : 99-GAM -024-SL"C, :-2.3 .7 .8-TC'DF"C,-2.3 .7 .8-TODD"C,-.-1 .2.3 .7 .8-PcCDF"C, :- l .? 3 .7 .8-P,.CDD13C, :- 1 .2_.3 .6.7.9-HpCDF"Cu-t' 3 .6.7 .9- Flx('DD'IC, :- .2.-;1 .4 .6.7, 8-HpCDF"C, :-1 .23 .4 .6.7.9-HpCDD"C, _ .1 2.3 .4 .6.7 .9 .9-0CDD13013613613313818316921738264 .267 .367 .266 .068 .690 .783 .610794 .640%-130%40%-130%40%-130%40%-130%40%-130%40%-130%25 %-130%25%-130%25%-130%0.770.851 .491 .460 .511 .160 .430 .990 .8325 :5226 :3529 :4930 :5133 :2434 :0536:1737 :1840:52'C, :-2.3 .4,7.8- PeCDF"C, . 1 .1 .4.7 .8-HpCDF"C, :-1 .23 .4.7 .9-HxCDD"C, :-1 ' x .4 .7 .9 .()-HpCDF14712816321172.963 .680 .710540%-130%1 .460 .501170 .4333 :1833 :5937 :48"C'L-2_ .3 .7 .9-T(')D11 .858 .240% -130%Conc {perRRCavaryCC tanksRado92.090.840%-130%0 .510 .5234:390.8326 :2434 :23Aitsnat. Standards O%yin )1 .2 .3 .7 .9 .'-HpCDF 186"C, :-'_3 .4.6 .7 .9- lUxCDF 1831 .2_ Z .4-TCDD(' _-1 .2 .3 .7 .9 O-HxCDD40%-130%40%-130%25%-130%40%-130%26 :361 .20Data ReviewerV VPage 2 of 230:3133:5309/1411999s ? vsa .t .a .Lbm6 ;s00Triangl. Laboratories, Inc .*801 Capitola Drive • Durham , North Carolina 27713. Printed : 03 :16 09/1411999TLI Project :Client Sample :49337 Method 8290 TCDD/TCDF Analysis ( DB-225)99 .4255- 14 Client Sample ID : 99-GAM -024-SL Analysis File : P993262TLI ID :Gambell, AKSOIL244-42-4Sample Size :Dry Weight:GC Column :10 .500 g9.912 gDB-225Client Project:Sample Matrix :Date Received: 08121/1999Date Extr3c- ed: 08129/1999Date Analyzed: 09/'1411999Spike Fide:ICal :ConCal :SPCZNF2SFF27079P993252Dilution F wtoc n/aBlank File :P993270Analyst :SS% Moisture :% Lipid:% Solids :5.6n/a94.4FigsAAWytw0-62.3 .7,8-TCDF0 .6723 :000 .7722 :590 .7821 :50J-ltt146"C, :-= .3 .7 .8-TCDF40%-130%72.21wy stwxbm.3 .4-TCDD"C, : .1 .2Data Reviewer.09/ 1611999VPage 1 of 1CZW _PW .20'. LAR S 6. :7 00Triangl e Laboratorls, Inc .s801 Capitola Drive • Durham, North Carorma 27713 Printed : 20 :08 09/16/1999-^ - 'n .1)\ c .4-r'rnO . Ce . . !a101 CA .1_e A'n .,-nCT&E Environmental Services Inc .cACT&E Ref.#Client NameProject Name/#Client Sample IDMatrix994282005Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date/TimeCollected Date/ TimeReceived Date/Time91309 /01/99 15 :1208/14/99 17 :3008 /18/99 1 :35Technical Director . Spjdn CeSoil/SolidOrdered ByPWSIDReleased BySample Remarks :8270 - CCV recovery for 2,4-dinitrophenol is biased low . The results for this compound are estimated .8270 - LCS/LCSD recovery for pyridine and 3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .DRO - Pattern consistent with highly weathered middle distillate .DRO - Heavier hydrocarbons contributing to diesel range quantitation .ParameterTotal SolidsGasoline Range OrganicsResultsPQL94 .72 .05 U2 .05AllowablePrepLimitsDate DateAnalysisUnitsMethodInit%SM18 2540G08/24/99 MPAmg/KgAK101 GRO08/14/99 08/27/99 DAR%%AK101 GROAK101 GROSW846 - 8260SW846 - 8260SW846 - 8260SW846-8260SW846 - 826008 /14/99 08/27/99 DRS08 /14/99 08/27/99 DRS08 / 14/99 08/27/99 DRS08 / 14/99 08/27/99 DRS08 / 14/99 08/27/99 DRSSW846 - 8260SW846 - 8260SW846 - 826008 / 14/99 08 /27/99 DRS08 / 14/99 08/27/99 DRS08 / 14/99 08/27/99 DRSSW846 - 826008 / 14/99 08/27/99 DRSSurrogates4-Bromofluorobenzene 1,4-Difluorobenzene 72 .593 .7( 50-150 )(50 - 150)08/14 / 99 08/27/9908/14/99 08/27/99VOA by GC/ MS Method SW8260DichlorodifluoromethaneChloromethaneVinyl chlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneCarbon disulfidelethylene chloride0 .020 U0 .020 U0 .020 U0 .20 U0 .20 U0 .020 U0 .0200 .020mg/Kgmg/Kg0 .0200 .200 .200 .020mg/Kgmg/Kgmg/Kgmg/Kg0 .020 U0 .20 U0 .10 U0 .0200 .200 .10mg/Kgmg/Kgmg/Kg` 1IL I CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994282005Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAiM-025-SLClient PO#Printed Date /TimeCollected Date /TimeReceived Date /Time91309/01/99 15 :1208/14/99 17 :3008/18/99 16 :35MatrixSoil/SolidTechnical Director : Stephen C . EdeOrdered ByPWSIDAllowableParametertrans-1,2-Dichloroethene1,1-DichLoroethane2-Butanone (MEK)2,2-Dichloropropanecis-1,2-DichloroetheneromochLoromethaneChloroform1,1,1-TrichloroethaneCarbon tetrachloride1,1-DichLoropropeneBenzene1,2-DichloroethaneTrichloroetheneResults0 .020 U0 .020 U0 .20 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U1,2-DichloropropaneDibromomethaneBromodichtoromethane2-chloroethytvinyl ethercis-1,3-DichLoropropene4-Methyl-2-pentanone ( MIBK)Toluenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachLoroethene1,3-Dichloropropane2-HexanoneDibromochloromethane1,2-DibromoethaneChLorobenzene1,1,1,2-Tetrachloroethane0 .020 U0 .020 U0 .20 U0 .020 U0 .20 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .20 U0 .020 U0 .020 U0 .020 U0 .020 UEthyLbenzene& M -Xylene,-Xylene0 .020 U0 .020 U0 .020 UPOLUnitsMethod0 .0200 .020mg/Kgmg/Kg0 .200 .0200 .0200 .0200 .0200 .020mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-82600 .0200 .0200 .0200 .0200 .0200 .0200 .020mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0200 .0200 .0200 .0200 .0200 .200 .0200 .0200 .0200 .020mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0200 .0200 .020mg/Kgmg/Kgmg/Kg0 .0200 .200 .0200 .20SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260LimitsPrepAnalysisDateDate Init08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRSSW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRSSW846-8260SW846-826008/14/99 08/27/99 DRS08/14/99 08/27/99 DRS,AI ° CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994282005Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsStyreneBromoformIsopropylbenzene (Cunene)Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U2-Chtorotoluene4-Chlorotoluene1,3,5-Trimethylbenzenetert-Butylbenzene1,2,4-Trimethytbenzene0 .020 U0 .020 U0 .020 U0 .020 U0 .020 Usec-Butytbenzene1,3-DichLorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butylbenzene1,2-Dibromo-3-chtoropropane1,2,4-TrichtorobenzeneHexachlorobutadiene0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .020 U0 .20 U0 .020 U0 .020 U0 .020 U0 .020 UNaphthalene1,2,3-TrichlorobenzenePQL91309 /01/99 15 :1208 /14/99 17 :3008 /18/99 16 :35AllowablePrepAnalysisLimitsDateDateUnitsMethod0 .0200 .0200 .0200 .0200 .0200 .020mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0200 .0200 .0200 .0200 .020mg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRSSW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS0 .0200 .0200 .0200 .0200 .0200 .0200 .0200 .200 .0200 .0200 .0200 .020mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRS08/14/99 08/27/99 DRSSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260Surrogates1,2-Dichtoroethane-D4 92 .2Dibromofluoromethane Toluene-d8 10610689 .64-Bromofluorobenzene XXXXSW846-8260SW846-8260SW846-8260SW846-8260Init(74-123)(80-118)(79-130)(71-141)08/14/99 08/27/9908/14/99 08/27/9908/14/99 08/27/9908/14/99 08/27/99'CG~CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994282005Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date /TimeMatrixSoil/SolidTechnical Director: Stephen C . Ede91309/01/99 15 :1208/14/99 17 :3008/18/99 16 :35Ordered ByPWSIDParameterResultsPQLUnitsMethodAllowableLimitsPrep AnalysisDate DateInitDR0/RRO CombinationDiesel Range OrganicsResidual Range Organics GC24 .850 .19 .17 mg/Kg15 .1 mg /KgAK102/ 103AK102/ 10393 .1127%%AK102/ 103AK102/1030 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 mg/Kg0 .33 mg/KgSW846-827008/24/99 08/28/99 MMP08 / 24/99 08/28/99 MMPSurrogates5a Androstane d-Triacontane (50-150 )(50 - 150)08/24 /99 08/28/9908 / 24/99 08/28/99Semivolatiles by GC/MSN-NitrosodimethylaminePyridineAnilinePhenolBis(2 -Chloroethyt) ether2-Chlorophenot1,3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1,2-Dichlorobenzene2-MethylphenoL ( o-Cresol )bis(2 -chloroisopropyt) ether3&4-Methylphenol ( p&m-Cresol )N-Nitroso - di-n-propylamineHexachtoroethaneNitrobenzeneIsophorone'- NitrophenoL., 4-Dimethylphenol0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/Kg0 .33 mg/KgSW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846-8270SW846 - 8270SW846-8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 827008/ 22/99 08/25/99 LZ08/22/99 08 / 25/99 LZ08/22/99 08/ 25/99 LZ08/22/99 08/ 25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08 /22/99 08/25/99 LZ08 /22/99 08/25/99 LZ08 /22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/ 22/99 08 / 25/99 LZ08/22/99 08 / 25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZILCA ~CT&E Environmental Services Inc .CT&E Ref.#994282005Client NameOil Spill ConsultantsProject Namel#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsBenzoic acidBis(2-Chloroethoxy ) methane1,2,4-Trichlorobenzene1 .7 U0 .33 U0 .33 UNaphthalene4-Chloroanilinelexachlorobutadiene4-Chloro-3 - methylphenol2,4-Dichlorophenol2-MethytnaphthaleneHexachlorocyctopentadiene2,4,6-Trichlorophenot2,4,5-TrichtorophenoL2-Chloronaphthalene2-Nitroaniline0 .33 U0 .68 U0 .33 U0 .68 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 UDimethylphthalateAcenaphthylene2,6-DinitrotoLuene3-NitroanilineAcenaphthene2,4-DinitrophenoL4-NitrophenolDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl - phenyletherFluorene4-Nitroaniline2-Methyl - 4,6-dinitrophenolN-Nitrosodiphenytamine4-Bromophenyl - phenylether1exachlorobenzeneentachlorophenol1 .7 U0 .33 U0 .33 U0 .33 U1 .7 U0 .33 U1 .7 U1 .7 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U1 .7 U0 .33 U0 .33 U0 .33 U1 .7 UPQLUnits1 .7mg/Kg0 .330 .33mg/Kgmg/Kg0 .330 .680 .330 .680 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .33mg/Kg0 .330 .331 .70 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg1 .7mg/Kg0 .331 .7mg/Kgmg/Kg1 .7mg/Kg0 .330 .330 .330 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg1 .70 .330 .33mg/Kgmg/Kgmg/Kgmg/Kg0 .331 .7mg/Kgmg/Kg91309/01/99 15 :1208/14/99 17 :3008/18/99 16 :35AllowableMethod LimitsPrepDateSW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 827008/22 / 99 08/ 25/99 LZ08/22 / 99 08/ 25/99 LZ08/22/99 08/25/99 LZSW846 - 8270SW846- 8270SW846- 8270SW846-8270SW846-8270SW846- 8270SW846- 8270SW846- 8270SW846- 8270SW846 - 8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846-8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846- 8270AnalysisDate Init08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08 /22/99 08/25/99 LZ08/22 /99 08/ 25/99 LZ08/22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08 / 22/99 08/25/99 LZ08/22 / 99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/ 22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZLtd. CT&E Environmental Services Inc .CT&E Ref .#994282005Client NameOil Spill ConsultantsProject Name /#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date/TimeCollected Date /TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterPhenanthreneAnthraceneDi-n-butylphthalateFluoranthenePyrene\zobenzeneautylbenzylphthalate3,3-DichlorobenzidineBenzo (a)AnthraceneChrysenebis(2-Ethylhexyl)phthalatedi-n-OctylphthalateBenzo[b]FluorantheneBenzo[klfluorantheneBenzo[a ]pyreneIndeno[1,2,3-c,dl pyreneDibenzo[a,h]anthraceneBenzo[g,h,ilperyleneResults0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .68 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 U0 .33 UPQLUnitsMethod0 .330 .330 .330 .330 .330 .330 .33mg/KgSW846-8270SW846-8270SW846-8270SW846-82700 .680 .330 .330 .330 .330 .330 .33mg/Kg0 .330 .330 .330 .33mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg91309/01/99 15 :1208 /14/99 17 :3008 /18/99 16 :35AllowablePrepAnalysisLimitsDateDate Init08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZSW846-8270SW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZ08/22/99 08/25/99 LZSW846-8270SW846-8270SW846-8270SurrogatesPhenol-d6 Terphenyl-d14 2-Fluorobiphenyl 2-Fluorophenol 80 .361 .411571 .452 .8Nitrobenzene-d5 60 .22,4,6-Tribromophenol XXXXXXSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270(18-122)(24-88)(21-142)(30-103)(18-83)(18-109)08/22/99 08/25/9908/22/99 08/25/9908/22/99 08/25/9908/22/99 08/25/9908/22/99 08/25/9908/22/99 08/25/99ALCT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994282005Oil Spill ConsultantsGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date /TimeCollected Date/TimeReceived Date /TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsPQLUnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846 8082SW846 808291309/01/99 15 :1208/14/99 17 :3008 /18/99 16 :35AllowableLimitsPrepDateAnalysisDate InitPCB's by GC ECDAroclor-1016Aroclor-1221lroclor-1232Aroclor-1242Aroctor-1248Aroclor-1254Aroclor-12600 .00341 U0 .00341 U0 .00341 U0 .00341 U0 .00341 U0 .00341 U0 .00341 U0 .003410 .003410 .003410 .003410 .003410 .003410 .00341mg/Kgmg/KgSW846 8082SW846 8082SW846 8082SW846 8082SW846 8082XSW846 8082mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A08 / 20/99 08/23/99 WAA08 / 20/99 08/23/99 WAA08 / 20/99 08/ 23/99 WAA08/20 /99 08/ 23/99 WAA08/20 /99 08/23/99 WAA08/20 /99 08/ 23/99 WAA08/20 /99 08/ 23/99 WAASurrogatesDecachlorobiphenyl < Surr>95 .8(53 .3-125 ) 08/20 / 99 08/23/99Pesticidesalpha-BHCbeta-BHCgamma - Chlordanealpha - Chlordanegamma - BHC (Lindane)delta-BHCHeptachlorAtdrinHeptachlor epoxideEndosulfan I4,41-ODEDieldrinEndrin‚ndosulfan II,,4'-DDD0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .0003410 .000341mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0003410 .000341mg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A08/20/99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20/99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ08/20 / 99 08/25/99 LZ'AlL ~CT&E Environmental Services Inc .CT&E Ref.#994282005Client NameOil Spill ConsultantsProject Name/#Client Sample IDGambell DACA85-97-0010 DO 499-GAM-025-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterEndrin aldehyde4,41-DDTEndosulfan sulfateEndrin ketoneMethoxychlorToxapheneResultsPQL0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .000341 U0 .0341 U0 .0003410 .0003410 .0003410 .0003410 .0003410 .0341UnitsMethodmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081AxSW846- 8081ASW846-8081A91309/01/99 15 :1208/14/99 17 :3008 /18/99 16 :35AllowableLimitsPrepDateAnalysisDate Init08/20/ 99 08/ 25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/ 25/99 LZ08/20/99 08/25/99 LZ08/20 /99 08/25/99 LZ08/20 /99 08/25/99 LZSurrogatesDecachlorobiphenyt Tetrachloro - m-xylene 74 .164 .1x(46-154)( 25-120 )08/20 / 99 08/25/9908/20 / 99 08/25/99A ILCT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOrdered ByPWSIDCT&E Environmental Services Inc .994255015Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-025-SLSoil/SolidClient PO#Printed Date/ TimeCollected Date / TimeReceived Date / TimeTechnical Director •91309/09/99 16 :2908/14/99 17 :3008/18 /99 16 :35tephen C . EdeSample Remarks :Sample analyzed for Dioxins (SW8290) by Triangle Laboratories of Durham, NC .AllowableParametertotal SolidsResultsPQL94 .7LimitsPrep AnalysisUnitsMethodDate Date InitXSM18 2540G08/24/99 BJSMetals by ICPCopper49 .34 .23mg/KgSW846 6010809/02/99 09/03/99 WTA0 .204 U0 .204mg/KgSW846-704108/24/99 08/27/99 KGF0 .6040 .204mg/KgSW846 706008/24/99 08/30/99 JMO0 .1290 .0204mg/KgSW846-713108/24/99 08/25/99 KGF9 .022 .04mg/KgSW846-742108/24/99 08/25/99 KGFMetals by Graphite FurnaceAntimonyMetals by Graphite FurnaceArsenicMetals by Graphite FurnaceCadmiumMetals by Graphite FurnaceLeade-TLI Project : 49337 Method 8290 PCDD/PCDF Analysis (b)Client Sample : 99 .4255-15 Client Sample ID : 99-GAM -025-S L Analysis File : U316707Gambeil, AKClient Project :SOILSample Matrix :TLI ID : 244-42-5Sample Size :Dry Weight:GC Column :10.500S9.9658DB-53 .7 .8-TCDDI .2.3 .7 .8- PeCDD1 .2,3,4 .7 .8-HxCDD1 . 2. 3., 6. 7 ,.88-131 .2.3.7 .8 .9-HxCDD1,23.4 .6.7 .8-Hp(MI)1 .2 .? .4 .6.7 . 8 .9-0(DDDate Received: 08/21/1999Date :Extracted 08/29/1999Date Analyzed : 09/1111999Spike File : SPMTF22sICal : UF58319CoaCal:U993166Dilution Factor. n/aBlank File :U315501Analyst:Sw% Moisture : 5.1% Lipid : n/a% Solids : 94.9ND0.70.80.60 .60.6NDNDNDND1.39 .72.3 .7,5-TCDF1 .2 3 .7 .X-Pe('DF2.3 .4.7 .8-PeCDFI .2 .3 .4 .7 .8-HpCDFI .' 3.6 .7 .$-HpCDF?.3 .4.6 .7 .8-HxC'DF1?.3.7 .X 1)-HpCDFI .2.3.4 .6 .7 .8-HpCDFNDNDND1 .2NDNDNDI .2 .3 .4 .7 .8 .9-HpCDF12.3.4 .6 .7 .8 .94XDFNDENIPCTotal T('DDNDTotal PeCDDTotal Hx('DDford IIp('DDNDTotal 'IC I )ENDTotal Pe('I)FTotal Hx('DFTotal I tp('1)FND2.124.1237 :1940:53TB1 .2833 :1810 .9236 :18JBJB0.70.60.70.40.50.52.4ND2.30.940.840.71 .9J0.70.80.620.70.6Page 1 of 2har. 1"9t • I a. URS 615 •XTriangle Laboratories, Inca801 Capitola Drive • Durham , North Carolina 27713Phone (919) 544-5729 • Fax : (919) 544-5491Printed: 03 :17 09 /141199911TLI Project : 49337Client Sample : 99 .4255-15Method 8290 PCDD/PCDF Analysis (b)Analysis File : U316707Client Sample ID : 99-GAM-025-SLknerma 5Cone.:oov..yQC Llift12314961 .20 .7514471 .678 .182.896 .910212640%-130%40%-130%40%-130%40%-130%40%-130%40%-130%25 %-130%0 .4425%-130%1 .040 .86"C, :-2 .3 .7 .8-TCDF"C, :-2.3 .7 .8-TC-DD1 3 C, :-1 . 2 .3 .7 .8-PcCDF"C, :- I .'3 .7 .8-PeCDD.2? .6.7 .8-HxCDF.-1"C,"C, :-1 .2 .? .6.7 .8-HxCDD"C,-- 1 .2.1-4 .6.7,S- HpCDF''C',--1 .' 3 .4 .67 .8-HpCDD"C, :-1 .2 .? .4 .6.7 .8.9-OCDD2-53487--2.3 .4.7 .8-PeCDF"C, . l .' 3 .4 .7 .8-HxCDF''C, :- 4 ._' .3 .4 .1 .8-HxCDD"(', :-I ' 3 .4 .7 .8 .9-HpCDF180166182267"('L-2_.3 .7 .8-TODD;'G-- l .2A7X1)-HxCDF"C, :-'_ .3 .1 .6 .7 .8-HxCDF' C,15716619420574 .40 .821 .461 .430 .521 .2325 :5226:3529 :4930:5133 :2434 :0436 :1737 :1812125%-130%89.640%-130%1 .4982.840%-130%0.5190.713340%-130%25%-130'0 .4413 .265.840%-130%21721310840%-130%0.5110640%-130%0 .5234:3933:530 .821 .1926:2534 :23"(', :-1 .2 .3 .4-TC DDc .-1 .2 .3 .7 .84 QQ-HxCDDData Reviewer.Phone (919) 544-5729 • Fax : (919 ) 544-549134.3133 :1834 :0037 :4826 :3609/1411999Page 2of2Triangl e Laboratoris, Inc .s801 Caprtola Drive • Durham . North Carolina 277131 .2440:53%on-ra ., 0•. WAS t a :oPrinted : 03 :17 09/14/19994 A 114L.CT&E Environmental Services Inc.Laboratory Division200 W . Porter DriveAnchorage , AK 9951a.1605Tel : (907) 562-2343Fax : (907) 561-5301Oil Spill Consultantsattention: Randy Easley209 E 51stAnchorage, AK 99503Account : Oil Spill ConsultantsContact : Randy EasleyProject: Gambell DACA85-97D-001ƒ DO 4Received: 08/18/99 16:35CT&E Ref# : 99 .4255Print Date : 09/20/999 :59Work order 99 .4255 was analyzed for Dioxinsby Triangle Laboratories Inc . of Durham, NC 27713-4411..126'Ahk tCT&E Environmental Services Inc .CT&E Ref .# 994255016Client PO#Client NamePrinted Date/Time91309/09/99 16 :29Collected Date/Time 08/14/99 18 :47Received Date/Time08/18/99 16 :35Technical Directortey h„ i C . EdeOil Spill ConsultantsProject Name /# Gambell DACA85-97-D-0010 DO 4Client Sample ID 99-GAM-026-SLMatrixSoil/SolidOrdered ByPWSIDReleased BySample Remarks :8270 - LCS/LCSD recovery for pyridine and3,3-dichlorobenzidine is biased low . The results for these compounds areestimated .8270 - Internal standard phenanthrene-d12 is biased low . The samples are non-detect . The results are not affected .RRO - Surrogate recovery outside controls due to matrix interference .ParameterTotal SolidsResultsPQL98 .4UnitsAllowableMethod LimitsPrepAnalysisDateDate Init%SM18 2540G08/24/99 BJSRCRA MetalsArsenicBariumCadmiumChromiumLeadMercury by Cold VaporSeleniumSilver5 .305 .950 .0202 U1 .333 .470 .0109 U0 .202 U0 .04192 .023 .670 .02020 .2022 .020 .01090 .2020 .0403mg / Kgmg/ Kgmg/Kgmg/ Kgmg/ Kgmg/ Kgmg/Kgmg/KgSW846 7060SW846 60108SW846-7131SW846-7191SW846-7421SW846-7471SW846 -7740SW846 -776108/24/99 08/30/99 JMO08/26/99 08/31/99 WTA08/ 24/99 08 /25/99 KGF08/24/99 08/25/99 KGF08/24/99 08/25/99 KGF08/25/99 08/25/99 RMV08/24/99 08/27/99 GCP08/24/99 08/25/99 KGFGasoline Range Organics1 .36 U1 .36mg/KgAK101 GRO08 /14/99 08/24/99 DAR%%AK101 GRO ( 50-150 )AK101 GRO (50-150 )08/14/99 08/24/9908/14/99 08/24/99Surrogates4-Bromofluorobenzene 1,4-Difluorobenzene 74 .194 .5A11F=L -CT&E Environmental Services Inc .CT&E Ref.#994255016Client NameOil Spill ConsultantsProject Namel#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-026-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director: Stephen C . EdeParameterResultsPOLUnits91309/09/99 16 :2908/14/99 18 :4708/18/99 16 :35AllowableMethod LimitsPrepDateAnalysissW846-8260SW846-8260SW846-8260SW846-826008/14/99 08/25/99 DRS08/14 / 99 08 /25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRSDate InitVOA by GC/ MS Method SW8260Dichlorodifluoromethane0 .014 UChloromethaneVinyl chlorideBromomethaneChtoroethaneTrichlorofluoromethane1,1-DichloroetheneCarbon disulfideMethylene chloridetrans-1,2-Dichloroethene0 .014 U0 .014 U0 .14 U0 .14 U0 .014 U0 .014 U0 .14 U1,1-Dichloroethane2-Butanone ( MEK)2,2-Dichloropropanecis-1,2 - DichloroetheneBromochloromethaneChloroform1,1,1-TrichloroethaneCarbon tetrachloride1,1-DichloropropeneBenzene1,2-DichloroethaneTrichLoroethene1,2-DichloropropaneDibromomethaneBromodichLoromethane0 .1010 .014 U0 .014 U0 .14 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U2-Chloroethyl Vinyl Ethercis-1,3-DichloropropeneMethyl-2 - pentanone ( MIBK)oluene0 .14 U0 .014 U0 .14 U0 .014 U0 .0140 .014mg/Kgmg/Kg0 .0140 .14mg/Kgmg/Kg0 .14mg/Kg0 .0140 .0140 .140 .068mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0140 .0140 .140 .014mg/Kgmg/Kgmg/Kg0 .014mg/Kg0 .0140 .014mg/Kgmg/Kg0 .014mg/Kg0 .014mg/Kgmg/Kg0 .0140 .014mg/Kg0 .0140 .0140 .0140 .0140 .0140 .14mg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0140 .140 .014mg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260sW846-8260SW846-8260SW846-8260SW846-8260sW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-826008/14 / 99 08 /25/99 DRS08/14/99 08/25/99 DRS08/14 / 99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 / 99 08 /25/99 DRS08/14/ 99 08 /25/99 DRS08/14 / 99 08 /25/99 DRS08/14/ 99 08 /25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08 / 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08 / 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS`C_'Ak-CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994255016Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-026-SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParametertrans - 1,3-Dichloropropene1,1,2-TrichLoroethaneTetrachloroethene1,3-Dichloropropane2-Hexanonelibromochloromethane1,2-DibromoethaneChLorobenzene1,1,1,2-TetrachloroethaneEthytbenzeneP & M -Xyleneo-XyleneStyreneBromoformIsopropylbenzene ( Cumene )Bromobenzene1,1,2,2-Tetrachloroethane1,2,3-Trichloropropanen-Propylbenzene2-Chlorotoluene4-Chlorotoluene1,3,5-TrimethyLbenzenetert - Butylbenzene1,2,4-TrimethyLbenzenesec-ButyLbenzene1,3-Dichlorobenzene4-Isopropyttoluene1,4-Dichtorobenzene1,2-DichLorobenzenen-Butytbenzene1,2-Dibromo-3 - chloropropane, 2,4-TrichlorobenzeneResultsPQLUnitsAllowableMethod LimitsPrepDate08/14/99 08 / 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 /99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 / 99 08/25/99 DRS0 .014 U0 .014 U0 .014 U0 .014mg/KgSU846-82600 .014mg/Kg0 .014mg/Kg0 .014 U0 .14 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .0140 .140 .0140 .0140 .0140 .014mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-82600 .014mg/Kg0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014 U0 .014mg/Kg0 .014 U0 .014 U0 .14 U0 .014 U91309/09/99 16 :2908/14/99 18 :4708/18/99 16 :350 .014mg/Kg0 .0140 .0140 .014mg/Kgmg/Kgmg/Kg0 .0140 .014mg/Kgmg/Kg0 .014mg/Kg0 .014mg/Kg0 .014mg/Kg0 .014mg/Kg0 .0140 .0140 .0140 .014mg/Kgmg/Kgmg/Kg0 .0140 .0140 .0140 .0140 .014mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .140 .014mg/Kgmg/KgSW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SW846-8260SU846-8260SW846-8260SW846-8260AnalysisDate Init08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14 / 99 08/25/99 DRS08/14 / 99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14 / 99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14 / 99 08/ 25/99 DRS08/14/99 08/ 25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRSCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name /#Client Sample ID994255016Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-026-SLClient PO#Printed Date/TimeCollected Date/ TimeReceived Date / TimeMatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeParameterHexachlorobutadieneNaphthalene1,2,3-TrichlorobenzeneResultsUnitsMethod0 .0140 .014mg/Kgmg/Kg0 .014mg/KgSW846-8260SW846-8260SW846-8260POL0 .014 U0 .014 U0 .014 U91309 /09/99 16 :2908/14/99 18 :4708/18 /99 16 :35AllowableLimitsPrep AnalysisDateDate Init08/14/99 08/25/99 DRS08/14/99 08/25/99 DRS08/14/99 08/25/99 DRSSurrogates1,2-Dichloroethane-D4 DibromofLuoromethane Toluene-d8 4-Bromofluorobenzene 10810710198 .5XXXXSW846-8260SW846- 8260SW846-8260SW846-8260mg/Kgmg/KgAK102/103AK102/103XXAK102/103AK102/103mg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270(74-123)(80-118)(79-130)(71-141)08/14/99 08/25/9908/14/99 08/25/9908/14/99 08/25/9908/14/99 08/25/99DRO/RRO CombinationDiesel Range OrganicsResidual Range Organics GC9 .35 U25 .69 .3515 .408/24/99 08/28/99 MMP08/24/99 08/28/99 MMPSurrogates5a Androstane d-Triacontane !125186(50-150)(50-150)08/24/99 08/28/9908/24/99 08/28/99Semivotatites by GC/MSN-NitrosodimethylaminePyridineAnilinePhenolBis(2 -Chloroethyl)ether2-Chlorophenol0 .31 U0 .31 U0 .310 .310 .31 U0 .31 U0 .31 U0 .31 U0 .310 .310 .310 .311,3-Dichlorobenzene1,4-DichlorobenzeneJenzyl alcohol0 .31 U0 .31 U0 .31 U0 .310 .310 .31mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-827008/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ~,ACT&E Environmental Services Inc .CT&E Ref .#994255016Client NameOil Spill ConsultantsProject Name/#Client Sample IDGambell DACA85-97-D-0010 DO 499-GAM-026-SLClient PO#Printed Date/TimeCollected Date / TimeReceived Date / Time91309/09/99 16 :2908/14/99 18 :4708 /18/99 16 :35MatrixOrdered ByPWSIDSoil/SolidTechnical Director : Stephen C . EdeAllowableParameter1,2-Dichlorobenzene2-Methylphenol (o-Cresol)bis(2-chloroisopropyt)ether3&4-Methylphenol (p&m-CresoL)N-Nitroso-di-n-propytamine4exachloroethanenitrobenzeneIsophorone2-Nitrophenol2,4-DimethylphenotBenzoic acidBis(2-ChLoroethoxy)methane1,2,4-TrichtorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2,4-Dichlorophenol2-MethytnaphthaleneHexachlorocyclopentadiene2,4,6-Trichlorophenol2,4,5-Trichlorophenot2-Chloronaphthalene2-NitroanilineDimethytphthalateAcenaphthylene2,6-Dinitrototuene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenollibenzofuranResults0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U0 .31 U0 .31 U0 .64 U0 .31 U0 .64 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U1 .6 U1 .6 U0 .31 UPQL0 .310 .31UnitsMethodmg/Kgmg/Kgmg/Kgmg/KgSW846-82700 .31mg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-82700 .31mg/Kgmg/KgSW846-8270SW846-82700 .310 .310 .310 .310 .310 .311 .60 .31mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgsu846-82700 .31mg/Kg0 .31mg/Kg0 .640 .310 .640 .31mg/Kgmg/Kgmg/Kgmg/Kg0 .31mg/Kg0 .310 .31mg/Kgmg/Kg0 .31mg/Kg0 .31mg/Kg1 .6mg/Kg0 .310 .310 .31mg/Kgmg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846 -8270SW846-8270SW846- 8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-8270SW846-82701 .60 .311 .61 .60 .31mg/Kgmg/Kgmg/Kgmg/KgSW846-8270SW846-8270SW846-8270SW846-8270SW846-8270LimitsPrepAnalysisDateDate Init08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08 /24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/ 99 08 /24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22 /99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ08/22/99 08/24/99 LZ'A LCT& E Environmental Services Inc .CT&E Ref .#Client NameProject Name /#Client Sample ID994255016Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-026- SLClient PO#Printed Date/TimeCollected Date/TimeReceived Date/Time91309/09/99 16 :2908/14/99 18 :4708 /18/99 16 :35MatrixSoil/SolidTechnical Director: Stephen C . EdeOrdered ByPWSIDParameter2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl - phenyletherFluorene4-Nitroaniline?-Methyl-4,6 - dinitrophenolri-Nitrosodiphenylamine4-Bromophenyl - phenyletherHexachlorobenzenePentachtorophenolPhenanthreneAnthraceneDi-n-butylphthalateFluoranthenePyreneAzobenzeneButylbenzylphthalate3,3-DichlorobenzidineBenzo ( a)AnthraceneChrysenebis(2-Ethylhexyl)phthalatedi-n-OctylphthalateBenzo[b]FluorantheneBenzo[k ] fluorantheneBenzo[a ] pyreneIndeno[1,2 , 3-c,d] pyreneDibenzota , hlanthraceneBenzo[g , h,ilperyleneResults0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U0 .31 U0 .31 U1 .6 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .64 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 U0 .31 UPQL0 .310 .310 .310 .310 .311 .60 .310 .310 .311 .60 .310 .310 .310 .310 .310 .310 .310 .640 .310 .310 .310 .310 .310 .310 .310 .310 .310 .31UnitsMethodmg / Kgmg/Kgmg / Kgmg / Kgmg /Kgmg/Kgmg /Kgmg /KgSW846 - 8270SW846- 8270SW846 - 8270SW846 - 8270SW846 - 8270mg /Kgmg /Kgmg /Kgmg /Kgmg/Kgmg/Kgmg /Kgmg /Kgmg /Kgmg/Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /Kgmg /KgAllowableLimitsmg /Kgmg/Kg%SW846 - 8270AnalysisDateInit08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZSW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846-8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846 - 8270SW846 - 8270SW846-8270SW846-8270PrepDate08 / 22/99 08 /24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08 / 24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08 / 24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22 / 99 08 / 24/99 LZ08/22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08 / 22/99 08/24/99 LZ08/22 / 99 08 / 24/99 LZSurrogates!,4,6-Tribromophenol 83 .1( 18-122 )08/22 / 99 08/24/99.t4LCT&E Environmental Services Inc .Z 091309/09/99 16 :2908/14/99 18 :4708/18 /99 16 :35CT&E Ref.#Client NameProject Name/#Client Sample ID994255016Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-026- SLClient PO#Printed Date /TimeCollected Date/TimeReceived Date/TimeMatrixSoil/SolidTechnical Director: Stephen C . EdeOrdered ByPWSIDParameterAldrinHeptachlor epoxideEndosulfan I4,4'-DDEDieldrinindrinEndosuLfan II4,4'-DDDEndrin aldehyde4,4'-DDTEndosutfan sulfateEndrin ketoneMethoxychlorToxapheneResultsPOL0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .0326 U0 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0003260 .0326UnitsMethodmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081Amg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/KgAllowablePrepAnalysisLimitsDateDate08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081Amg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081ASW846-8081A%%SW846-8081ASW846-8081A08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20/99 08/25/99 LZ08/20 /99 08/25/99 LZ08/20/99 08/25/99 LZSurrogatesDecachlorobiphenyl Tetrachloro-m-xylene 82 .671 .6Init(46-154)(25-120)08/20/99 08/25/9908/20/99 08/25/99AtL, CT&E Environmental Services Inc .CT&E Ref .#Client NameProject Name/ #Client Sample IDMatrixOrdered ByPWSID913Client POD09/09/99 16 :29Printed Date/TimeCollected Date /Time 08/14/99 18 :4708/18 /99 16 :35Received Date/ TimeTechnical Director : Stephen C . Ede994255016Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-026-SLSoil/SolidParameterResultsUnitsMethodXXXXXSW846 - 8270SW846 - 8270SW846 - 8270SW846 - 8270SW846-82700 .003260 .003260 .00326mg/Kgmg/Kgmg/KgSW846 8082SW846 8082SW846 80820 .003260 .003260 .003260 .00326mg/Kgmg/Kgmg/Kgmg/KgSW846 8082SW846 8082sw846 8082SW846 8082XSW846 80820 .0003260 .0003260 .0003260 .0003260 .000326mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8081ASW846-8081ASW846-8081ASW846-8081A0 .0003260 .000326mg/Kgmg/KgPQLAllowableLimitsPrepDateAnalysisDate Init( 24-88 )( 21-142 )( 30-103 )08/22 / 99 08/24/9908/22 / 99 08/24/9908/22 / 99 08/24/9908/22/99 08/24/9908/22/99 08/24/99SurrogatesPhenol-d6 Terphenyl - d14 '- Fluorobiphenyl < Surr>--Fluorophenot < Surr>Nitrobenzene - d5 73 .414278 .565 .773 .5(18-83)(18-109 )PCS's by GC ECDAroclor-12210 .00326 U0 .00326 UAroclor-1232Aroclor - 1242Aroclor-1248Aroclor - 1254Aroclor-12600 .00326 U0 .00326 U0 .00326 U0 .00326 U0 .00326 UAroclor - 101608/20/99 08/23/99 WAA08/20 /99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAA08/20/99 08/23/99 WAASurrogatesDecachlorobiphenyl < Surr>105( 53 .3-125 ) 08/20/99 08/23/99Pesticidesalpha-BHCbeta-BHCgamma - Chlordanealpha - Chlordanegamma-BHC (Lindane)delta-BHC,eptachlor0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 U0 .000326 USW846-8081ASW846-8081ASW846-8081A08/20/ 99 08/25/99 LZ08/20/99 08/ 25/99 LZ08/20/ 99 08/ 25/99 LZ08/20/ 99 08/ 25/99 LZ08/20 / 99 08/ 25/99 LZ08/20/ 99 08/ 25/99 LZ08/20 / 99 08/25/99 LZA dL -0CT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOrdered ByCT&E Environmental Services Inc .994255017Oil Spill ConsultantsClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeGambell DACA85-97-D-0010 DO 499-GAM-027-SLSoil/SolidTechnical Director02/05/200114 :0008/18/1999 16 :35ephen C . EdeReleased BySample Remarks :Corrected report : Prep date for 8260 corrected .ParameterResultsPQLAllowableLimitsPrepDateAnalysisDate InitUnitsMethod%SM20 2540Gmg/KgAK101 GRO08/24/9908/24/99 DAR%AK101 GRO 50-15008/24/9908/24/99 DAR%AK101 GRO 50-15008/24/9908/24/99 DARSW846-8260BS W 846-8260B08/22/9908/22/9908/22/99 DRS08/22/99 DRSSW846-8260B08/22/9908/22/99 DRSSW846-8260B08/22/9908/22/99 DRSS W 846-8260BSW846-8260B08/22/9908/22/9908/22/99 DRSSW846-8260BSW846-8260B08/22/9908/22/9908/22/9908/22199 DRS08/22/99 DRSSolidsTotal Solids10008/23/99 BJSVolatile Fuels DepartmentGasoline Range Organics12 .62 .50rogates1,4-Difluorobenzene 4-Bromofluorobenzene 96.269 .9Volatile Gas Chromatography/ Mass SpectroscopyDichlorodifluoromethane0 .0262 U0 .0262mg/KgChloromethaneVinyl chloride0 .0262 U0 .0262mg/Kg0 .0262 UBromomethane0 .262 UChloroethaneTrichlorofluoromethane0 .262 U0 .02620 .2620 .262mg/Kgmg/Kgmg/Kg0 .0262 U0 .0262 U0 .0262mg/Kg0 .0262mg/Kg0 .262 U0 .131 U0 .2620 .131mg/Kgmg/Kg0 .0262 U0 .02620 .262mg/Kgmg/Kg0 .0262mg/Kg0.0262 U0 .0262I,1-Dichloroethane0.0262 Ucis-1,2-DichloroetheneBromochloromethane0.0262 U0 .0262 U1, 1 -DichloroetheneCarbon disulfideMethylene chloridetrans-l,2-Dichloroethene2-Butanone (MEK)2,2-Dichloropropane1, 1, 1 -Trichloroethane)roform0 .262 U0.0262 U0 .0262 Ut,arbon tetrachloride0 .0262 UBenzene0 .0262 US W 846-8260BSW846-8260B08/22/9908/22/99 DRS08/22/99 DRS08/22/99 DRSSW846-8260B08/22/99mg/KgSW846-8260BS W 846-8260B08/22/9908/22/990 .0262mg/KgS W 846-8260B08/22/9908/22/99 DRS0 .02620 .02620 .02620 .02620.0262mg/KgS W 846-8260B08/22/99mg/KgSW846-8260BS W 846-8260B08/22/9908/22/9908/22/99 DRS08/22/99 DRSS W 846-8260B08/22/9908/22/99 DRSS W 846-8260B08/22/9908/22/99 DRSmg/Kgmg/Kgmg/Kg08/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/99 DRSCT&E Environmental Services Inc .'AhkIDCT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOrdered By994255017Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-027-SLSoil/SolidParameterResultsClient PO#Printed Date /TimeCollected Date/TimeReceived Date/TimeTechnical DirectorPOLAllowableLimits02 /05/2001 14 :0008/18/1999 16 :35Stephen C. EdePrep AnalysisDate Date InitUnitsMethodmg/KgS W 846-8260B08/22/9908/22/99 DRSS W 846-8260BSW846-8260B08/22/9908/22/9908/22/99 DRS08/22/99 DRSVolatil e Gas Chromatography / Mass Spectroscopy1, 1 -Dichloropropene0 .0262 U0 .02621,2-Dichloroethane0 .0262 U0 .0262mg/KgTrichloroethene0 .0262mg/Kg1,2-Dichloropropane0 .0262 U0 .0262 U08/22/9908/22/99 DRS0 .0262 Umg/Kgmg/KgS W 846-8260BDibromomethane0 .02620 .0262S W 846-8260BBromodichloromethane0 .0262 U0 .0262mg/KgS W 846-8260B08/22/9908/22/9908/22/99 DRS08/22/99 DRS2-Chloroethyl Vinyl Ether0 .262 US W 846-8260BS W 846-8260B08/22/99 DRS0 .0262 U0 .0262 Umg/Kgmg/Kg08/22/991,1,2-Trichloroethane0 .2620 .026208/2219908/22/9908/22/99 DRS08/22/99 DRS0 .262mg/Kgmg/KgSW846-8260B08/22/990 .02620 .02620 .0262mg/Kgmg/Kgmg/Kg08/22/99 DRS08/22/99 DRScis-1,3-Dichloropropene[ethyl-2-pentanone (MIBK)0 .262 Utrans-l,3-Dichloropropene0 .0262 U0 .0262 UTetrachloroethee0 .0262 UToluene1,3-Dichloropropane0 .0262 U0 .262 U0 .0262S W 846-8260BSW846-8260BS W 846-8260B0 .0262mg/KgS W 846-8260BS W 846-8260B0 .262mg/KgS W 846-8260BDibromochloromethane1,2-Dibromoethane0 .0262 U0 .0262mg/KgS W 846-8260B0 .0262 U0 .0262mg/Kg1, 1, 1,2-Tetrachloroethane0 .0262 U0 .0262mg/KgS W 846-8260BS W 846-8260BChlorobenzene0.0262 Umg/KgS W 846-8260BEthylbenzeneP & M -Xylene0 .0262 U0 .02620 .0262mg/Kg0 .0262 U0 .0262mg/KgS W 846-8260BSW846-8260Bo-Xylene0 .0262 U0 .0262Styrene0 .0262 UBromoform0 .0262 U0 .02620 .0262mg/Kgmg/Kgmg/KgIsopropylbenzene (Cumene)0 .0262 UBromobenzene1,2, 3-Trichloropropane0 .0262 Un-Propylbenzene0 .0262 U0 .02620 .02620 .02620 .02620 .02620 .02620 .0262mg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kgmg/Kg0 .0262 U0 .0262 U0 .0262mg/Kg0 .0262mg/KgS W 846-8260BSW846-8260B0 .0262 U0 .0262mg/KgS W 846-8260B2-Hexanone1,1,2,2-Tetrachloroethane2-Chlorotoluene4-Chlorotoluene',5-Trimethylbenzene.-Butylbenzene1,2,4-Trimethylbenzene0 .0262 U0 .0262 U0 .0262 U0 .0262 US W 846-8260BSW846-8260BS W 846-8260BS W 846-8260B08/22/9908/22/9908/22/99 DRS08/22/9908/22/99 DRS08/22/9908/22/9908/22/9908/22/99 DRS08/22/99 DRS08/22/9908/22/9908/22/9908/22/9908/22/9908/22/9908/22/9908/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/99 DRS08/22/9908/22/99 DRS08/22/9908/22/99 DRS08/22/99 DRSS W 846-8260B08/22/99SW846-8260B08/22/9908/22/9908/22/99 DRS08/22/9908/22/99 DRS08/22/99 DRSS W 846-8260B08/22/9908/22/99 DRSSW846-8260B08/22/9908/22/9908/22/99 DRSS W 846-8260BS W 846-8260B08/22/9908/22/99 DRS08/22/99 DRS08/22/9908/22/99 DRS'AlLICT&E Environmental Services Inc .CT&E Ref.#994255017Client PO#Client NameProject Name/#Client Sample IDOil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-027-SLSoil/SolidPrinted Date/TimeCollected Date/TimeReceived Date/Time02/05/2001 14 :00Technical DirectorStephen C . EdeMatrix08/13/1999 16 :35Ordered ByParameterResultsPQLUnitsMethodLimitsAllowable Prep AnalysisDate Date InitVolatile Gas Chromatography/Mass Spectroscopysec-Butylbenzene1,3-Dichlorobenzene4-Isopropyltoluene1,4-Dichlorobenzene1,2-Dichlorobenzenen-Butylbenzene0 .0262 U0 .0262 U0 .0262 U0 .0262 U0.0262 U0 .02620 .02620 .02620 .0262mg/Kgmg/Kgmg/Kgmg/Kgmg/KgSW846-8260BSW846-8260BSW846-8260BSW846-8260BSW846-8260BSW846-8260B0 .0262 U0 .02620 .02621,2-Dibromo-3-chloropropane0.262 U0 .2621,2,4-Trichlorobenzene0 .0262 U0.0262 U0 .02620 .0262mg/Kg0 .0262 U0 .0262 U0 .0262mg/Kgmg/KgSW846-8260B101%SW846-8260B", xachlorobutadiene.,hthalene1,2,3-Trichlorobenzene0 .0262mg/Kgmg/Kgmg/KgSW846-8260BSW846-8260BSW846-8260B08/22/9908/22/9908/22199 DRS08/22/99 DRS08/22/9908/22/99 DRS08/22/9908/22/9908/22/99 DRS08/22/99 DRS08/22/9908/22/99 DRS08/22/9908/22/9908/22/99 DRS08/22/9908/22/99 DRS08/22/99 DRS08/22/9908/22/9908/22/99 DRS80-11808/22/9908/22/99 DRSSW846-8260B08/22/99 DRSSurrogatesDibromofluoromethane 1,2-Dichloroethane-D4 106Toluene-d8 99 .9%%SW846-8260BSW846-8260B74-12379-13008/22/9908/22/9908/22/99 DRS08/22/99 DRS4- Bromo fluoro benzene 100%SW846-8260B71-14108/22/9908/22/99 DRSCT&E Environmental Services Inc .CT&E Ref.#Client NameProject Name/#Client Sample IDMatrixOrdered By994255018Oil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-028-SLOther LiquidsClient PO#Printed Date/TimeCollected Date/TimeReceived Date/TimeTechnical Director _ .02/05/200114 :0008/13/1999 16 :35Stephen C. EdeSample Remarks :Corrected report : Sample matrix changed to other liquid, sample was a vial of Methanol .ParameterResultsPQLPrepDateAnalysisDate InitAK101 GRO08/24/9908/24/99 ELBUnitsMethodmg/LAllowableLimitsVolatile Fuels DepartmentGasoline Range Organics0 .0900 U0 .0900Surrogates1,4-Difluorobenzene 90 .7%AKIO1 GRO 50-15008/24/9908/24/99 ELB4-Bromofluorobenzene 81 .7%AK IOI GRO 50-15008/24/9908/24/99 ELB0 .001000 .00100mg/LSW846-8260Bmg/L08/20/9908/20/9908/20/99 SPM08/20/99 SPM0 .00100mg/LS W 846-8260BS W 846-8260B08/20/9908/20/99 SPM08/20/99 SPM08/20/99 SPMVolatile Gas Chromatography/ Mass SpectroscopyDichlorodifluoromethaneChloromethane0 .00100 UVinyl chlorideBromomethane0 .00100 U0 .00100 U0 .00100mg/LS W 846-8260B08/20/99Chloroethane0 .00100 U0 .00100mg/LTrichlorofluoromethane1,1-Dichloroethene0 .00100 U0 .00100 U0 .00500 U0 .0100 US W 846-8260BSW846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMtrans- 1,2-Dichloroethene1, 1 -DichloroethaneS W 846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMSW846-8260BSW846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMcis-I ,2-Dichloroethene0.00100 U0 .001000 .001000 .00100mg/L2,2-Dichloropropane0 .00100 U0 .00100 U0.00100 Umg/Lmg/Lmg/Lmg/Lmg/L08/20/9908/20/99Methylene chlorideCarbon disulfide0 .001000 .001000 .005000 .01000 .00100SW846-8260BSW846-8260B2-Butanone (MEK)0.0100 U0 .0100mg/LSW846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMBromochloromethane0 .00100 U0 .00100mg/LS W 846-8260BChloroform0 .00100 U0 .00100 U0 .00100 US W 846-8260BSW846-8260B1, 1 -Dichloropropene0 .00100 Umg/Lmg/Lmg/Lmg/L08/20/99 SPM08/20/99 SPM1, 1, 1 -TrichloroethaneCarbon tetrachloride0 .001000 .001000 .001000 .0010008/20/9908/20/99n ‚nzene0 .00100 U0 .00100mg/LDichloroethaneTrichloroethene0 .00100 U0 .00100 Umg/Lmg/LS W 846-8260BSW846-8260B1,2-Dichloropropane0 .00100 U0 .001000 .001000 .00100mg/LS W 846-8260B0 .00100 Umg/Lmg/L08/20/99 SPM08/20/9908/20/99 SPMSW846-8260B08/20/9908/20/99 SPMSW846-8260B08/20/99S W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPM08/20/99 SPM08/20/9908/20/99 SPM08/20/9908/20/99 SPML1 ..ME Environmental Services Inc .CT&E Ref.#994255018Client NameProject Name/#Client Sample IDMatrixOrdered ByOil Spill ConsultantsGambell DACA85-97-D-0010 DO 499-GAM-028-SLOther LiquidsParameterResultsClient PO#Printed Date /TimeCollected Date/TimeReceived Date/TimeTechnical DirectorPQLUnits Method02/05/200114 :0008/18/1999 16 :35Stephen C . EdeAllowable PrepAnalysisLimitsDate Date InitVolatile Gas Chromatography/Mass SpectroscopyDibromomethane0.00100 UBromodichloromethane0.00100 U2-Chioroethyl Vinyl Ethercis- 1,3-Dichloropropene0.0100 U0.00100 UToluene0.00100 U0.00100 Utrans-1,3-Dichloropropene1,1,2-Trichloroethane0.00100 UTetrachloroethene)ichloropropane0 .00100 U0 .00100 Uiioromochloromethane0 .00100 U1,2-DibromoethaneChlorobenzene0 .00100 U0 .00100 U1, 1, 1,2-Tetrachloroethane0 .00100 UEthylbenzeneP & M -Xylene0 .00100 U0 .00100 Uo-XyleneStyrene0 .00100 U0 .00100 UBromoform0 .00100 UIsopropylbenzene (Cumene)0 .00100 UBromobenzene0 .00100 U0 .00100 U1,1,2,2-Tetrachloroethane1,2,3-Trichlorop ropanen-Propylbenzene0 .00100 U0 .00100 U0 .001000 .00100mg/LS W 846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPM0 .00100mg/LSW846-8260B08/20/9908/20/99 SPM0 .001000 .00100mg/LS W 846-8260B08/20/99 SPMmg/L0 .00100mg/LS W 846-8260BS W 846-8260B08/20/9908/20/990 .001000 .001000 .001000 .00100mg/Lmg/L0 .00100mg/Lmg/LSW846-8260BSW846-8260B08/20/9908/20/99 SPM08/20/99 SPMmg/Lmg/LS W 846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMmg/LS W 846-8260BSW846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMS W 846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMmg/Lmg/LS W 846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMmg/Lmg/LS W 846-8260BS W 846-8260B08/20/9908/20/9908/20/99 SPM08/20/99 SPMmg/LSW846-8260B08/20/9908/20/99 SPMmg/L08/20/9908/20/99 SPM08/20/99 SPM0 .001000 .001000 .001000 .001000 .001000 .001000 .001000 .001000 .001001, 3 , 5-Trimethy lb enzenetert-Butylbenzene0 .00100 U0 .001000 .001000 .001000 .001000 .001000 .001000 .001000 .001000 .001001,3-Dichlorobenzene0 .00100 U0 .00100 U' - .,)propyltoluene)ichlorobenzene0 .00100 U1,2-Dichlorobenzene0 .00100 Un-Butylbenzene0 .00100 U08/20/99 SPM08/20/99 SPMmg/Lmg/L0 .00100 U0 .00100 U08/20/99 SPM08/20/9908/20/990 .01000 .001000 .00100sec-Butylbenzene08/20/990 .001000 .001000.00100 U1,2,4-TrimethylbenzeneS W 846-8260BS W 846-8260BS W 846-8260B2-Chlorotoluene4-Chlorotoluene0 .00100 U0 .00100 Umg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/LS W 846-8260BS W 846-8260BS W 846-8260BSW846-8260B08/20/9908/20/9908/20/9908/20/9908/20/9908/20/9908/20/99 SPM08/20/99 SPM08/20/99 SPM08/20/99 SPM08/20/99 SPM08/20/99 SPMmg/LSW846-8260BSW846-8260Bmg/LSW846-8260B08/20/9908/20/99mg/Lmg/Lmg/Lmg/LSW846-8260B08/20/9908/20/99 SPM08/20/99 SPMS W 846-8260BS W 846-8260B08/20/9908/20/99 SPM08/20/9908/20/9908/20/99 SPMS W 846-8260Bmg/LSW846-8260B08/20/9908/20/99 SPM08/20/99 SPM`G'ANIL 4CT&E Environmental Services Inc .Client PO#CT&E Ref.# 994255018Client NamePrinted Date/Time 02/05/2001 14 :00Collected Date/TimeReceived Date/Time 08/18/1999 16 :35Technical Director Stephen C . EdeOil Spill ConsultantsProject Name/# Gambell DACA85-97-D-0010 DO 4Client Sample ID 99-GAM-028-SLOther LiquidsMatrixOrdered ByParameterResultsPQLUnitsMethodAllowable Prep AnalysisDateLimitsDateInit08/20/99 08/20/99SPM08/20/99 08/20/9908/20/99 08/20/99SPM08/20/99 08/20/9908/20/99 08/20/99SPM08/20/99 08/20/99SPM08/20/99 08/20/99SPMVolatile Gas Chromatog raphy/Mass Spectroscopy1,2-D ibromo- 3-ch loropropane1,2,4-Trichlorobenzene0 .00100 U 0 .00100 mg/L SW846-8260B0 .00100 U 0 .00100 mg/L SW846-8260B0.00100 U 0 .00100 mg/L SW846-8260B0.00100 U 0 .00100 mg/L SW846-8260BHexachlorobutadieneNaphthalene1,2,3-Trichloro benzene4-Methyl- 2-pentanone (MIBK)2-Hexanone0.00100 U 0 .00100 mgfL SW846-8260B0 .0100 U 0 .0100 mg/L SW846-8260B0 .0100 U 0 .0100 mg/L SW846-8260BSPMSPM:rogatesDibromofluoromethane 98 .2% SW846-8260B1,2-Dichloroethane-D4 99 .3% SW846-8260B% SW846-8260B96 .64-Bromofluorobenzene 99 .2Toluene-d8% SW846-8260B08/20/99 08 /20/99 SPM08/20 /99 08 /20/99 SPM08/20 /99 08 /20/99 SPM08/20 /99 08/20/99 SPMAppendix GData Deliverables for Project SamplesPlease Note : Data deliverables package for project samples is in a separate binder .Appendix HSafety and Health Phase-Out ReportAppendix HSafety and Health Phase-Out ReportSafety and Health Phase -Out ReportDebris Removal and Containerized Hazardous Waste Removal and Toxic Waste RemovalDelivery Order No . 004, Contract No . DACA85-97-D-0010Gambell, AlaskaScope of WorkFrom July 5, 1999, through August 18, 1999, Oil Spill Consultants removed the following wastefrom formerly used defense sites at Gambell, Alaska :Hazardous and Toxic Waste (HTW) . Approximately, 26 .8 tons of HTW (battery, parts,dried paint, drums, and transformer carcasses) were collected from five locations atthe project site .•Metal Debris . Based on field weights, 142,234 pounds of metal debris consisting ofrunway matting, cable, fuel tanks and equipment parts were removed from sitesidentified by USAEDA .•Contaminated Soil . Workers using picks and shovels excavated 52 tons ofcontaminated soil from Sevuokuk Mountain .•Stained Soil . A total of 20 tons of petroleum-stained soil were excavated from severalsites at Gambell .This waste was shipped from the project site to state and EPA-approved disposal facilities inthe Lower 48 following EPA and U .S . Department of Transportation guidelines .Safety PerformanceFrom start to finish, 5,629 man-hours were required to complete this project . Local personnelresiding in Gambell, Alaska, provided 61 percent (3,434 man-hours) of the project labor .There were no accidents, near misses, spills or equipment failures during this project . This isa noteworthy achievement in view of the environmental conditions at the project site . Thescope of work required Oil Spill Consultants to remove contaminated soil and metal debris soilfrom Sevuokuk Mountain (about 600 ft . above sea level) . Large boulders and narrow trailsprecluded the use of heavy equipment on the mountain top . Dense fog frequently limitedvisibility to 50 ft . or less . Despite these conditions the work was complete without any safetyproblems because:• Daily safety meetings addressed site hazards and emphasized safety precautions .• Experienced supervisors were used .• Local residents were familiar with the terrain and accustomed to working in theenvironmental conditions at the project site .• The government QAR provided insight, which helped Oil Spill Consultants resolveH-2problems that were unique to the Gambell environment . For example, when it wasrecognized that the boulders on Sevuokuk Mountain limited heavy equipment and truckto access Site 4/Area 4B, the QAR recommended using Argos (small track-mountedvehicles) to haul the excavated soil and debris down the mountain . Implementing thisrecommendation prevented vehicle roll-over accidents that could have resulted if truckswere used .During the 1999 summer season, Gambell residents experienced three serious accidents thatwere not related to this project . One local resident was injured when a rifle discharged whileshe was removing fresh game from a small boat . Another resident drove a wooden stakethrough his hand while performing maintenance at this home . A young child experienced aneye injury while playing in her home .In general, the accident frequency is high in Alaska's bush communities . However, by adheringto the requirements set forth in the site-specific safety and health plan for this project andproviding experienced supervision, it was possible to complete an accident-free project withlocal labor .Lessons LearnedThe following lessons were learned regarding safety during this project :•Limit crew hours . Due to the requirement to have all waste removed and packagedprior to the arrival of the southbound barge at Gambell, Alaska, from Seattle,Washington, we elected to work seven 12-hour days per week . After the first 21 days,crew morale rapidly declined, and constant friction existed between various crewmembers . Since low morale and friction could compromise safety, it would be prudentto limit the normal workday at remote sites to 10 hours a day, six days a week .•Conduct site visit prior to submitting cost proposal . The scope of work prepared by thegovernment for this project neglected to identify wet tundra in Site 10 and boulders inSite 4 . As a result, inappropriate equipment was identified for soil excavation at Site 4and for transporting soil and debris through Site 10 . Since inappropriate equipmentcould cause accidents, contractors should always conduct a site visit for projects inremote areas .Exposure MonitoringPrior to excavation, a portable photoionization detector (PID) was used to field screen areaswith stained soil . During this project, all PID readings were zero . The PID was also used tofield screen the drums that were removed from Site 10 . All of the drums contained large holescreated by rust and contained a few inches of rainwater . The PID readings from these drumswere zero .Signatureer/Assistant Site Safety and Health OfficerH-3Appendix IChemical Data Quality ReviewLABORATORY DATA CONSULTANTS, INC.7750 EI Camino Real, Suite 2C Ca isbad, CA 92009 Phone : 760/634-0437 Fax : 760/634-0439LDC Project# : 4332U .S . Army Corps of EngineersAlaska DistrictBLDG 21-702Elmondorf AFB, AK 99506Attn : Mr. Bret WaltersJanuary 19, 200081 JANIn USubject: Gambell HTW Debris RemovalDear Mr. Walters,Enclosed is our EPA Level 3 Data Review Report for the uGambell HTW Debris Removal'project . The analyses were performed by Quanterra Environmental Services inAnchorage, Alaska, CT & E Environmental Services, Inc . in Anchorage, Alaska, andTriangle Laboratories Inc . in Durham, North Carolina . . The laboratory data was receivedon December 30, 1999 under Sample Delivery Group No . 994255 . The laboratory splitdata was received on December 8, 1999 under Sample Delivery Group No . 064096 .Please feel free to call me at (760) 6340437 if you have any questions .Richard M . AmanoPresident/PrincipalChemistRECEIVEDJAN 2 4 20004332COV .ARMREVIEW OF ANALYTICAL CHEMISTRY RESULTSGambell HTW , Debris RemovalProject# 99-092 /LDC# 4332This report details the findings of an EPA Level 3 documentation review of analyticalchemistry results generated in support of the Gambell HTW, Debris Removal project .Analyses were performed by Quanterra Environmental Services in Anchorage, Alaska,CT & E Environmental Services, Inc . in Anchorage, Alaska, and Triangle Laboratories,Inc. in Durham, North Carolina . Samples were analyzed for GC/MS Volatiles by EPASW 846 Method 8260B, GC/MS Sernivolatiles by EPA SW 846 Method 8270,Organochlorinated Pesticides by EPA SW 846 Method 8081, PolychlorinatedBiphenyls by EPA SW 846 methods 8082, Metals by EPA SW 846 Methods6010/7000, Gasoline Range Organics by Alaska Method AK101, Diesel RangeOrganics & Residual Range Organics by Alaska Methods AK102/AK103, and Dioxinsby EPA SW 846 Method 8290 . Samples are referenced under the following SampleDelivery Groups : 064096 and 994255. See the Sample Analysis Table (Attachment 1)for the number of samples reviewed and the Sample Validation Table (Attachment 2)for the sample identifications and analyses for the primary samples .The QC criteria used for review purposes is that specified in the National FunctionalGuidelines for Organic/Inorganic Data Review, February 1994 .Where specificguidance is not available, the data has been evaluated in a conservative mannerconsistent with industry standards using professional experience . The following itemswere evaluated during the review :• Holding Times• Sample Preservation• Cooler Temperatures• GC/MS Instrument Performance Check• Initial and Continuing Calibration• Blanks• Surrogates• Matrix Spike/Matrix Spike Duplicates• Laboratory Control Samples• Detection and Quantitation LimitsOnly issues which require comment o,r action are discussed in this report . Datadeficiencies are arranged by method, and presented as numbered findings . Potentialeffects of data anomalies have been described where possible .1LaboratoryData Consultants, Inc .ReviewofAnalyticalDataGambell HTW, Debris RemovalI. Overall Data AssessmentOut-of-control events experienced by the laboratory have warranted the qualification ofa portion of the data set as estimated (J) and some detectable results were qualified asestimated (J) and are discussed in detail by finding . Based upon the informationreviewed, the overall data quality is considered acceptable with the noted limitations .The HRGC/HRMS instrument performance check, Initial calibration, and routinecalibration data were not provided for the dioxin/dibenzofuran analysis for SDG 994255and therefore were not reviewed .II . Chain of Custody/Cooler Temperatures /PreservationThe chain-of-custodies were reviewed for documentation of cooler temperatures andsample preservation . All appropriate samples were preserved and all cooler temperaturesmet validation criteria .III . GC/MS Volatiles by EPA SW 846 Method 8260BFor GC/MS volatile organic analysis , holding times, instrument calibrations , instrumentperformance checks , blanks , internal standards , field QC , and all accuracy and precisionresults were within validation criteria with the following exceptions :Finding 1 : Continuing calibration percent differences (%D) between the initialcalibration RRF and the continuing calibration RRF were within the QClimits with the following exceptions :DateCompound%a (limits )Associated Samples8/26/992 -Butanone2-Chloroethylvinyl ether42..7 (c25 .0)2T_0 (525 .0)AN samples in SOG 064096JJ8/20/99Chloroethane26.6 (525 .0 )99-GAM-028-SL256433JFlagAction:Samples were qualified as estimated (J) as indicated above . This isconsidered a technical deficiency .Finding 2 :Method blanks were reviewed for each matrix as applicable . No volatilecontaminants were found in the method blanks with the followingexceptions :2Laboratory Data Consultants, Inc .Gambell HTVV. Debris RemovalReview of Analytical DataMethod Blank ID256479AnalysisDate8/22/99CompoundTIC (RT In minutes)Concentration0 .238 mg/KgMethylene chlorideAssociated Samples99-GAM-009-SL99-GAM-01 0SL99-GAM-011 SL99-GAM-01 2-SL99-GAM-01 3-SL99-GAM-01 4-SL99-GAM-01 5-SL99-GAM-01 7-SL99-GAM-01 8-SL99-GAM-01 9-SL99-GAM-02r--SL99-GAM-027-SL2564338/ 20/990.0018 mg/L0.0019 mg/LMethylene chlorideBromomethane99-GAM-028-SLSample concentrations were compared to concentrations detected in the method blanks .The sample concentrations were either not detected or were significantly greater (> 1 OXfor common contaminants, >5X for other contaminants) than the concentrations foundin the associated method blanks with the following exceptions :Sample99-GAM-026-SLCompoundTIC (RT in minutes)ReportedConcentrationMethylene chloride0.101 mg/KgTModified FinalConcentration0.101U mg/KgFinding 3: Surrogates were added to all samples and blanks as required by themethod . All surrogate recoveries (% R) were within QC limits with thefollowing exceptions :SampleSurrogate%R (Umits)CompoundFlag99-GAM-009-SLBromofluorobenzene69 .3 (71-141)All TCL compoundsJ99-GAM-014-SLBromafluorobenzene64 .6 (71-141)All TCL compoundsJ99-GAM-0I5-SLBromofluorobenzene60(71-141)AU TCL compoundsJAction :Samples were qualified as estimated (J) as indicated above . This isconsidered a protocol violation .3 Laboratory Data Consultants, Inc .Gambell HTW, Debris RemovalReview of Analytical DataSampleSurrogate%R (Umits )CompoundFlag99-GAM-016 SLBra mofluo robe nz ene144 (70 130)All TCL compoundsJ (all detects)Action:Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a protocol violation .Finding 4 :Matrix spike (MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable with the following exceptions :SampleCompoundAU samples in SDGs064096 and 994255AU TCL compoundsCriteriaFlagMS/MSO required.NoneFindingNo MS/MSD associated with thesesamples.For the samples listed in the table above, surrogate, laboratory control sample andlaboratory control sample duplicates were used to assess precision and accuracy . Sincethese were acceptable with the exceptions noted in this report, sample results were notqualified based on this finding . This is considered a protocol violation .Finding 5 : Laboratory control samples were reviewed for each matrix asapplicable . Percent recoveries (% R) and relative percent differences(RPD) were within QC limits with the following exceptions :LCS 10(AssociatedSamples )256434/256435(99-GAM-028-SL256433)Action :CompoundICS%R (Omits)LCSD%R (Omits)RPD(Umits)FlagMethylene chloride139 (71-138)146 (71-138)-J (all detects)Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a protocol violation .Samples 99-GAM-027-SL and 99-GAM-028-SL were identified as trip blanks . No volatilecontaminants were found in these blanks .Samples 99-GAM-014-SL and 99-GAM-015-SL were identified as field duplicates . Novolatiles were detected in any of the samples .4Laboratory Data Consultants . Inc .Gamb.ll HTW, Debris RemovalReview of Analytical DataSamples 99-GAM-014-SL (original ) and 99 -GAM-016 -SL (referee ) and samples 99-GAM015-SL ( original ) and 99-GAM-016-SL (referee ) were compared . No volatiles weredetected in any of the samples .IV. GC/MS Semivolatiles by EPA SW 846 Method 8270For GC/MS semivolatiles organic analysis, holding times, instrument calibrations,instrument performance checks, blanks, and all accuracy and precision results werewithin validation criteria with the following exceptions :Continuing calibration percent differences (%D) between the initialcalibration RRF and the continuing calibration RRF were within QClimits with the following exceptions :Finding 1 :CompoundDate9/9/99N-Nitrosodimet ytamine%.D (Umits)Associated Samples34 .9 (525)All samples in SOG 064096-Action :FlagJjiSamples were qualified as estimated (J) as indicated above . This isconsidered a technical deficiency.Finding 2 : Matrix spike ( MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable with the following exceptions :SampleAll samples in SOGs064096 and 994255CompoundAll TCL compoundsFindingNo MSIIMSD associated with thesesamples .CriteriaFlagMS/MSD required.NoneFor the samples listed in the table above , surrogate, laboratory control sample andlaboratory control sample duplicates were used to assess precision and accuracy . Sincethese were acceptable with the exceptions noted in this report , sample results were notqualified based on this finding . This is co nsidered a protocol violation .Finding 3 : Laboratory control samples were reviewed for each matrix asapplicable . Percent recoveries (% R) and relative percent differences(RPD) were within QC limits with the following exceptions :5Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW, Debris RemovalLCS 10(AssociatedSamples )CompoundBS990825E(All samples in SOG 064096 )AnilinePyridine256464 /256465(AU samples in SDG 994255 )3 ,3'-DichlorobenzidinePyridineAction:LCSLCSORPO% R (Limits)%R (Umits )( Umits)Flag-12 (510)16 (510)JJ46.3 (54-94 )2 .12 (10-32)Samples were qualified as estimatedconsidered a protocol violation .47 .6 (54-94)JJ2.19 (10-32)(J) as indicated above . This isLCS ID(AssociatedSamples )256464/256465(All samples in SOG 994255)CompoundLCS%R (Omits)LCSD%R (Limits)RPD(Omits)FlagButylbenzyiphthalateDi-n-octylphthalateBis(2-ethyihexyl)phthalate164 (52-108)124 (62-103)Ill (63-110)180 (52-108)128 (62-103)-J (ad detects)J (all detects)J (al detects)Action:Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a protocol violation .Finding 4:All internal standard areas and retention times were within QC limitswith the following exceptions :Sample99-GAM-01 G-SLInternal StandardsChrysene-dl 2Perylene-dl 2Area ( Omits )374446 (479142-1916566)110378 (252634-1010534)6CompoundFlagPyreneButylbenzyiphthalateJJ3 .3'-DichlorobenzidineJBenzo (a)anthraceneJChryseneJBis(2-ethylhexyl)phthalateDi-noctylphthalateBenzo (b)fluorantheneJJJBenzo (k)fluorantheneJBenzo (a)pyreneIndeno (1 .2.3-cd)pyreneDibenz(a.h)anthraceneJJJBenzo (g,h,i)peryleneJLaboratory Data Consultants . Inc .Review of Analytical DataSample99-GAM-011 -SL99-GAM-01 2-SL99-GAM-013-SLGambell HTW, Debris RemovalInternal StandardsPerylene-d12Perylene-dl 2Perylene-d12Area (Umtts)186395 (252634-1010534)243384 (252634-1010534)191381 (252634-1010534)CompoundDi-n-octylphthalateJBenzo (b)fluorantheneBenzo ( k)fluorantheneBenzo ( a)pyreneJPerylene-dl 2220558 (252634-1010534)JJJBenzo (g,h.)peMeneJDi-n-octylphthaiataBenzo ( b)fluorantheneBenzo ( k)fluorarttheneJJBenzo(a )pyreneIndeno (1,2.3cd) pyreneDibenz(a .h)anthraceneBenzo (g,h,)peryleneJJJDi-n-octylphthalateBenzo(k)fluorantheneJlndeno (1 .2.3-ed)pyreneJDibenz ( a.h)anthraceneBenzo (g,h,)peryleneJJDi-rwctylphthalateBenzo (b)fluorantheneJJJBenzo (g,h,i)perylene99-GAM-0I7-SLPerylene-dl2216575 (252634-1010534)238092 (252634-1010534)7JBenzo (a)pyreneDibenz(a.h)anthracenePerylene-d12JJJJBenzo (k)fluorantheneBenzo (a)pyreneIndeno (1,2,3cd)pyrene99-GAM-01 5SLJIndeno (1,2 .3-cd)pyre neDibenz(a.h)anthraceneBenzo( b)fluoranthene99-GAM-014-SLFlagJJJJDi-n-octylphthatateBenzo( b)fluorantheneBenzo( k)fluorantheneBenzo( a)pyreneIndeno(1 .2.3-cd)pyreneDibenz( a.h)anthraceneJJJJJBenzo (g .h,i)peryleneJ01-n-octylphthalateBenzo (b)fluorartheneBenzo (k)fluorantheneJJJBenzo (a)pyreneJlndeno (1,2 .3cd)pyreneJDibenz (a.h)anthraceneBenzo (g .h.i)peryleneJJJLaboratory Data Consultants, Inc .Review of Analytical DataSample99-GAM-01 8-SLGambell HTW, Debris RemovalInternal StandardsPerylene-d12Area (Llmlts )237086 (252634-1010534)CompoundDi-n-octylphthalateBenzo(b)fluorantheneBenzo( k)fluorantheneBenzo(a)pyrenelndeno (1 .2.3-cd) pyreneDibenz ( a.h)anthraceneBenzo ( g,h,)perylene99-GAM-019-SL99-GAM-02r.--SLPerylene-d12Perylene-d12228312 (252634-1010534)232377 (252634-1010534)FlagJJJJJJJDi-noctylphthalateJBenzo (b)fluorantheneBenzo (k)fluorantheneBenzo (a)pyreneIndeno (1,2 .3cd) pyreneDibenz (a.h)an hraceneJBenzo ( g.h.)peryleneJDi-n-octylphthalateJBenzo ( b)fluorantheneBenzo ( k)fluorantheneJJBenzo(a)pyreneIndeno (1 .2,3cd) pyreneJJDibenz ( a .h)anthraceneJBenzo (g,h. )peryleneJJJJJSurrogates were diluted out in sample 99-GAM-016-SL . No data qualifications wereperformed based on diluted surrogate results .No field blanks were identified in these SDGs .Samples 99-GAM -014-SL and 99-GAM-015-SL were identified as field duplicates . Nosemivolatiles were detected in any of the samples .Samples 99-GAM-014-SL (original) and 99 -GAM-016-SL (referee) and samples 99-GAM015-SL ( original) and 99-GAM-016-SL (referee) were compared . No semivolatiles weredetected in any of the samples .VI . Organochlorine Pesticides by EPA SW 846 method 8081For GC Organochlorine Pesticides analysis, holding times, instrument calibrations,blanks, and all accuracy and precision results were within validation criteria with thefollowing exceptions :Finding 1 :Matrix spike ( MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable with the following exceptions :8 Laboratory Data Consultants . Inc .Review of Analytical DataGambell HTW. Debris RemovalSampl .--~All samples in SDGsCompoundAll TCL compounds064096 and 994255FindingNo MS/ MSD associated with thesesamples.CriteriaFlagMS/MSD required .NoneFor the samples listed in the table above, surrogate, laboratory control sample andlaboratory control sample duplicates were used to assess precision and accuracy . Sincethese were acceptable with the exceptions noted in this report, sample results were notqualified based on this finding . This is considered a protocol violation .Finding 2 :Laboratory control samples were reviewed for each matrix asapplicable . Percent recoveries (%R) and relative percent differences(RPD) were within QC limits with the following exceptions :LCS ID(Associate dSamples )S9908251 LCS/LCSDWI samples in SDG 064096)Action :CompoundLCS%R (Umits )LCSD% R (Umits )RPO(Umits)FlagEndosulfan sulfate64(65-138)64(65-138)-JSamples were qualified as estimated (J) as indicated above . This isconsidered a protocol violation .Surrogates were diluted out in samples 99-GAM-012-SL and 99-GAM-018-SL No dataqualifications were performed based on diluted surrogate results .No field blanks were identified in these SDGs .Samples 99-GAM-014-SL and 99-GAM-015-SL were identified as field duplicates . Nochlorinated pesticides were detected in any of the samples .Samples 99-GAM-014-SL (original) and 99-GAM-016-SL (referee) and samples 99-GAM015-SL (original) and 99-GAM-016-SL (referee) were compared . No chlorinated pesticideswere detected in any of the samples .VII . Polychlorinated Biphenyls by EPA SW 846 method 8082For GC Polychlorinated Biphenyls analysis, holding times, instrument calibrations, blanks,and all accuracy and precision results were within validation criteria with the followingexceptions :9Laboratory Data Consultants, Inc .Gambell HTW , Debris RemovalReview of Analytical DataFinding 1 :Surrogates were added to all samples and blanks as required by themethod . All surrogate recoveries (% R) were within QC limits with thefollowing exceptions :SampleColumnSurrogate%R (Umits )99-GAM-009-SLNot specfiedDecachlorobiphenyl130 (53-125)Action :CompoundFlagAll TCL compoundsJ (all detects)Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a protocol violation .Surrogates were diluted out in sample 99-GAM-018-SL . No data qualifications wereperformed based on diluted surrogate results .Finding 2 :Matrix spike (MS) and matrix spike duplicate ( MSD) samples werereviewed for each matrix as applicable with the following exceptions :SampleAll samples in SDGs064096 and 994255CompoundAll TCL compoundsFindingNo MS/MSD associated with thesesamples-CriteriaFlagMS/MSD required .NoneFor the samples listed in the table above, surrogate, laboratory control sample andlaboratory control sample duplicates were used to assess precision and accuracy . Sincethese were acceptable with the exceptions noted in this report, sample results were notqualified based on this finding . This is considered a protocol violation .No field blanks were identified in these SDGs .Samples 99 -GAM-014-SL and 99 -GAM-015-SL were identified as field duplicates . Nopolychlorinated biphenyls were detected in any of the samples with the followingexceptions :10Laboratory Data Consultants, inc .Review of Analytical DataGambell HTW, Debris RemovalConcentration (D .t.eticun limit) (mg/Kg)99-GAM-014-SLCompoundArodor-1260Dilution :Prep Date:Analysis data :0 .03170 .8988/ 20/998/22/990 .0034U99-GAM-015-SLDilution :0 .934Prop Data :8/20/99Analysis data: 8 /22/990 .01110 .0035UDifferenceDisagreement/Major DisagreementFactor (X)(D/MD)2.9-The comparability of the field duplicate sample data was considered technicallyacceptable.Samples 99-GAM-014-SL (original) and 9.3-GAM-016-SL (referee) and samples 99-GAM015-SL (original) and 99-GAM-016-SL (referee) were compared . No polychlorinatedbiphenyls were detected in any of the samples with the following exceptions :Concentration (D.t.cticwn limit) (mg/Kg)Compound99-GAM-014-SL99-GAM-016-SLDilution:0 .898Prop Data : 8/20/99Analysis data: 8/22/99D181utlon :1 .0Prop Date: 8/25/99Aasaiysis data: 9/7/99Factor (X)Disagreement/Major Disagreement(DMD)NC-Dlff . r.nceFactor (X)Disagreement/Major Disagreement(D/MD)NC-Difference-11For-12600.03170.0034U0.038U0.0038UConcentration (Det.cfios1an limit) (mg/Kg)99-GAM -0I5-SLCompoundArodor-1260Dilution :Prop Date:Analysis data :0 .9348/20/990 .01110 .0035U8/22/9999-GAM-0I6-SLD tlon :1 .0Pr+. p Date : 8/25/99Analysis data :9/7/990 .038U0 .038UThe comparability of the QA split sample data was considered technically acceptable .In cases where the detection limit of a non-detect result is greater than a detected result,the comparison of the data is not technically significant . These cases are flagged witha "NC" (not calculable) notation .11Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW, Debris RemovalVIII . Gasoline Range Organics by Alaska Method AK101For gasoline range organic analysis, holding times, instrument calibrations, blanks, fieldQC, and all accuracy and precision results were within validation criteria with thefollowing exceptions :Finding 1 : Surrogates were added to all samples and blanks as required by themethod . All surrogate recoveries ( %R) were within QC limits with thefollowing exceptions :SampleSurrogate%R (Umits )CompoundFlag99-GAM -009-SL4-8romofluorobenzene41 .8 (50 -150)Gasoline range organicsJ99-GAM -0 1 1 SL4-Bromoftuorobenzene47.2 (50-150 )Gasoline range organicsJ99-GAM-01 4-SL4-8ro mofluoro benzene37.2 (50-150)Gasoline range organicsJ99-GAM-01 5-SL4-8ro mofluoro benzene27.3 (50-150)Gasoline range organicsJ99-GAM -016-SL4-Bromofluorobenzene40(50-150)Gasoline range organicsJAction:Samples were qualified as estimated (J) as indicated above . This isconsidered a protocol violation .Finding 2 :Matrix spike (MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable with the following exceptions :SampleAll samples in SDGs064096 and 994255LCompoundGasoline range organicsFindingNo lu1S/MSD associated with thesesamples .CriteriaFlagMS/MSD required .NoneI--J1For the samples listed in the table above , surrogate, laboratory control sample andlaboratory control sample duplicates were used to assess precision and accuracy . Sincethese were acceptable with the exceptions noted in this report , sample results were notqualified based on this finding . This is considered a protocol violation .12Laboratory Data Consultants, Inc.Gambell HTW , Debris RemovalReview of Analytical DataSamples 99-GAM-027-SL and 99-GAM-028-SL were identified as trip blanks . No gasolinerange organics were found in these blanks with the following exceptions :Trip Blank ID99-GAM-027-SLConcentration ( mg/Kg)CompoundGasoline range organics12 .8Samples 99-GAM-014-SL and 99-GAM-015-SL were identified as field duplicates . Nogasoline range organics were detected in any of the samples .Samples 99-GAM-014-SL (original) and 99-GAM-016-SL (referee) and samples 99-GAM015-SL (original) and 99-GAM-016-SL (referee) were compared . No gasoline rangeorganics were detected in any of the samples .IX. Diesel Range Organics and Residual Range Organics by Alaska MethodsAK102/AK103For diesel range and residual range organic analysis , holding times , instrumentcalibrations , blanks , field QC, and all accuracy and precision results were withinvalidation criteria .Finding 1 : Method blanks were reviewed for each matrix as applicable . No totalpetroleum hydrocarbons as diesel contaminants were found in themethod blanks with the following exceptions :Method Blank IDExtractionDate5931 XXXMB8/24199CompoundDiesel range organicsConcentrationAssociated Samples4 .71 mg/KgAll samples in SDG 994255Sample concentrations were compared to concentrations detected in the method blanks .The sample concentrations were either not detected or were significantly greater ( >5Xblank contaminants) than the concentrations found in the associated method blanks withthe following exceptions :Sample99-GAM-011 SLCompoundDiesel range organics13ReportedConcentrationModified FinalConcentration20.5 mg/Kg20.5U mg/KgLaboratory Data Consultants. Inc .Gambell HTW, Debris RemovalReview of Analytical DataSample99-GAM-0I7SLCompoundDiesel range organicsReportedConcentrationModified FinalConcentration15 .3 mg/Kg15 .3U mg/KgFinding 2 : Surrogates were added to all samples and blanks as required by themethod. All surrogate recoveries (% R) were within QC limits with thefollowing exceptions :SampleS9908241 MBAction :SampleSurrogateo-Terphenyl%R (Limits)52(50-150)CompoundDiesel range organicsFlagJSamples were qualified as estimated (J) as indicated above . This isconsidered a protocol violation .Surrogate%R (Umits )CompoundFlag99-GAM-016-SLTriacontane160 (50- 150)Residual range organicsJ (all detects)99-GAM-014-SLn-Triacontane217 (50- 150)Diesel range organicsResidual range organicsJ ( all detects)J (all detects)99-GAM-019-SL5a-Androstanen-Triacontane176 (50- 150)189 (50- 150)Diesel range organicsResidual range organicsJ ( all detects)J (all detects)99-GAM-026-SLn-Triacontane186 (50-150)Diesel range organicsResidual range organicsJ (all detects)J (all detects)Action :Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a protocol violation .Surrogates were diluted out in samples 99-GAM-009-SL, 99-GAM-010-SL, and 99-GAM018-SL. No data qualifications were performed based on diluted surrogate results .Finding 3 :Matrix spike (MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable with the following exceptions :14Laboratory Data Consultants, Inc .Review of Analytical DataSampleAll samples in SDGs064096 and 994255Gambell HTW, Debris RemovalCompoundFindingDiesel range organicsResidual range organicsNo MSIMSD associated with thesesamples .CriteriaFlagMS/MSO required .NoneNOAeFor the samples listed in the table above, surrogate, laboratory control sample andlaboratory control sample duplicates were used to assess precision and accuracy . Sincethese were acceptable with the exceptions noted in this report, sample results were notqualified based on this finding . This is considered a protocol violation .No field blanks were identified in these SDGs .Samples 99 -GAM-014-SL and 99-GAM-0 15-SL were identified as field duplicates . Nodiesel range organics or residual range organics were detected in any of the sampleswith the following exceptions :Concentration ( Detectnon limit) (mg/Kg)99-GAM-014-SL99-GAM-015-SLDilution :Prep Date:Analysis date :0 .9528/24/998/28/99Diesel range organics84 .09 .91 U68.8Residual range organics59216 .4U303CompoundOfution :0 .872Prop Date:8/24/99Analysis date :8/28/99DifferenceDisagreement/ Major DisagreementFactor (X)(DMD)9 .91U1 .2-16.4U2 .0The comparability of the field duplicate sample data was considered technicallyacceptable .Samples 99-GAM-014-SL (original) and 99-GAM-016-SL (referee) and samples 99-GAM01 5-SL (original) and 99-GAM-016-SL (referee) were compared . No diesel range organicsor residual range organics were detected in any of the samples with the followingexceptions:3sLaboratory Data Consultants . Inc .Review of Analytical DataGambell HTW, Debris RemovalConcentration (Dst.rction limit) (mg/Kg)99-GAM - 014-SL99-GAM-016-SLDilution :0 .952Prep Date :Analysis date :8/24/998/28/99Diesel range organics84.010 .7U724 .6111 .2Residual range organics59217 .711270111.)2.2-1 .08/24/998/28/99DifferenceDisagreement/Major Disagreement(D/MD)724 .6111 .0270111.11 .1Compound1 .0Dilution:6/24/99Prep Date :Analysis date : 8/28/99DifferenceFactor (X)Disagreement/Major Disagreement(D/MD)Concentration ( Detraction limit) (mg/Kg)99-GAM-015-SL 99-GAM-016-SLDilution :0 .872 ( Dilution:Prep Date : 8/24/99 Prep Date :Analysis data :8/28/99 Analysis date :CompoundDiesel range organics68 .89.91Residual range organics30316 .41- -- IU-Factor (X)JThe comparability of the QA split sample data was considered technically acceptable .X. Metals by EPA SW 846 Methods 6010 and 7000For metals analysis, holding times, instrument calibrations, instrument performancechecks, blanks, internal standards, and all accuracy and precision results were withinvalidation criteria with the following exceptions :Finding 1 :Method blanks were reviewed for each matrix as applicable . Dataqualification by the preparation blanks (PBs) was based on themaximum contaminant concentration in the PBs in the analysis of eachanalyte . No contaminant concentrations were found above the IDL inthe initial, continuing and preparation blanks with the followingexceptions :1 6 Laboratory Data Consultants, Inc .Gembell HTW, Debris RemovalReview of Analytical DataMethod Blank IDICB/CCSAnalyt.TAssociate d SamplesLead0.1 ugJL1 .3 ug/L99-GAM-009-SL99-GAM-01 0SL99-GAM-011 SL99-GAM-01 2-SL99-GAM-013-SLBarium0.2 ug/LChromium.5 ug/L299-GAM-014-SL99-GAM-01 5-SL99-GAM-01 7-SLCadmiumICB/CCBMaximumConce ntration99-GAM-018-SL99-GAM-019-SL99-GAM-026-SLSample concentrations were compared to the maximum contaminant concentrationsdetected in the PBs . The sample concentrations were either not detected or weresignificantly greater ( >5X blank contaminants) than the concentrations found in theassociated method blanks .Finding 2 :Matrix spike (MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable .SampleAna"TFindingAll samples in SDGCopperNo MS /MSD associated with these064096Antimonysamples.All samples in SDG064096All TAL metalsNo MS / MSD associated with thesesamples.CriteriaFlagMS/MSD required.NoneNoneMS/ MSD required.NoneFor the samples listed in the table above, laboratory control samples were used toassess precision and accuracy . Since these were acceptable, sample results were notqualified based on this finding . This is considered a protocol violation .Finding 3 : Matrix spike (MS) and matrix spike duplicate ( MSD) percent recoveries(%R) and relative percent differences (RPD) were within QC limits withthe following exceptions:17Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW , Debris RemovalSpike ID(AssociatedSamples )MS (%R)MSD (%R)RPD(Limits )( Limits)(Limits)Flag-JAnalyteE9H21 01 61-002MS /MSD(All samples in SOG 064096)Cadmium77 (75-125)Samples were qualified as estimated (J) as indicated above . This isconsidered a technical deficiency .Action :Spike ID(AssociatedSamples )AnalyteE9H21 01 61-002MS/MSD(All samples in SOG 064096)Action:ChromiumLeadMS (%R)(Limits)MSD (%R)( Limits )RPD( Limits)Flag155 (75-125)268 (75-125)198 (75-125)-J (all detects)J (all detects)Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a technical deficiency .No field blanks were identified in these SDGs .Samples 99-GAM-014-SL and 99-GAM-015-SL and samples were identified as fieldduplicates . No metals were detected in any of the samples with the following exceptions :Concentration ( Detection limit) (mg/Kg)99-GAM-014-SLAna"Dilution :Prop Date :Analysis date :1, 10, 2008/26/998125-31,9999-GAM-015-SLDilution :1, 4, 100Prop Date: 8/26/99Analysis date :8/25-31 /99Factor ( X)Disagreement/ Major Disagreement(D/MD)DIfferenceArsenic1 .750 .0492U1 .600 .0492U1 .1-Barium57 .30 .0550U66.70 .0550U1 .2-Cadmium0.6590 .0072U1 .570 .0072U2.4OChromium13 .20.0532U23.90.053201 .8Lead2120.0615U3110.0615U1 .518-Laboratory Data Consultants . Inc .Review d Analytical DataGambell HTW, Debris RemovalConcentration (Detection limit) (mg/Kg)99-GAM-014-SLAnalyt.Dilution : 1, 10, 200Prop Date :8/25/99Analysis date : 8/25-31 /9999-GAM-015-SLDilution : 1, 4, 100Prep Data :8/26/99Analysis date : 8/25-31199Diffe renceFactor (X)Disagreement/Major Disagreement(D/MD)Mercury0 .1010.005U0 .1150.005U1 .1Selenium0 .12700.127U0 .4020 .0724U3 .2MD1 .620 .0069U0.1690.0069U9 .6MODifferenceFactor (X)Disagreement/Major Disagreement(D/MD)SilverConcentration ( Detection limit) ( mg/Kg)99-GAM-020-SLAnalyt.Dilution : 1,10Prep Date:8/26,9/2/99Analysis date : 8 /25-9/3 /9999-GAM-021-SLDilution : 1,10Prop Oat. : 8/26,9/2/99Analysis date :8/25-9 /3/99Arsenic0.9780 .0492U0 .6420 .049201 .5-Cadmium0 .09650.007200 .09270 .0072U1 .0-Copper63.90.335033.20 .33501 .9Lead16.10 .0615U22.20.0615U1 .4-The comparability of the field duplicate sample data was considered technicallyacceptable with the exceptions of Cadmium, Selenium, and Silver in sample pair 99GAM-014-SL and 99-GAM-015-SL . No specific reason for this difference was identifiedduring the review of QA/QC results . For the soil samples, sample homogeneity orsubsampling could possibly account for this problem .Samples 99-GAM-014-SL (original) and 99-GAM-016-SL (referee) and samples 99-GAM01 5-SL (original) and 99-GAM-016-SL (referee) were compared . No metals were detectedin any of the samples with the following exceptions :19Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW, Debris RemovalConcentration ( Detection limit) (mg/Kg)99-GAM-014-SLAna"Dilution :1, 10, 200Prop Date : 8/26/99Analysis date:8/25-31 /9 999-GAM-0I 6-SLDillution :1, & 2Prop Date : 8/23/99Analysis date :8/24-25/99Factor (X)Disagreement/Major Disagreement(DMD)DifferenceArsenic1 .750 .049208 .32.31)4 .7MDBarium57 .30.0550057 .04 .6111 .0-Cadmium0.6590.007201 .201 .20NCChromium13 .20.0532024 .72 .301 .9-Lead2120.06151)1971 .201 .1-Mercury0 .1010.00500 .12O.10U1 .2Selenium0.127U0.07241)1 .31 .2010.21 .620 .00691)2.302.30NCSilverMDConcentration (Detection limit) (mg/Kg)99-GAM-015-SLAnalyt.Dilution :Prop Date :Analysis date:1, 4, 1008/26/998/25-31 /9999-GAM-0I 6-SLDiiu6on : 1, & 2Prop Date:8/23/99Anatysis date :8/24-25 /9 9Factor (X)Disagreement/Major Disagreement(DMD)MDDiffe renceArsenic1 .600.049208.32 .305 .2Barium66.70.0550U57.04 .601 .2Cadmium1 .570 .007201 .21)1 .2U1 .3-Chromium23 .90 .0532024 .72.301 .0-Lead3110 .0615U1971 .201 .620Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW, Debris RemovalConcentration ( Detection limit) (mg/Kg)99-GAM-0 15-SLDilution :AnalytePrep Date:Analysis data :1, 4, 1008/26/998125-31/9999-GAM-01 6-SLDilrotion :1, & 28/23/99Prop Date:Analysis date: 8/24-25 /99DifferenceFactor (X)Disagreement/Major Disagreement(D/MD)Mercury0.1150.00500 .120.1001 .0Selenium0.4020 .0724U1 .31 .2U3 .2DSilver0.1690.006902 .31)2 .30NC.DifferenceFactor (X)Disagreement/Major Disagreement(DMD)Concentration ( Detection limit) ( mg/Kg)99-GAM -020-SLAna"Dilution : 1,10Prep Date :8/26,9 /2/99Analysis date:8/25-9 /3/9999-GAM-022-SLDilution :IPrep Date :8/23/99Analysis date: 8/25/99Arsenic0.9780 .049201 .11 .001 .1Cadmium0.09650 .007200 .63U0.631)NC-Copper63 .90 .335065 .71 .001 .0-Lead16.10.0615036 .50 .50(12.3DDifferenceFactor (X)Disagreement/Major Disagreement(DMD)Concentration ( Detection limit) (mg/Kg)99-GAM -021-SLAnalyteDilution : 1,10Prep Date:8/26,9/2 /99Analysis date: 8125-9/3/9999-GAM-022-SLDiluon :IPrep Date : 8/23/99Analysis date :8/25/99Arsenic0 .6420 .049201 .11 .001 .7-Cadmium0 .09270 .0072U3.631.10.630NC-Copper33 .20 .335U-65.71 .01)2 .0-21Laboratory Data Consultants, Inc .Review of Analytical DataGanibeil HTW, Debris RemovalConcentration ( Detection limit) (mg/Kg)99-GAM-021-SLDilution:Prep Date :Analyt.1,108/26,9 / 2/99Analysis date :8 /25-9/3/99Lead22.20.06151.199-GAM-022-SLDilution :IProp Date:8/23/99Analysis date :8 / 25/9936.5DifferenceDisagreement/Major DisagreementFactor (X)(D/MD)0 .50U1 .6The comparability of the QA split sample data was considered technically acceptablewith the exceptions of Arsenic and Selenium in sample pair 99-GAM-014-SL and 99-GAM016-SL, Arsenic, Selenium, and Silver in sample pair 99-GAM-015-SL and 99-GAM-016SL, and Lead in sample pair 99-GAM-020-SL and 99-GAM-022-SL . No specific reason forthis difference was identified during the review of CA/QC results . For the soil samples,sample homogeneity or subsampling could possibly account for this problem . In caseswhere the detection limit of a non-detect result is greater than a detected result, thecomparison of the data is not technically significant . These cases are flagged with a "NC"(not calculable) notation .XI . Dioxins by EPA SW 846 Method 8290For HRGC/HRMS dioxin/dibenzofuran analysis, holding times, instrument calibrations,instrument performance checks, blanks, internal standards, field QC, and all accuracyand precision results were within validation criteria with the following exceptions :Finding 1 :All of the routine calibration percent differences (%D) between theinitial calibration RRF and the routine calibration RRF were less thanor equal to 20 .0% for unlabeled compounds and less than or equal to30.0% for labeled compounds with the following exceptions :Dab9/4/99Compound"C-OCOD%OAssociated Samples32Method blankFlagJAction :Samples were qualified as estimated (J) as indicated above. This isconsidered a protocol violation .Finding 2:Method blanks were reviewed for each matrix as applicable . Nopolychlorinated dioxin /dibenzofuran contaminants were found in themethod blanks with the following exceptions :22Laboratory Data Consultants, Inc .Gambeil HTN , Debris RemovalReview of Analytical DataMethod Blank IDExtractionDateMethod blank8/25/99TU BlankCompoundConcentrationAssociated SamplesAli samples in SDG 0640961,2.3 .4,6 .7,8-HpCDD3 .3 pgjgTotal HpC00OCOD3 .3 pg/g1 ,2,3 .4,6.7,8-HpCOD0 .80 pg/goC002,3,7 .8-TCDF0.81 pg/g0.76 pg/g0.71 p9/91 .7 p9/g0.80 P9/90.76 pg/g0.71 Mg8/29/997 .0 pgjg1,2,3 .4,6.7 .8-HpCDFTotal HxCODTotal HpCDOTotal TCDFTotal HpCDFAY samples in SDG 994255Sample concentrations were compared to concentrations detected in the method blanks .The sample concentrations were either not detected or were significantly greater ( >5Xblank contaminants) than the concentrations found in the associated method blanks withthe following exceptions :SampleCompoundReportedModified FinalConcentrationConcentration3 .5U pg/g99-GAM-020-SL2.3 .7 .8-TCDF3.5 pgjg99-GAM-025-SL1,2 .3 .4,6.7.8-HpCD01,2 .3 .4 .6.7.8-HpCDFTotal HpCDD1 .3 pg/g1 .31 .1 pg/g2.4 pgjg2.4U pg/92.3 pg/g2.3U pgjgTotal HxCDD6.6 pg/g6 .6U pgjg99-GAM-024-SLFinding 3 :Matrix spike (MS) and matrix spike duplicate (MSD) samples werereviewed for each matrix as applicable with the following exceptions:SampleAll samples in SDGs064096 and 994255CompoundAll TCL compoundsFindingNo MS/MSD associated with thesesamples .23CriteriaFlagMS /MSD required .NoneLaboratory Data Consultants, Inc .Review of Analytical DataGambell HTW, Debris RemovalFor the samples listed in the table above, laboratory control samples were used toassess precision and accuracy . Since these were acceptable with the exceptions notedin this report, sample results were not qualified based on this finding . This is considereda protocol violation .Finding 4 :All internal standard recoveries were within QC limits with the followingexceptions :Sample99-GAM-021 -SL99-GAM-023-SLInternal Standards%R (Limits)"C-1 .2,3 .4,6,7,8-HpCDD146 (25-130)"C-1 .2,3,4,6.7,8-HpCDO150 (25-130)CompoundFlag1,2 .3.4,6 .7,8-HpCDDTotal HpCDDJ (all detects)J ( al detects)1 .2.3,4,6,7,8-HpCDDJ (all detects)Total HpCDDJ (all detects)Action : Sample results reported as detectable were qualified as estimated (J) asindicated above . This is considered a protocol violation .No field blanks were identified in these SDGs .Samples 99-GAM-020-SL and 99-GAM-021-SL were identified as field duplicates . Nopolychlorinated dioxins /dibenzofurans were detected in any of the samples with thefollowing exceptions :Concentration ( Detection limit) (ppt)Compound99-GAM-020-SL99-GAM-021-SLDilution :IPrep Date :8/29/99Analysis date :9/11/99Dilution:1Prep Date : 8/29/99Analysis date:9/11/99Dtffer. nceFactor (X)1,2 .3,7 .8-PeCDD2 .6-2.2-1 .21,2 .3,4,7.8-HxCDD3 .8-3.0-1 .31 .2 .3,6,7,8-HxCDD14 .1-8.9-1 .61,2 .3,7,8,9-HpCDD10 .9-8.2-1 .31,2,3 .4,6,7.8-HpCDD266-151-1 .824Disagreement/Major Disagreement(D/MD)-Laboratory Data Consultants . Inc .Review of Analytical DataGambol] HTW, Debris RemovalConcentration ( Detection limit) (ppt)Compound99-GAM -020-SL99- GAM-021-SLDilution :IProp Date :8/29/99Analysis date :9 /11/99Dilution :1Prop Data : 8/29/99Analysis data :9/11/99Dlttersnc.Factor () )Disagreement/Major Disagr. .m .nt(D/MD)1 .6-OCOD1250-8002 .3 .7.8-TCDF0 .74-0 .92-1 .21,2.3,7, 8-PeCDF0.6U0.6U0 .97 EMPC'-1 .6-2 .3,4,7, 8-PeCDF1 .2-1 .7-1 .4-1,2.3,4.7, 8-HxCDF4 .3-4 .6-1 .11,2.3,6,7,8d-ixCDF1 .7-1 .8-1 .1-2.3,4,6,7,8-HxCOF2.9-2.9-1-1,2.3 .4, 6,7.8-HxCDF107-74 .1-1 .4-1 .2.3,4, 7,8,9-HpCDF6.5-4.8-1 .4OCOF596-436-1 .4Total TCDD1 .7-1 .5-1 .1-Total PeCOD24 .3-19.1-1 .3-Total HxCDD97 .9-67.1-1 .5-Total HpCDD461-263-2-Total TCDF24 .9-26.7-1 .1Total PeCDF8.6-12.8-1 .525-Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW . Debris RemovalConcentration (Dwtection limit) (ppt)Compound99-GAM-020-SL99-GAM-021 -SLDilution:IPrep Date : 8/29/99Analysis date : 9/11/99Dilution :1Prep Date : 8/29/99Analysis date : 9/11/99DifferenceFactor (X)Total HxCOF85 .5-59 .4-1 .4Total HpCDF526-362-1 .5Disagreement/Major Disagreement(D/MD)_•EMPC = estimated maximum possible concentrationThe comparability of the field duplicate sample data was considered technicallyacceptable .Samples 99 -GAM-020-SL ( original ) and 99-GAM-022- SL (referee) and samples 99-GAM021-SL ( original ) and 99-GAM-022-SL (referee) were compared . No polychlorinateddioxins / dibenzofurans were detected in any of the samples with the following exceptions :Concentration (D .. action limit) (ppt)Compound99-GAM -020-SL99-GAM-022-SLDilution :IPrep Date :8/29/99Analysis date :9/11/99Dilution :IPrep Data:8/25/99Analysis date : 9/11/99DifferenceDisagreement/Major DisagreementFactor (X)(D/MD)2,3,7.8-TCOD0 .8U0.8U0 .60-NC-1,2 .3 .7,8-PeCDD2 .6-2 .2U2.2U1 .2-1,2.3,4,7,8-HxCDD3 .8-3 .3-1 .2-1,2.3,6.7,8-HxCDD14 .1-12-1 .2-1,2.3,7,8,9-HxCDD10 .95 .1-2.1-1 .2.3 .4 .6.7,8-HpCDO266250-1 .1-OCOD12501100-1 .1--26Laboratory Data Consultants, Inc .Review of Analytical DataGambol[ H1W, Debns RemovalConcentration (Detection limit) (ppt)Compound99-GAM-020-SL99-GAM-022-SLDilution :1Prop Date :8/29/99Analysis date : 9/11/99Dilution :1Prop Date :8/25/99Analysis date :9/11/99Factor (X)Disagreement/Mayor Disagreement(D/MD)Difference2,3,7,8-TCOF0.74-1 .2-1 .6-2,3,4 .7 .8-PeCOF1 .2-1 .5U1 .5UNC-1 .2,3,4,7.8-HxCDF4 .3-2.9U2.9U1 .5-1,2,3,6 ,7,8-HxCDF1 .7-2.1U2 .1UNC-2,3,4,6,7,8-HxCDF2.9-1 .8U1 .8U1 .61,2 .3.4,6,7 .8-HpCOF107-96-1 .1-1,2 .3.4,7,8 .9-HpCDF6.5-5.0-1 .3-OCDF596-570-1-Total TCDD1 .7-7 .6-4 .5DTotal PeCOD24 .3-4.5U4 .5U5 .4MDTotal HxCDD97 .9-68-1 .4Total HxCDD461-430-1 .1Total TCOF24 .9-47•-1 .9Total PeCOF8 .6-11-1 .3Total HxCOF85 .5-61-1 .4-Total HpCOF526-470-1 .1-27-Laboratory Data Consultants, Inc .Review of Analytical DataGambeli HTW , Debris Remove)Concentration (D.t.ction limit) (ppt)99-GAM - 021-SL99-GAM-022-SLDilution :Prop Date :Analysis date :18/29/999 / 11/992 .3,7,8-TCDD0 .6U0.6U0.60-11,2.3 .7, 8-PeCOD2.2-2.2U-I1,2,3 .4, 7,8-HxCOD3 .0-3 .3-1 .11,2,3 .6,7,8-HxCDD8.912-1 .31,2,3 .7, 8 .9-HxCDD8.2-5 .1-1 .61 .2.3,4 .6 .7 . 8-HpCDO151-250-1 .7OCDD800-1100-1 .42.3,7 , 8-TCDF0 .92-1 .21,2.3,7, 8-PeCOF0.97 EMPC •-1 .6U1 .6UNC2.3 .4 .7, 8-PeCOF1 .7-1 .51)1 .5U1 .11,2.3 .4,7,8-HxCDF4 .6-2 .91)-1 .61,2 .3.6 .7.8 -HxCDF1 .8-2.1U-NC2,3 .4,6,7,8-HxCDF2 .9-1 .81)-1 .6-1,2 .3,4 , 6.7,8-HpCOF74 .196-1 .3-1,2,3.4 .7,8 .9-HpCOF4 .8-5.0-1OCDF436-570-1 .3CompoundDilution :IProp Data: 8/25/99Analysis date :9/11/99DifferenceFactor ( X)1 .3Disagreement/Major Disagreement(DMD)•--28 Laboratory Data Consultants, Inc .Review of Analytical DataGambell HTW, Debris RemovalConcentration ( Detection limit) (ppt)99- GAM-022-SL99-GAM-021-SLCompoundDilution :IProp Oats :8/29/99Analysis date :9/11/99Dilution :Prep Date :Analysis date :18/25/999/11/99OlfforoncsFactor (X)Disagreement/Major Disagreement(D/MD)Total TCOO1 .5-7 .6-5 .1MDTotal PeCOD19 .1-4 .5U4.5U4 .2DTotal HxCDD67.1-68-1-Total HpCDD263-4301 .6-Total TCDF26.7-471 .7-Total PeCOF12.8-11-1 .2-Total HxCOF59 .4-61-1-Total HpCDF362-470-1 .3-•EMPC = estimated maximum possible concentrationThe comparability of the QA split sample data was considered technically acceptablewith the exceptions of Total TCDD and Total PeCDD in sample pair 99-GAM-020-SL and99-GAM-022-SL and sample pair 99-GAM-021-SL and 99-GAM-022-SL. No specificreason for these differences was identified during the review of QA/QC results . For thesoil samples, sample homogeneity or subsampling could possibly account for thisproblem . In cases where the detection limit of a non-detect result is greater than adetected result, the comparison of the data is not technically significant . These cases areflagged with a "NC" (not calculable) notation .29Laboratory Data Consultants . Inc .